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1. 发明公开

EP1324034A1 METHOD AND APPARATUS FOR CONTINUOUS FRACTIONAL ANALYSIS OF METALLIC MERCURY AND WATER-SOLUBLE MERCURY IN A GAS 有权
标题翻译：方法在气体金属汞与水汞的连续的部分分析
公开(公告)号：EP1324034A1
公开(公告)日：2003-07-02
申请号：EP01941201.4
申请日：2001-06-25
申请人： Central Research Institute of Electric Power Industry , Nippon Instruments Corporation
发明人： NODA, Naoki Central Research Institute of Electric , ITO, Shigeo Central Research Institute of Electric , MARUMOTO, Koji Central Res. Institute of Electric , TANIDA, Koji, c/o Nippon Instruments Corporation , HOSHINO, Munehiro, Nippon Instruments Corporation
IPC分类号： G01N31/00 , G01N1/22
CPC分类号： G01N33/0045 , G01N1/2214 , G01N1/2247 , G01N2001/2217 , G01N2001/227 , G01N2001/4066 , Y10T436/25375 , Y10T436/255 , Y10T436/25875
摘要： A method and an apparatus which continuously separate and measure mercury in an exhaust gas in accordance with each chemical conformation and display a measurement result in real time. According to the method and the apparatus, water-soluble mercury in a gas is absorbed into an absorption solution (7), the gas and the absorption solution (7) are then separated from each other, the water-soluble mercury in the absorption solution (7) is reduced to be converted into gaseous metal mercury and led to an analyzer (20), and metal mercury in the gas which is not absorbed into the absorption solution (7) is led to an analyzer (22) in the form of gas. As a result, the water-soluble mercury and the non-water-soluble mercury contained in the gas can be captured and measured/analyzed in respective measurement systems in accordance with each chemical conformation. In addition, a concentration of the metal mercury and that of the water-soluble mercury in the gas can be continuously monitored in real time. In this analysis, it is preferable to use the absorption solution (7) to absorb an acid gas which is an inhibitive component to mercury measurement, together with the water-soluble mercury.
摘要翻译：一种方法和装置，以它连续地在排气中雅舞蹈与每个化学构象分离和测量汞和实时显示的测量结果。。根据该方法和装置中，在气体中的水溶性汞被吸收到吸收溶液（7），气体和吸收溶液（7）然后，从海誓山盟分离，在吸收溶液中的水溶性汞（7）还原为被转换成气态金属汞，并导致在分析仪（20）和金属汞的气 - 所有这些都没有被吸收到吸收溶液（7）被引导到在形式分析仪（22）气体。其结果是，该水溶性汞和气体中所含的非水溶性汞可以被捕获并测量/在respectivement测量系统中分析雅舞蹈与每个化学构象。此外，金属汞的浓度，并做了水溶性汞的气体中可以连续地实时监测。在该分析中，它是优选使用的吸收溶液（7）在酸性气体吸收在所有这是抑制成分汞测定，水溶性汞在一起。

2. 发明公开

EP1489412A1 Method and apparatus for measuring mercury contained in gaseous medium 审中-公开
标题翻译：对包含在气态介质中汞的连续测量的方法和装置
公开(公告)号：EP1489412A1
公开(公告)日：2004-12-22
申请号：EP04252111.2
申请日：2004-04-08
申请人： Central Research Institute of Electric Power Industry , Nippon Instruments Corporation
发明人： Makino, Hisao , Shirai, Hiromi
IPC分类号： G01N33/00 , B01D53/86 , B01D15/08
CPC分类号： B01D53/8665 , G01N33/0045
摘要： To provide a method of and an apparatus for continuously measuring elemental mercury and bivalent mercury both contained in a gaseous medium fractionally with a simplified structure, the concentration of a total mercury (Metallic Mercury + Bivalent Mercury) and the concentration of elemental mercury contained in gases are measured continuously and fractionally. In the practice of this mercury measuring method, a first column 1, filled with a first fixed catalyst, and a second column 11, filled with a second fixed catalyst, are fluid connected in parallel relation to each other. The gases G are introduced into those first and second columns 1 and 11. In the first column 1, the first fixed catalyst collects and removes the bivalent mercury, but passes only the elemental mercury in the gases through the first column. In the second column 11, the second fixed catalyst reduces the bivalent mercury into elemental mercury and passes through the second column 11 the elemental mercury in the gases containing the elemental mercury into which the bivalent mercury has been reduced. The concentration of the elemental mercury in the gases, from which the bivalent mercury has been removed after passage thereof through the first column 1 and, also, the concentration of the elemental mercury in the gases into which the bivalent mercury has been reduced after passage thereof through the second column 11 are measured as the concentration of the elemental mercury contained in sampled gases and as the concentration of the total mercury in the sampled gases, respectively by utilization of first and second mercury measuring instruments.
摘要翻译：为了提供和设备的方法用于连续地测量元素汞和二价汞都包含在具有简化的结构分馏气态介质中，包含在气体完全汞（金属汞+二价汞）的浓度和元素汞的浓度连续和分级测定。在这种汞测量方法中，第一塔1，填充有第一固定催化剂，和第二列11，填充有第二固定催化剂的实践中，是流体连接以平行关系海誓山盟。的气体G引入这些第一和第二列1和11在第一列1中，第一固定催化剂收集和移除二价汞，而是通过第一列中的气体中仅通过单质汞。在第二列11，第二固定催化剂降低了二价汞成元素汞和穿过第二塔11含元素汞成二价汞已经减少的气体中的元素汞。的气体中的元素汞，从该二价汞通道之后通过第一柱1和它们的被除去的浓度，因此，在气体中的元素汞的浓度到其中的二价汞已被通道及其后减压通过第二柱11测量值：载采样气体中和作为总汞的采样气体中，分别由第一和第二汞测量仪器的利用率浓度元素汞的浓度。

4. 发明申请

US20130236361A1 HEATING COMBUSTION TUBE, PYROLYSIS APPARATUS AND MERCURY ANALYZING APPARATUS IN ANALYSIS OF MERCURY 审中-公开
标题翻译：加热燃烧管，热分析装置和汞分析装置在汞分析中的应用
公开(公告)号：US20130236361A1
公开(公告)日：2013-09-12
申请号：US13988982
申请日：2011-10-24
申请人： Tomoaki Watanabe , Ryuta Kurokawa , Tadashi Nakatani , Koji Tanida , Shintaro Kotake
发明人： Tomoaki Watanabe , Ryuta Kurokawa , Tadashi Nakatani , Koji Tanida , Shintaro Kotake
IPC分类号： G01N31/12
CPC分类号： G01N31/12 , G01N21/3103 , G01N21/6404 , G01N33/0045
摘要： A heating combustion tube 20 of the present invention is used in analysis of mercury in a heated state and includes a sample pyrolysis portion 10 in which a sample S is heated and decomposed, an oxidization portion 11 in which a fourth period metal oxide 13, which is a metal oxide in the fourth period on the periodic table, and a treating portion 12 in which an alkali metal compound and/or an alkali earth metal compound 14 is filled.
摘要翻译：本发明的加热燃烧管20用于分析处于加热状态的汞，并且包括其中样品S被加热和分解的样品热解部分10，其中第四周期金属氧化物13的氧化部分11，其中是元素周期表中的第四周期中的金属氧化物，其中填充有碱金属化合物和/或碱土金属化合物14的处理部分12。

5. 发明授权

US08223332B2 Mercury measuring apparatus for measuring mercury contained in sample composed mainly of hydrocarbon 有权
标题翻译：用于测量主要由碳氢化合物组成的样品中汞含量的汞测量装置
公开(公告)号：US08223332B2
公开(公告)日：2012-07-17
申请号：US12674354
申请日：2008-08-19
申请人： Yasuyuki Yamada , Munehiro Hoshino
发明人： Yasuyuki Yamada , Munehiro Hoshino
IPC分类号： G01J3/42 , G01N25/00 , G01N37/00
CPC分类号： G01N33/2835 , G01N1/4044 , G01N1/405 , G01N21/6404 , G01N2021/3107
摘要： To provide a mercury measuring apparatus of a closed system capable of performing automatically a process ranging from collection to injection of the sample composed mainly of hydrocarbon, which is effective to accomplish a highly reliable measurement. The mercury measuring apparatus 100 includes a column 1 filled with a first adsorbent 11 and a reducing agent 13, an injecting unit 3 for injecting a sample into the column 1, a first heating unit 12, a second heating unit, a mercury collecting tube 18 filled with a second adsorbent 17, a third heating unit 19, a mercury measuring unit 2, gas flow passages FP1, FP2 and FP4, flow switching valves V1 to V3, V5 and V6 for selecting one of the gas flow passages FP1, FP2 and FP4, and a control unit 4.
摘要翻译：提供一种封闭式系统的水银测量装置，其能够自动执行从主要由烃组成的样品的收集到注入的过程，其有效地实现高度可靠的测量。汞测量装置100包括填充有第一吸附剂11和还原剂13的柱1，用于将样品注入柱1的注入单元3，第一加热单元12，第二加热单元，汞收集管18 填充有第二吸附剂17，第三加热单元19，汞测量单元2，气体流路FP1，FP2和FP4，用于选择气体流路FP1，FP2中的一个的流量切换阀V1〜V3，V5，V6， FP4和控制单元4。

6. 发明授权

US07928033B2 Catalyst for reducing mercury, a mercury conversion unit, and an apparatus for measuring total mercury in combustion exhaust gas by using the same 有权
标题翻译：用于还原汞的催化剂，汞转化单元，以及通过使用它们来测量燃烧废气中的总汞的装置
公开(公告)号：US07928033B2
公开(公告)日：2011-04-19
申请号：US11724540
申请日：2007-03-15
申请人： Shigeyuki Akiyama , Junji Kato , Fujio Koga , Koji Ishikawa
发明人： Shigeyuki Akiyama , Junji Kato , Fujio Koga , Koji Ishikawa
IPC分类号： B01J27/00 , B01J27/02 , B01J27/055 , B01J21/18 , B01J27/20 , B01J20/00 , C01G11/00 , C01G9/00 , B01D47/00 , B01D53/46 , B01D53/56 , B01D53/02 , C01B17/42 , C01B31/24 , C01D5/00 , C01D15/06 , C01D17/00 , C01D7/00 , C01F5/42 , C01F11/46 , C01F5/24 , A62D3/30 , A62D3/36 , A62D3/40
CPC分类号： G01N21/33 , G01N21/74 , Y10S95/90 , Y10S95/901
摘要： The present invention relates to a catalyst for reducing mercury, which comprises a reagent comprising any of the sulfites of potassium, sodium, calcium and magnesium, or any of the phosphates thereof, or a combination of them, as a main reagent of a catalyst component. And the present invention relates to the catalyst for reducing mercury, wherein the catalyst component is mixed with a different salt as an agent for inhibiting crystallization of the catalyst component.
摘要翻译：本发明涉及一种用于还原汞的催化剂，其包括试剂，其包含钾，钠，钙和镁的任何亚硫酸盐或其任何磷酸盐，或它们的组合作为催化剂组分的主要试剂。本发明涉及用于还原汞的催化剂，其中将催化剂组分与不同的盐混合，作为抑制催化剂组分结晶的试剂。

7. 发明申请

US20060137433A1 Apparatus for measuring mercury contained in gaseous medium 有权
标题翻译：用于测量气态介质中所含汞的装置
公开(公告)号：US20060137433A1
公开(公告)日：2006-06-29
申请号：US11305259
申请日：2005-12-19
申请人： Koji Tanida
发明人： Koji Tanida
IPC分类号： G01N33/00
CPC分类号： G01N31/005 , G01N33/0013 , G01N33/0045
摘要： To provide a highly reliable apparatus for measuring mercury contained in the gaseous medium, in which the outlet port 3b of the reducing tube and the gas-liquid separator, both susceptible to deposition of stain, can be automatically cleaned to avoid reduction of the sensitivity of the measuring instrument, the apparatus for measuring mercury contained in the gaseous medium includes a reducing tube 3 for reducing divalent mercury contained in a gaseous medium to zerovalent mercury, a gas-liquid separator 4 for removing a liquid component (drain) from the gaseous medium that has passed through the reducing tube 3, a measuring instrument 6 for measuring the quantity of the mercury contained in the gaseous medium delivered from the gas-liquid separator 4, and a cleaning system 10 for running a cleaning liquid from an outlet port of the reducing tube 3 past the gas-liquid separator 4 to emerge outwardly of the gas-liquid separator 4.
摘要翻译：为了提供用于测量包含在气体介质中的汞的高度可靠的装置，其中可以自动清洁可能被污染沉积的还原管和气液分离器的出口3b，以避免降低灵敏度测量仪器中包含的汞的测量装置包括用于将气态介质中所含的二价汞降低至零价汞的还原管3，用于从气体中去除液体组分（排出）的气液分离器4 已经通过还原管3的介质，用于测量从气液分离器4输送的气态介质中所含的汞的量的测量仪器6，以及用于将清洗液从出口还原管3经过气 - 液分离器4从气 - 液分离器4的外部露出。

8. 发明授权

US07367225B2 Apparatus for measuring mecury contained in gaseous medium 有权
标题翻译：用于测量包含在气体介质中的碎屑的装置
公开(公告)号：US07367225B2
公开(公告)日：2008-05-06
申请号：US11305259
申请日：2005-12-19
申请人： Koji Tanida
发明人： Koji Tanida
IPC分类号： G01N33/00
CPC分类号： G01N31/005 , G01N33/0013 , G01N33/0045
摘要： To provide a highly reliable apparatus for measuring mercury contained in the gaseous medium, in which the outlet port 3b of the reducing tube and the gas-liquid separator, both susceptible to deposition of stain, can be automatically cleaned to avoid reduction of the sensitivity of the measuring instrument, the apparatus for measuring mercury contained in the gaseous medium includes a reducing tube 3 for reducing divalent mercury contained in a gaseous medium to zerovalent mercury, a gas-liquid separator 4 for removing a liquid component (drain) from the gaseous medium that has passed through the reducing tube 3, a measuring instrument 6 for measuring the quantity of the mercury contained in the gaseous medium delivered from the gas-liquid separator 4, and a cleaning system 10 for running a cleaning liquid from an outlet port of the reducing tube 3 past the gas-liquid separator 4 to emerge outwardly of the gas-liquid separator 4.
摘要翻译：为了提供用于测量包含在气体介质中的汞的高度可靠的装置，其中可以自动清洁可能被污染沉积的还原管和气液分离器的出口3b，以避免降低灵敏度测量仪器中包含的汞的测量装置包括用于将气态介质中所含的二价汞降低至零价汞的还原管3，用于从气体中去除液体组分（排出）的气液分离器4 已经通过还原管3的介质，用于测量从气液分离器4输送的气态介质中所含的汞的量的测量仪器6，以及用于将清洗液从出口还原管3经过气 - 液分离器4从气 - 液分离器4的外部露出。

9. 发明申请

US20110299072A1 MERCURY MEASURING APPARATUS FOR MEASURING MERCURY CONTAINED IN SAMPLE COMPOSED MAINLY OF HYDROCARBON 有权
标题翻译：用于测量组合物主要成分的汞的汞测量装置
公开(公告)号：US20110299072A1
公开(公告)日：2011-12-08
申请号：US12674354
申请日：2008-08-19
申请人： Yasuyuki Yamada , Munehiro Hoshino
发明人： Yasuyuki Yamada , Munehiro Hoshino
IPC分类号： G01J3/42 , G01N25/00
CPC分类号： G01N33/2835 , G01N1/4044 , G01N1/405 , G01N21/6404 , G01N2021/3107
摘要： To provide a mercury measuring apparatus of a closed system capable of performing automatically a process ranging from collection to injection of the sample composed mainly of hydrocarbon, which is effective to accomplish a highly reliable measurement. The mercury measuring apparatus 100 includes a column 1 filled with a first adsorbent 11 and a reducing agent 13, an injecting unit 3 for injecting a sample into the column 1, a first heating unit 12, a second heating unit, a mercury collecting tube 18 filled with a second adsorbent 17, a third heating unit 19, a mercury measuring unit 2, gas flow passages FP1, FP2 and FP4, flow switching valves V1 to V3, V5 and V6 for selecting one of the gas flow passages FP1, FP2 and FP4, and a control unit 4.
摘要翻译：提供一种封闭式系统的水银测量装置，其能够自动执行从主要由烃组成的样品的收集到注入的过程，其有效地实现高度可靠的测量。汞测量装置100包括填充有第一吸附剂11和还原剂13的柱1，用于将样品注入柱1的注入单元3，第一加热单元12，第二加热单元，汞收集管18 填充有第二吸附剂17，第三加热单元19，汞测量单元2，气体流路FP1，FP2和FP4，用于选择气体流路FP1，FP2中的一个的流量切换阀V1〜V3，V5，V6， FP4和控制单元4。

10. 发明授权

US07144736B2 Method and apparatus for continuous fractional analysis of metallic mercury and water-soluble mercury in a gas 有权
$Method and apparatus for continuous fractional analysis of metallic mercury and water-soluble mercury in a gas$
标题翻译：气体中金属汞和水溶性汞的连续分数分析方法和装置
公开(公告)号：US07144736B2
公开(公告)日：2006-12-05
申请号：US10363807
申请日：2001-06-25
申请人： Naoki Noda , Shigeo Ito , Koji Marumoto , Koji Tanida , Munehiro Hoshino
发明人： Naoki Noda , Shigeo Ito , Koji Marumoto , Koji Tanida , Munehiro Hoshino
IPC分类号： G01N33/20 , G01N21/33 , G01N21/01 , G01N1/22
CPC分类号： G01N33/0045 , G01N1/2214 , G01N1/2247 , G01N2001/2217 , G01N2001/227 , G01N2001/4066 , Y10T436/25375 , Y10T436/255 , Y10T436/25875
摘要： A method and an apparatus which continuously separate and measure mercury in an exhaust gas in accordance with each chemical conformation and display a measurement result in real time. According to the method and the apparatus, water-soluble mercury in a gas is absorbed into an absorption solution (7), the gas and the absorption solution (7) are then separated from each other, the water-soluble mercury in the absorption solution (7) is reduced to be converted into gaseous metal mercury and led to an analyzer (20), and metal mercury in the gas which is not absorbed into the absorption solution (7) is led to an analyzer (22) in the form of gas. As a result, the water-soluble mercury and the non-water-soluble mercury contained in the gas can be captured and measured/analyzed in respective measurement systems in accordance with each chemical conformation. In addition, a concentration of the metal mercury and that of the water-soluble mercury in the gas can be continuously monitored in real time. In this analysis, it is preferable to use the absorption solution (7) to absorb an acid gas which is an inhibitive component to mercury measurement, together with the water-soluble mercury.
摘要翻译：根据每个化学构型连续分离和测量废气中的汞并且实时显示测量结果的方法和装置。根据该方法和装置，气体中的水溶性汞被吸收到吸收溶液（7）中，然后将气体和吸收溶液（7）相互分离，吸收溶液中的水溶性汞（7）被还原成为气态金属汞并导致分析器（20），并且不吸收到吸收溶液（7）中的气体中的金属汞被引导到分析器（22）的形式加油站。结果，气体中所含的水溶性汞和非水溶性汞可以根据每种化学构型在相应的测量系统中被捕获和测量/分析。此外，可以实时地连续监测金属汞和气体中的水溶性汞的浓度。在该分析中，优选使用吸收溶液（7）与水溶性汞一起吸收作为汞测定的抑制成分的酸性气体。

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