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1. 发明申请

US20090182066A1 CROSSLINKABLE FLUOROPOLYMER, CROSSLINKED FLUOROPOLYMERS AND CROSSLINKED FLUOROPOLYMER MEMBRANES 失效
标题翻译：可交联氟聚合物，交联氟聚合物和交联氟聚合物膜
公开(公告)号：US20090182066A1
公开(公告)日：2009-07-16
申请号：US12344881
申请日：2008-12-29
申请人： Zhen-Yu Yang , Mark Gerrit Roelofs , Randal L. Perry , Amy Qi Han
发明人： Zhen-Yu Yang , Mark Gerrit Roelofs , Randal L. Perry , Amy Qi Han
IPC分类号： C08F214/26 , C08F279/00 , C08J3/28 , B05D5/12
CPC分类号： C08F214/00 , C08F8/00 , C08J5/2237 , C08J2327/18 , H01M4/623 , H01M8/1023 , H01M8/1039 , H01M8/1072 , H01M10/0565 , H01M2300/0082 , Y02P70/56 , C08F214/26 , C08F210/02
摘要： Crosslinkable polymers and crosslinked fluoropolymers are prepared from selected fluorinated dienes and monomers containing Br and I. Also disclosed are proton conductive membranes of these crosslinked fluoropolymers.
摘要翻译：可选择的氟化二烯和包含Br和I的单体制备可交联的聚合物和交联的含氟聚合物。还公开了这些交联的含氟聚合物的质子传导膜。

2. 发明申请

US20100093878A1 CROSSLINKABLE FLUOROPOLYMER, CROSSLINKED FLUOROPOLYMERS AND CROSSLINKED FLUOROPOLYMER MEMBRANES 审中-公开
标题翻译：可交联氟聚合物，交联氟聚合物和交联氟聚合物膜
公开(公告)号：US20100093878A1
公开(公告)日：2010-04-15
申请号：US12344768
申请日：2008-12-29
申请人： ZHEN-YU YANG , Amy Qi Han , Mark Gerrit Roelofs , Randal L. Perry
发明人： ZHEN-YU YANG , Amy Qi Han , Mark Gerrit Roelofs , Randal L. Perry
IPC分类号： C08J5/20 , C08F28/02 , C08F214/18 , C08F24/00 , B05D5/12
CPC分类号： C08F214/18 , C08F24/00 , C08F28/02 , C08J5/2206 , C08J5/225 , C08J5/2293 , C08J2327/18 , H01M8/1023 , H01M8/1039 , H01M8/1072 , Y02P70/56
摘要： Crosslinkable fluoropolymers and crosslinked fluoropolymers prepared from select fluorinated monomers by dimerization and trimerization. Also disclosed are proton conductive membranes of these crosslinked fluoropolymers.
摘要翻译：可交联的含氟聚合物和由选择的氟化单体通过二聚和三聚制备的交联的含氟聚合物。还公开了这些交联的含氟聚合物的质子传导膜。

3. 发明授权

US07737190B2 Process to prepare stable trifluorostyrene containing compounds grafted to base polymers using a solvent/water mixture 失效
标题翻译：使用溶剂/水混合物制备接枝到基础聚合物上的稳定的含三氟苯乙烯的化合物的方法
公开(公告)号：US07737190B2
公开(公告)日：2010-06-15
申请号：US11388272
申请日：2006-03-24
申请人： Mark Gerrit Roelofs , Zhen-Yu Yang , Amy Qi Han, legal representative
发明人： Mark Gerrit Roelofs , Zhen-Yu Yang
IPC分类号： C08J5/20
CPC分类号： H01M8/1023 , B01D67/009 , B01D67/0093 , B01D71/32 , B01D71/78 , B01D2323/385 , C08F259/08 , C08F291/00 , C08F291/18 , C08J5/225 , C08J5/2293 , C08J7/18 , C08J2327/12 , C08J2351/06 , C08L51/003 , H01M4/8605 , H01M8/1004 , H01M8/1039 , H01M8/106 , Y02P70/56 , C08L2666/02
摘要： A fluorinated ion exchange polymer is prepared by grafting at least one grafting monomer derived from trifluorostyrene on to at least one base polymer in a organic solvent/water mixture. These ion exchange polymers are useful in preparing catalyst coated membranes and membrane electrode assemblies used in fuel cells.
摘要翻译：通过在有机溶剂/水混合物中将至少一种衍生自三氟苯乙烯的接枝单体接枝到至少一种基础聚合物上来制备氟化离子交换聚合物。这些离子交换聚合物可用于制备用于燃料电池的催化剂涂覆的膜和膜电极组件。

4. 发明申请

US20080206624A1 Trifluorostyrene Containing Compounds, and their Use in Polymer Electrolyte Membranes 失效
标题翻译：含三氟苯乙烯的化合物及其在聚合物电解质膜中的应用
公开(公告)号：US20080206624A1
公开(公告)日：2008-08-28
申请号：US10570024
申请日：2004-06-25
申请人： Biswajit Choudhury , Mark Gerrit Roelofs , Zhen-Yu Yang
发明人： Biswajit Choudhury , Mark Gerrit Roelofs , Zhen-Yu Yang
IPC分类号： H01M4/90 , C08F259/08
CPC分类号： C08F259/08 , C08F255/02 , C08F291/18 , C08F291/185
摘要： A fluorinated ion exchange polymer prepared by grafting a monomer on to a base polymer, wherein the grafting monomer is selected from the group consisting of structure 1a, structure 1b and mixtures thereof, (INSERT 1a and 1b HERE) wherein Y is selected from the group consisting of —RFSO2F (sulfonyl fluoride), —RFSO3M (fluorosulfonic acid or salt), RFSO2NH2 (fluorosulfonamide), and —RFSO2N(M)SO2R2F (imide); wherein M is H, an alkali cation, or ammonium; and RF and R2F groups are perfluorinated or partially fluorinated, and may optionally include ether oxygens; and n is between 1 and 2 for 1a, or n is between 1 and 3 for 1b. These ion exchange polymers are useful in preparing catalyst coated membranes and membrane electrode assemblies used in fuel cells.
摘要翻译：通过将单体接枝到基础聚合物上制备的氟化离子交换聚合物，其中接枝单体选自结构1a，结构1b及其混合物（INSERT 1a和1b HERE），其中Y选自基团由-SO 2 SO 2 F（磺酰氟）组成，-RF 3 SO 3 M（氟磺酸或盐），R 2 SO 2 NH 2（氟磺酰胺）和R 1 F SO 2 2 N（M）SO 2 R 2（酰亚胺）; 其中M为H，碱性阳离子或铵; 并且R 1和R 2基团是全氟化的或部分氟化的，并且可任选地包括醚氧; 对于1a，n对于1和2之间，对于1b，n对于1和3之间。这些离子交换聚合物可用于制备用于燃料电池的催化剂涂覆的膜和膜电极组件。

5. 发明授权

US07563532B2 Trifluorostyrene containing compounds, and their use in polymer electrolyte membranes 失效
标题翻译：含三氟苯乙烯的化合物，以及它们在聚合物电解质膜中的应用
公开(公告)号：US07563532B2
公开(公告)日：2009-07-21
申请号：US10570024
申请日：2004-06-25
申请人： Biswajit Choudhury , Mark Gerrit Roelofs , Zhen-Yu Yang
发明人： Biswajit Choudhury , Mark Gerrit Roelofs , Zhen-Yu Yang
IPC分类号： H01M8/10 , C08J5/22
CPC分类号： C08F259/08 , C08F255/02 , C08F291/18 , C08F291/185
摘要： A fluorinated ion exchange polymer is prepared by grafting a monomer onto a base polymer, wherein the grafting monomer is selected from the group consisting of structure 1a, 1b and mixture thereof; wherein Y is selected from the group consisting of —RFSO2F, —RFSO3M, —RSO2NH2 and —RFSO2N(M)SO2R2F, where in M is hydrogen, an alkali cation or ammonium; and RF and R2F are perfluorinated or partially fluorinated, and may optionally include ether oxygens; and n is between 1 and 2 for 1a, or n is between 1 and 3 for 1b. These ion exchange polymers are useful is preparing catalyst coated membranes and membrane electrode assemblies for fuel cells.
摘要翻译：通过将单体接枝到基础聚合物上制备氟化离子交换聚合物，其中接枝单体选自结构1a，1b及其混合物; 其中Y选自-RFSO2F，-RFSO3M，-RSO2NH2和-RFSO2N（M）SO2R2F，其中M为氢，碱性阳离子或铵; RF和R2F是全氟化或部分氟化的，并且可任选地包括醚氧; 对于1a，n对于1和2之间，对于1b，n对于1和3之间。这些离子交换聚合物可用于制备用于燃料电池的催化剂涂覆的膜和膜电极组件。

6. 发明授权

US06268430B1 Ionomers and ionically conductive compositions 有权
标题翻译：离聚物和离子导电组合物
公开(公告)号：US06268430B1
公开(公告)日：2001-07-31
申请号：US09588885
申请日：2000-06-07
申请人： Susan Kuharcik Choi , Christopher Marc Doyle , Mark Gerrit Roelofs , Lin Wang , Zhen-Yu Yang
发明人： Susan Kuharcik Choi , Christopher Marc Doyle , Mark Gerrit Roelofs , Lin Wang , Zhen-Yu Yang
IPC分类号： C08L2712
CPC分类号： H01M2/1653 , C08F8/44 , C08L101/12 , H01B1/122 , H01M4/13 , H01M4/621 , H01M8/1023 , H01M8/1039 , H01M8/1058 , H01M8/1081 , H01M10/052 , H01M10/0565 , H01M2300/0085 , Y02P70/56
摘要： Disclosed are ionomers comprising functionalized polyolefins having fluoroalkyl sulfonate pendant groups and ionically conductive compositions formed therefrom by the addition of solvents.
摘要翻译：公开了包含具有氟烷基磺酸酯侧基的官能化聚烯烃和通过加入溶剂由其形成的离子导电组合物的离聚物。

7. 发明申请

US20130245219A1 IONOMERS AND IONICALLY CONDUCTIVE COMPOSITIONS 审中-公开
标题翻译：离子和离子导电组合物
公开(公告)号：US20130245219A1
公开(公告)日：2013-09-19
申请号：US13989149
申请日：2011-12-20
申请人： Randal L. Perry , Mark Gerrit Roelofs , Robert Clayton Wheland , Ralph Munson Aten
发明人： Randal L. Perry , Mark Gerrit Roelofs , Robert Clayton Wheland , Ralph Munson Aten
IPC分类号： C08F14/18
CPC分类号： C08F14/18 , C08F214/18 , C08F214/182 , C08F216/1408 , C08F216/1466 , C08J5/2237 , C08J2327/18 , C08L23/0876 , H01G11/58 , H01M8/1004 , H01M8/1025 , H01M8/1039 , H01M8/1044
摘要： This invention relates to ionomers and to ionically conductive compositions formed therefrom. The ionomers comprise polymerized units of monomers A and monomers B, wherein monomers A are perfluoro dioxole or perfluoro dioxolane monomers, and the monomers B are functionalized perfluoro olefins having fluoroalkyl sulfonyl, fluoroalkyl sulfonate or fluoroalkyl sulfonic acid pendant groups, CF2═CF(O)[CF2]nSO2X. The ionically conductive compositions of the invention are useful in fuel cells, electrolysis cells, ion exchange membranes, sensors, electrochemical capacitors, and modified electrodes.
摘要翻译：本发明涉及离聚物和由其形成的离子导电组合物。离聚物包括单体A和单体B的聚合单元，其中单体A是全氟二氧杂环戊烯或全氟二氧戊环单体，单体B是具有氟代烷基磺酰基，氟烷基磺酸酯或氟烷基磺酸侧基的全氟烯烃官能化的CF 2 = CF（O） [CF2] nSO2X。本发明的离子导电组合物可用于燃料电池，电解槽，离子交换膜，传感器，电化学电容器和改性电极。

8. 发明授权

US07829603B2 Stable trifluorostyrene containing compounds grafted to base polymers, and their use as polymer electrolyte membranes 失效
标题翻译：稳定的含三氟苯乙烯的化合物接枝到基础聚合物上，它们用作聚合物电解质膜
公开(公告)号：US07829603B2
公开(公告)日：2010-11-09
申请号：US11547239
申请日：2004-06-25
申请人： Zhen-Yu Yang , Mark Gerrit Roelofs
发明人： Zhen-Yu Yang , Mark Gerrit Roelofs
IPC分类号： C08J5/20
CPC分类号： C08F291/18 , C08F255/02 , C08F259/08 , C08F291/185 , C08J5/225 , C08J2327/12 , C08J2351/06 , H01B1/122 , H01M8/1023 , H01M8/1039 , H01M8/1053 , H01M8/106 , H01M8/1072 , H01M2300/0082 , H01M2300/0091 , Y02P70/56 , C08F212/14
摘要： A fluorinated ion exchange polymer prepared by grafting at least one grafting monomer on to at least one base polymer, wherein the grafting monomer comprises structure 1a or 1b: wherein Z comprises S, SO2, or POR wherein R comprises a linear or branched perfluoroalkyl group of 1 to 14 carbon atoms optionally containing oxygen or chlorine, an alkyl group of 1 to 8 carbon atoms, an aryl group of 6 to 12 carbon atoms or a substituted aryl group of 6 to 12 carbon atoms; RF comprises a linear or branched perfluoroalkene group of 1 to 20 carbon atoms, optionally containing oxygen or chlorine; Q is chosen from F, —OM, NH2, —N(M)SO2R2F, and C(M)(SO2R2F)2, wherein M comprises H, an alkali cation, or ammonium; R2F groups comprises alkyl of 1 to 14 carbon atoms which may optionally include ether oxygens or aryl of 6 to 12 carbon atoms where the alkyl or aryl groups may be perfluorinated or partially fluorinated; and n is 1 or 2 for 1a, and n is 1, 2, or 3 for 1b. These ion exchange polymers are useful in preparing catalyst coated membranes and membrane electrode assemblies used in fuel cells.
摘要翻译：通过将至少一种接枝单体接枝到至少一种基础聚合物上制备的氟化离子交换聚合物，其中接枝单体包含结构1a或1b：其中Z包含S，SO 2或POR，其中R包含直链或支链全氟烷基任选含有氧或氯的1至14个碳原子，1至8个碳原子的烷基，6至12个碳原子的芳基或6至12个碳原子的取代的芳基; RF包括任选含有氧或氯的1-20个碳原子的直链或支链全氟烯基; Q选自F，-OM，NH2，-N（M）SO2R2F和C（M）（SO2R2F）2，其中M包括H，碱性阳离子或铵; R 2 F基团包括1至14个碳原子的烷基，其可任选地包括醚氧基或6至12个碳原子的芳基，其中烷基或芳基可全氟化或部分氟化; 对于1a，n为1或2，对于1b，n为1,2或3。这些离子交换聚合物可用于制备用于燃料电池的催化剂涂覆的膜和膜电极组件。

9. 发明授权

US6100324A Ionomers and ionically conductive compositions 失效
标题翻译：离聚物和离子导电组合物
公开(公告)号：US6100324A
公开(公告)日：2000-08-08
申请号：US61132
申请日：1998-04-16
申请人： Susan Kuharcik Choi , Christopher Marc Doyle , Mark Gerrit Roelofs , Lin Wang , Zhen-Yu Yang
发明人： Susan Kuharcik Choi , Christopher Marc Doyle , Mark Gerrit Roelofs , Lin Wang , Zhen-Yu Yang
IPC分类号： C08J5/22 , C08F8/12 , C08F8/44 , C08L101/12 , H01B1/06 , H01B1/12 , H01M2/16 , H01M4/13 , H01M4/62 , H01M8/10 , H01M10/052 , H01M10/0565 , H01M10/36 , C08F255/00
CPC分类号： H01M2/1653 , C08F8/44 , C08L101/12 , H01B1/122 , H01M10/052 , H01M10/0565 , H01M4/13 , H01M8/1023 , H01M8/1039 , H01M8/1081 , H01M2300/0085 , H01M4/621 , H01M8/1058 , Y02P70/56
摘要： Disclosed are ionomers comprising functionalized polyolefins having fluoroalkyl sulfonate pendant groups and ionically conductive compositions formed therefrom by the addition of solvents.
摘要翻译：公开了包含具有氟烷基磺酸酯侧基的官能化聚烯烃和通过加入溶剂由其形成的离子导电组合物的离聚物。

10. 发明授权

US09431661B2 Cathode catalyst layer, membrane electrode assembly and polymer electrolyte fuel cell and manufacturing method thereof 有权
标题翻译：阴极催化剂层，膜电极组件和聚合物电解质燃料电池及其制造方法
公开(公告)号：US09431661B2
公开(公告)日：2016-08-30
申请号：US13995635
申请日：2011-12-20
申请人： Nobuaki Nonoyama , Masanori Aimu , Randal Lewis Perry , Mark Gerrit Roelofs , Robert Clayton Wheland , Ralph Munson Aten
发明人： Nobuaki Nonoyama , Masanori Aimu , Randal Lewis Perry , Mark Gerrit Roelofs , Robert Clayton Wheland , Ralph Munson Aten
IPC分类号： H01M4/86 , H01M4/88 , H01M8/10
CPC分类号： H01M4/8657 , H01M4/8652 , H01M4/8663 , H01M4/8668 , H01M4/886 , H01M8/1004 , H01M2008/1095 , Y02E60/521 , Y02P70/56
摘要： A cathode catalyst layer used for a polymer electrolyte fuel cell that includes an electrolyte membrane is provided. The cathode catalyst layer comprises a catalyst having weight of not greater than 0.3 mg/cm2 of a reaction surface of the cathode catalyst layer that is adjoining the electrolyte membrane; and an electrolyte resin having oxygen permeability of not less than 2.2*10−14 mol/m/s/Pa in an environment of temperature of 80 degrees Celsius and relative humidity of 50%.
摘要翻译：提供了用于包含电解质膜的固体高分子型燃料电池的阴极催化剂层。阴极催化剂层包含负极与电解质膜相邻的阴极催化剂层的反应面重量不大于0.3mg / cm 2的催化剂; 以及在80℃的温度和50％的相对湿度的环境中具有不低于2.2×10-14mol / m / s / Pa的透氧度的电解质树脂。

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