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1. 发明申请

US20050049373A1 Higher alpha-olefin copolymers and process for preparation thereof 失效
标题翻译：高级α-烯烃共聚物及其制备方法
公开(公告)号：US20050049373A1
公开(公告)日：2005-03-03
申请号：US10925037
申请日：2004-08-25
申请人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
发明人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
IPC分类号： C08F4/645 , C08F4/659 , C08F4/6592 , C08F210/14 , C08F4/44
CPC分类号： C08F210/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F2500/20 , C08F2500/03
摘要： An object of the present invention is to provide crystalline high α-olefin copolymers which have excellent compatibility with thermoplastic resins, especially polyolefins, and compatibility with lubricant oils, fuel oils or waxes, excellent miscibility with inorganic fillers and secondary processability, and which have narrow temperature ranges for melting and crystallization, and to provide a process for preparation thereof. The present invention provides a crystalline higher α-olefin copolymer obtained by copolymerizing at least two higher α-olefins having 10 or more carbon atoms or at least one higher α-olefin having 10 or more carbon atoms with at least one other olefin, wherein it satisfies the following (1) to (3): (1): the content of higher α-olefin units is 50 mol % or greater, (2): the melting point (Tm) which is measured, by using a differential scanning calorimeter (DSC), from the melting endothermic curve obtained by maintaining the copolymer at 190° C. for 5 minutes under a nitrogen atmosphere, cooling it to −10° C. at a rate of 5° C./min, maintaining it at −10° C. for 5 minutes, and then elevating its temperature to 190° C. at 10° C./min is in the range of 20 to 100° C., and (3): in the intensity distribution of wide-angle X-ray scattering, a single peak X1 resulting from crystallization of side chains is observed at 15 deg
摘要翻译：本发明的目的是提供与热塑性树脂特别是聚烯烃具有优异相容性的结晶高α-烯烃共聚物，与润滑油，燃料油或蜡的相容性，与无机填料的混溶性和二次加工性，并且具有窄熔化和结晶的温度范围，并提供其制备方法。本发明提供通过使至少两种具有10个或更多个碳原子的高级α-烯烃或至少一个具有10个或更多个碳原子的高级α-烯烃与至少一种其它烯烃共聚得到的结晶高级α-烯烃共聚物，其中满足以下（1）〜（3）：（1）：高级α-烯烃单元的含量为50摩尔％以上，（2）：使用差示扫描量热计测定的熔点（Tm）（DSC）中，从在氮气气氛下将共聚物在190℃下保持5分钟而获得的熔融吸热曲线，以5℃/ min的速度将其冷却至-10℃， 10℃下5分钟，然后在10℃/分钟将其温度升至190℃/分钟在20至100℃的范围内，和（3）：在广角度的强度分布在15度<2度<30度观察到X射线散射，由侧链结晶产生的单峰X1。

2. 发明申请

US20060111526A1 Higher alpha-olefin copolymers and process for preparation thereof 有权
标题翻译：高级α-烯烃共聚物及其制备方法
公开(公告)号：US20060111526A1
公开(公告)日：2006-05-25
申请号：US11324304
申请日：2006-01-04
申请人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
发明人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
IPC分类号： C08F4/44
CPC分类号： C08F210/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F2500/20 , C08F2500/03
摘要： An object of the present invention is to provide crystalline high α-olefin copolymers which have excellent compatibility with thermoplastic resins, especially polyolefins, and compatibility with lubricant oils, fuel oils or waxes, excellent miscibility with inorganic fillers and secondary processability, and which have narrow temperature ranges for melting and crystallization, and to provide a process for preparation thereof. The present invention provides a crystalline higher α-olefin copolymer obtained by copolymerizing at least two higher α-olefins having 10 or more carbon atoms or at least one higher α-olefin having 10 or more carbon atoms with at least one other olefin, wherein it satisfies the following (1) to (3): (1): the content of higher α-olefin units is 50 mol % or greater, (2): the melting point (Tm) which is measured, by using a differential scanning calorimeter (DSC), from the melting endothermic curve obtained by maintaining the copolymer at 190° C. for 5 minutes under a nitrogen atmosphere, cooling it to −10° C. at a rate of 5° C./min, maintaining it at −10° C. for 5 minutes, and then elevating its temperature to 190° C. at 10° C./min is in the range of 20 to 100° C., and (3): in the intensity distribution of wide-angle X-ray scattering, a single peak X1 resulting from crystallization of side chains is observed at 15 deg
摘要翻译：本发明的目的是提供与热塑性树脂特别是聚烯烃具有优异相容性的结晶高α-烯烃共聚物，与润滑油，燃料油或蜡的相容性，与无机填料的混溶性和二次加工性，并且具有窄熔化和结晶的温度范围，并提供其制备方法。本发明提供通过使至少两种具有10个或更多个碳原子的高级α-烯烃或至少一个具有10个或更多个碳原子的高级α-烯烃与至少一种其它烯烃共聚得到的结晶高级α-烯烃共聚物，其中满足以下（1）〜（3）：（1）：高级α-烯烃单元的含量为50摩尔％以上，（2）：使用差示扫描量热计测定的熔点（Tm）（DSC）中，从在氮气气氛下将共聚物在190℃下保持5分钟而获得的熔融吸热曲线，以5℃/ min的速度将其冷却至-10℃， 10℃下5分钟，然后在10℃/分钟将其温度升至190℃/分钟在20至100℃的范围内，和（3）：在广角度的强度分布在15度<2度<30度观察到X射线散射，由侧链结晶产生的单峰X1。

3. 发明授权

US07109283B2 Higher α-olefin copolymers and process for preparation thereof 有权
标题翻译：高级α-烯烃共聚物及其制备方法
公开(公告)号：US07109283B2
公开(公告)日：2006-09-19
申请号：US11324304
申请日：2006-01-04
申请人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
发明人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
IPC分类号： C08F10/14
CPC分类号： C08F210/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F2500/20 , C08F2500/03
摘要： The present invention provides a crystalline higher α-olefin copolymer obtained by copolymerizing at least two higher α-olefins having 10 or more carbon atoms or at least one higher α-olefin having 10 or more carbon atoms with at least one other olefin, wherein it satisfies certain conditions.
摘要翻译：本发明提供通过使至少两种具有10个或更多个碳原子的高级α-烯烃或至少一个具有10个或更多个碳原子的高级α-烯烃与至少一种其它烯烃共聚得到的结晶高级α-烯烃共聚物，其中满足一定条件。

4. 发明授权

US07019091B2 Higher α-olefin copolymers and process for preparation thereof 失效
公开(公告)号：US07019091B2
公开(公告)日：2006-03-28
申请号：US10925037
申请日：2004-08-25
申请人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
发明人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
IPC分类号： C08F4/642 , C08F210/14
CPC分类号： C08F210/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F2500/20 , C08F2500/03
摘要： The present invention provides a crystalline higher α-olefin copolymer obtained by copolymerizing at least two higher α-olefins having 10 or more carbon atoms or at least one higher α-olefin having 10 or more carbon atoms with at least one other olefin, wherein it satisfies certain conditions.

5. 发明申请

US20050119374A1 Crystalline polymer of higher alpha-olefin and process for producing the same 有权
标题翻译：高级α-烯烃的结晶聚合物及其制备方法
公开(公告)号：US20050119374A1
公开(公告)日：2005-06-02
申请号：US10505046
申请日：2003-02-19
申请人： Yutaka Minami , Masami Kanamaru , Masanori Sera , Tatsuya Egawa , Takenori Fujimura
发明人： Yutaka Minami , Masami Kanamaru , Masanori Sera , Tatsuya Egawa , Takenori Fujimura
IPC分类号： C08F4/642 , C08F10/00 , C08F110/14 , C08L67/00
CPC分类号： C08F110/14 , C08F10/00 , C08F4/65927 , C08F2500/17 , C08F2500/03 , C08F2500/20 , C08F2500/18 , C08F2500/15
摘要： A crystalline higher (x-olefin polymer which is obtained from a C10 or more α-olefin and satisfies either (1) the melting point (Tm) as measured with a differential scanning calorimeter (DSC) is 20 to 100° C. or (2) in an examination of spin-lattice relaxation time (T1) by solid NMR analysis, a single T1 is observed at the temperatures not lower than the melting point; and a process for producing the α-olefin polymer with a specific metallocene catalyst. The crystalline higher α-olefin polymer is excellent in low-temperature characteristics, rigidity, heat resistance, compatibility with lubricating oils, mixability with inorganic fillers, and secondary processability.
摘要翻译：由差示扫描量热仪（DSC）测得的结晶高（X-α-烯烃聚合物，由C 10以上的α-烯烃得到并满足（1）熔点（Tm） 20至100℃或（2）通过固体NMR分析检查自旋晶格弛豫时间（T 1 N 2）时，在不低于熔点的温度;以及用特定的茂金属催化剂生产α-烯烃聚合物的方法，结晶高级α-烯烃聚合物的低温特性，刚性，耐热性，与润滑油的相容性，混合性无机填料，二次加工性能。

6. 发明授权

US07214755B2 Crystalline polymer of higher α-olefin and process for producing the same 有权
标题翻译：高级α-烯烃的结晶聚合物及其制备方法
公开(公告)号：US07214755B2
公开(公告)日：2007-05-08
申请号：US10505046
申请日：2003-02-19
申请人： Yutaka Minami , Masami Kanamaru , Masanori Sera , Tatsuya Egawa , Takenori Fujimura
发明人： Yutaka Minami , Masami Kanamaru , Masanori Sera , Tatsuya Egawa , Takenori Fujimura
IPC分类号： C08F110/14 , C08F210/14 , C08F4/6192
CPC分类号： C08F110/14 , C08F10/00 , C08F4/65927 , C08F2500/17 , C08F2500/03 , C08F2500/20 , C08F2500/18 , C08F2500/15
摘要： A crystalline higher α-olefin polymer which is obtained from a C10 or more α-olefin and satisfies either (1) the melting point (Tm) as measured with a differential scanning calorimeter (DSC) is 20 to 100° C. or (2) in an examination of spin-lattice relaxation time (T1) by solid NMR analysis, a single T1 is observed at the temperatures not lower than the melting point; and a process for producing the α-olefin polymer with a specific metallocene catalyst. The crystalline higher α-olefin polymer is excellent in low-temperature characteristics, rigidity, heat resistance, compatibility with lubricating oils, mixability with inorganic fillers, and secondary processability.
摘要翻译：由差示扫描量热仪（DSC）测得的，由C 10〜10以上的α-烯烃得到的满足（1）熔点（Tm）的结晶高级α-烯烃聚合物为20 至（100）℃，或（2）在通过固体NMR分析检查自旋晶格弛豫时间（T 1 N 2）时，在温度下观察到单个T 1 不低于熔点; 以及用特定的茂金属催化剂生产α-烯烃聚合物的方法。结晶高级α-烯烃聚合物的低温特性，刚性，耐热性，与润滑油的相容性，与无机填料的混合性以及二次加工性优异。

7. 发明授权

US07714081B2 Heat-storage material composition 失效
标题翻译：储热材料组成
公开(公告)号：US07714081B2
公开(公告)日：2010-05-11
申请号：US10577496
申请日：2004-10-27
申请人： Masanori Sera , Yutaka Minami , Takenori Fujimura
发明人： Masanori Sera , Yutaka Minami , Takenori Fujimura
IPC分类号： C08L23/00 , C08L23/02
CPC分类号： C09K5/063
摘要： The present invention relates to a heat storage material composition comprising 20 to 100% by weight of a heat storage material, 80 to 0% by weight of crystalline polyolefin (B) and 50 to 0% by weight of an elastomer (C), and the heat storage material described above contains a side chain-crystalline polymer (A), wherein the heat storage material described above comprises preferably a higher α-olefin polymer (a) containing 50 mole % or more of higher α-olefin having 10 or more carbon atoms and a petroleum wax (b) in which a melting point (Tm) is higher by 10° C. or more than that of the polymer (a). Provided is a heat storage material composition which has less bleeding and stickiness and is excellent in stability at high temperature and which can meet a change in temperature such as a difference in room temperature when applied to a material for floor heating and can avoid a heating state deviated to high temperature or low temperature.
摘要翻译：本发明涉及一种储热材料组合物，其包含20至100重量％的蓄热材料，80至0重量％的结晶聚烯烃（B）和50至0重量％的弹性体（C），以及上述储热材料含有侧链状聚合物（A），其中上述储热材料优选包含含有50摩尔％以上的具有10个以上的高级α-烯烃的高级α-烯烃聚合物（a）碳原子和熔点（Tm）高于聚合物（a）的10℃以上的石油蜡（b）。本发明提供一种蓄热材料组合物，其具有较少的渗透性和粘性，并且在高温下的稳定性优异，并且当施加到用于地板加热的材料时可以满足诸如室温差的温度变化并且可以避免加热状态偏向高温或低温。

8. 发明申请

US20090018288A1 CROSSLINKED OLEFIN POLYMERS AND PROCESS FOR PRODUCTION THEREOF 审中-公开
标题翻译：交联烯烃聚合物及其生产方法
公开(公告)号：US20090018288A1
公开(公告)日：2009-01-15
申请号：US11718834
申请日：2005-11-07
申请人： Ryo Aburatani , Yutaka Obata , Tomoaki Takebe , Masanori Sera , Yutaka Minami
发明人： Ryo Aburatani , Yutaka Obata , Tomoaki Takebe , Masanori Sera , Yutaka Minami
IPC分类号： C08F10/14 , C08F8/00
CPC分类号： C08F10/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F8/00 , C08F110/14 , C08F210/14 , C08F2500/20 , C08F2500/04 , C08F2500/03
摘要： Crosslinked olefin polymers which are reduced in stickiness and improved in rigidity, heat resistance, light resistance, and water resistance while retaining the molding properties such as injection moldability, spinnability, film-forming properties and the physical properties such as toughness (including elongation and break strength) and tackiness; and a process for the production thereof. Crosslinked olefin polymers which are obtained by reacting an α-olefin polymer produced by polymerization of at least one α-olefin having 6 or more carbon atoms or polymerization of at least one α-olefin having 6 or more carbon atoms with at least one other α-olefin with a crosslinking agent and which satisfy the following requirements: (1) the content of units of α-olefins having 6 or more carbon atoms is 50 mol % or more, (2) the molecular weight distribution (Mw/Mn) as determined by gel permeation chromatography (GPC) is 7.0 or more in terms of polystyrene, (3) the content of components having weight-average molecular weights (Mw) of 106 or more is 5% by mass or more as determined by GPC, and (4) the stereoregularity indication M4 is 75 mol % or less; and a process for the production of the polymers.
摘要翻译：在保持成型性，如注塑成型性，纺丝性，成膜性以及韧性（包括伸长率和断裂性等）的物理性能的同时，粘合性降低，刚性，耐热性，耐光性和耐水性降低的交联烯烃聚合物强度）和粘性; 及其生产方法。通过使至少一种具有6个或更多个碳原子的至少一种α-烯烃聚合而产生的α-烯烃聚合物或至少一种具有6个或更多个碳原子的至少一个碳原子的α-烯烃与至少一种其它的α-烯烃反应而获得的交联烯烃聚合物（1）具有6个或更多个碳原子的α-烯烃的单元含量为50摩尔％以上，（2）分子量分布（Mw / Mn）为通过凝胶渗透色谱法（GPC）测定的聚苯乙烯换算为7.0以上，（3）通过GPC测定，重均分子量（Mw）为106以上的成分的含量为5质量％以上，（4）立构规整性指示M4为75摩尔％以下; 以及聚合物的制造方法。

9. 发明申请

US20070079825A1 Heat-storage material composition 失效
标题翻译：储热材料组成
公开(公告)号：US20070079825A1
公开(公告)日：2007-04-12
申请号：US10577496
申请日：2004-10-27
申请人： Masanori Sera , Yutaka Minami , Takenori Fujimura
发明人： Masanori Sera , Yutaka Minami , Takenori Fujimura
IPC分类号： F24J2/34
CPC分类号： C09K5/063
摘要： The present invention relates to a heat storage material composition comprising 20 to 100% by weight of a heat storage material, 80 to 0% by weight of crystalline polyolefin (B) and 50 to 0% by weight of an elastomer (C), and the heat storage material described above contains a side chain-crystalline polymer (A), wherein the heat storage material described above comprises preferably a higher α-olefin polymer (a) containing 50 mole % or more of higher α-olefin having 10 or more carbon atoms and a petroleum wax (b) in which a melting point (Tm) is higher by 10° C. or more than that of the polymer (a). Provided is a heat storage material composition which has less bleeding and stickiness and is excellent in stability at high temperature and which can meet a change in temperature such as a difference in room temperature when applied to a material for floor heating and can avoid a heating state deviated to high temperature or low temperature.
摘要翻译：本发明涉及一种储热材料组合物，其包含20至100重量％的蓄热材料，80至0重量％的结晶聚烯烃（B）和50至0重量％的弹性体（C），以及上述储热材料含有侧链结晶聚合物（A），其中上述储热材料优选包含含有50摩尔％以上的具有10个或更多个的高级α-烯烃的高级α-烯烃聚合物（a）碳原子和熔点（Tm）高于聚合物（a）的10℃以上的石油蜡（b）。本发明提供一种蓄热材料组合物，其具有较少的渗透性和粘性，并且在高温下的稳定性优异，并且当施加到用于地板加热的材料时可以满足诸如室温差的温度变化并且可以避免加热状态偏向高温或低温。

10. 发明授权

US07981959B2 Resin composition, process for producing the same and molding of the resin composition 失效
标题翻译：树脂组合物，其制造方法和树脂组合物的成型
公开(公告)号：US07981959B2
公开(公告)日：2011-07-19
申请号：US11908292
申请日：2006-03-13
申请人： Akio Nodera , Yusuke Hayata , Masanori Sera , Takenori Fujimura
发明人： Akio Nodera , Yusuke Hayata , Masanori Sera , Takenori Fujimura
IPC分类号： C08K3/04 , C08J3/20
CPC分类号： C08J5/005 , B82Y30/00 , C08L23/24 , C08L69/00 , H01B1/24 , Y10S977/742 , C08L2666/06 , C08L2666/02
摘要： The present invention provides a resin composition including 100 parts by mass of a resin component containing 80 to 99 mass % of a thermoplastic resin (A) and 20 to 1 mass % of a side-chain crystalline polymer (B), and 0.1 to 30 parts by mass of carbon nanotube (C). The composition has a stabilized thermoplastic resin/side-chain crystalline polymer phase structure, is free from laminar peeling, and is excellent in conductive (antistatic) property, solvent resistance, flow characteristics, flame retardancy, impact resistance, molding appearance, etc.
摘要翻译：本发明提供一种树脂组合物，其包含100质量份含有热塑性树脂（A）80〜99质量％和侧链结晶性聚合物（B）20〜1质量％的树脂成分，0.1〜30质量％质量份的碳纳米管（C）。该组合物具有稳定的热塑性树脂/侧链结晶聚合物相结构，没有层状剥离，并且具有优异的导电性（抗静电）性，耐溶剂性，流动特性，阻燃性，耐冲击性，成型外观等。

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