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1. 发明授权

US07468167B2 Method for starting up reactor and reactor system 有权
标题翻译：启动反应堆和反应堆系统的方法
公开(公告)号：US07468167B2
公开(公告)日：2008-12-23
申请号：US11221213
申请日：2005-09-07
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： F28D7/00 , F28D21/00 , F28D15/00 , C07C53/00
CPC分类号： F28D7/0066 , B01J8/067 , B01J2208/00212 , B01J2208/00256 , B01J2208/00716 , B01J2219/00006 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for quickly starting up a reactor and a reactor system therefor are provided. A shell-and-tube reactor in the system is adapted to circulate a heat medium having a solid point in the range of 50-250° C. to the outside of the reaction tubes and characterized by initiating temperature elevation of the reactor by introducing a gas of a temperature in the range of 100-400° C. to the reaction tubes' side and then circulating the heat medium in a heated state to the outside of the reaction tubes. By introducing a gas of an elevated temperature preparatorily to the reaction tubes, it is made possible to prevent the heat medium after circulation from being solidified again and enable the reactor to be quickly started up.
摘要翻译：提供了一种用于快速启动反应器及其反应器系统的方法。系统中的管壳式反应器适于将具有在50-250℃范围内的固点的热介质循环到反应管的外部，并且其特征在于通过引入反应器的温度升高将温度在100-400℃范围内的气体加到反应管侧，然后将加热的热介质循环到反应管的外部。通过将升温的气体预先引入反应管，可以防止循环后的热介质再次固化，使反应器快速启动。

2. 发明授权

US06946573B2 Method for starting up reactor and reactor system 有权
标题翻译：启动反应堆和反应堆系统的方法
公开(公告)号：US06946573B2
公开(公告)日：2005-09-20
申请号：US09845694
申请日：2001-04-30
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： B01J19/00 , B01J12/00 , B01J19/24 , C07C45/35 , C07C47/22 , C07C51/235 , C07C51/25 , C07C57/05 , C07C57/055 , F28D7/00 , C07C57/02
CPC分类号： F28D7/0066 , B01J8/067 , B01J2208/00212 , B01J2208/00256 , B01J2208/00716 , B01J2219/00006 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for quickly starting up a reactor and a reactor system therefor are provided. A shell-and-tube reactor in the system is adapted to circulate a heat medium having a solid point in the range of 50-250° C. to the outside of the reaction tubes and characterized by initiating temperature elevation of the reactor by introducing a gas of a temperature in the range of 100-400° C. to the reaction tubes' side and then circulating the heat medium in a heated state to the outside of the reaction tubes. By introducing a gas of an elevated temperature preparatorily to the reaction tubes, it is made possible to prevent the heat medium after circulation from being solidified again and enable the reactor to be quickly started up.
摘要翻译：提供了一种用于快速启动反应器及其反应器系统的方法。系统中的管壳式反应器适于将具有在50-250℃范围内的固点的热介质循环到反应管的外部，并且其特征在于通过引入反应器的温度升高将温度在100-400℃范围内的气体加到反应管侧，然后将加热的热介质循环到反应管的外部。通过将升温的气体预先引入反应管，可以防止循环后的热介质再次固化，使反应器快速启动。

3. 发明申请

US20060009655A1 Method for starting up reactor and reactor system 有权
标题翻译：启动反应堆和反应堆系统的方法
公开(公告)号：US20060009655A1
公开(公告)日：2006-01-12
申请号：US11221213
申请日：2005-09-07
申请人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
发明人： Yukihiro Matsumoto , Takeshi Nishimura , Hideki Sogabe , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： C07C51/16 , B01J10/00
CPC分类号： F28D7/0066 , B01J8/067 , B01J2208/00212 , B01J2208/00256 , B01J2208/00716 , B01J2219/00006 , C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： A method for quickly starting up a reactor and a reactor system therefor are provided. A shell-and-tube reactor in the system is adapted to circulate a heat medium having a solid point in the range of 50-250° C. to the outside of the reaction tubes and characterized by initiating temperature elevation of the reactor by introducing a gas of a temperature in the range of 100-400° C. to the reaction tubes' side and then circulating the heat medium in a heated state to the outside of the reaction tubes. By introducing a gas of an elevated temperature preparatorily to the reaction tubes, it is made possible to prevent the heat medium after circulation from being solidified again and enable the reactor to be quickly started up.
摘要翻译：提供了一种用于快速启动反应器及其反应器系统的方法。系统中的管壳式反应器适于将具有在50-250℃范围内的固点的热介质循环到反应管的外部，并且其特征在于通过引入反应器的温度升高将温度在100-400℃范围内的气体加到反应管侧，然后将加热的热介质循环到反应管的外部。通过将升温的气体预先引入反应管，可以防止循环后的热介质再次固化，使反应器快速启动。

4. 发明授权

US06848501B2 Method for preventing plate type heat exchanger from blockage 失效
标题翻译：防止板式换热器堵塞的方法
公开(公告)号：US06848501B2
公开(公告)日：2005-02-01
申请号：US10356428
申请日：2003-01-31
申请人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
发明人： Harunori Hirao , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo , Tetsuji Mitsumoto , Takeshi Nishimura , Kazuhiko Sakamoto , Hiroo Iwato
IPC分类号： B01J19/00 , F28D7/16 , F28D9/00 , F28F19/00 , F28F27/02
CPC分类号： F28D9/0068 , B01J19/002 , B01J2219/00252 , F28D7/1607 , F28D7/1623 , F28D9/0062 , F28F9/0278 , F28F19/00 , F28F2250/102
摘要： In an apparatus provided with a plate type heat exchanger as a heater and/or a cooler and operated to treat a gas containing an easily blocking substance, a method for preventing the plate type heat exchanger from being blocked is disclosed which is characterized by i) setting the width of a flow path on a plate of the plate type heat exchanger in the apparatus in a range of 6-25 mm and ii) setting the average flow rate of the gas passing the plate type heat exchanger in the apparatus per unit cross-sectional area of the flow path on the plate in the range of 3-15 m/s. In the exchange of heat of an easily blocking substance by the use of a plate type heat exchanger, a method for preventing the plate type heat exchanger from blockage is disclosed which has the plate type heat exchanger provided in the port for introducing a gas containing an easily blocking substance with a gas dispersion plate. This invention, in the heat exchange of an effluent gas emanating from a process for the production of (meth)acrylic acid or an ester thereof or the disposal of the gas, significantly allays blockage of the interior of the plate type heat exchanger.
摘要翻译：在设置有作为加热器和/或冷却器的板式热交换器并且被操作以处理含有易阻塞物质的气体的装置中，公开了一种防止板式热交换器被堵塞的方法，其特征在于i）将设备中板式热交换器的板上的流路宽度设置在6-25mm的范围内，以及ii）将通过板式热交换器的气体的平均流量设置在每单位十字的装置中板上流路的截面面积在3-15 m / s的范围内。在通过使用板式热交换器交换容易堵塞物质的热的情况下，公开了一种防止板式热交换器堵塞的方法，其具有设置在用于引入含有用气体分散板容易地堵塞物质。本发明在从（甲基）丙烯酸或其酯的制备方法产生的流出气体的热交换或气体的处理中显着地阻止了板式热交换器的内部堵塞。

5. 发明授权

US07541490B2 Method for production of acrylic acid and apparatus for production of acrylic acid 有权
标题翻译：制备丙烯酸的方法和生产丙烯酸的设备
公开(公告)号：US07541490B2
公开(公告)日：2009-06-02
申请号：US11601417
申请日：2006-11-17
申请人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
发明人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： C07C51/16 , C07C51/235
CPC分类号： C07C51/215 , B01J19/0013 , B01J2219/00087 , B01J2219/00103 , B01J2219/00108 , B01J2219/0011 , B01J2219/00126 , B01J2219/00128 , C07C51/252 , C07C57/04
摘要： Chilled coolant is prepared by liquid coolant utilizing the latent heat generated by a gasification of liquefied propylene, for example, and this chilled coolant is used in heat exchangers which are used in a process for production of acrylic acid or acrolein. This method allows effective utilization of the latent heat which used to be discarded and permits a reduction of energy consumption of cooling required separately in the step for production. By recovering the chilled coolant with the liquid coolant, it makes possible to stabilize the gasification of propylene, etc. and consequently stabilize the production of acrylic acid. This invention consists of providing the method for the production of acrylic acid, etc. and the apparatus which make effective use of the latent heat generated in the steps of production.
摘要翻译：例如，通过液化丙烯气化产生的潜热的液体冷却剂制备冷冻冷却剂，并且该冷却的冷却剂用于用于生产丙烯酸或丙烯醛的方法中的热交换器。该方法允许有效利用以前被废弃的潜热，并且可以在生产步骤中单独地降低需要的冷却能量消耗。通过用液体冷却剂回收冷却的冷却剂，可以稳定丙烯等的气化，从而稳定丙烯酸的生产。本发明提供了生产丙烯酸等的方法和有效利用在生产步骤中产生的潜热的装置。

6. 发明申请

US20070066845A1 Method for production of acrylic acid and apparatus for production of acrylic acid 有权
公开(公告)号：US20070066845A1
公开(公告)日：2007-03-22
申请号：US11601417
申请日：2006-11-17
申请人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
发明人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： C07C51/16
CPC分类号： C07C51/215 , B01J19/0013 , B01J2219/00087 , B01J2219/00103 , B01J2219/00108 , B01J2219/0011 , B01J2219/00126 , B01J2219/00128 , C07C51/252 , C07C57/04
摘要： Chilled coolant is prepared by liquid coolant utilizing the latent heat generated by a gasification of liquefied propylene, for example, and this chilled coolant is used in heat exchangers which are used in a process for production of acrylic acid or acrolein. This method allows effective utilization of the latent heat which used to be discarded and permits a reduction of energy consumption of cooling required separately in the step for production. By recovering the chilled coolant with the liquid coolant, it makes possible to stabilize the gasification of propylene, etc. and consequently stabilize the production of acrylic acid. This invention consists of providing the method for the production of acrylic acid, etc. and the apparatus which make effective use of the latent heat generated in the steps of production.

7. 发明授权

US07198766B1 Method for production of acrylic acid and apparatus for production of acrylic acid 有权
标题翻译：制备丙烯酸的方法和生产丙烯酸的设备
公开(公告)号：US07198766B1
公开(公告)日：2007-04-03
申请号：US09705661
申请日：2000-11-03
申请人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
发明人： Kazuto Okazaki , Yukihiro Matsumoto , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： F25B39/02 , F25B39/00 , F25D17/00 , F25D17/02 , B01J7/00
CPC分类号： C07C51/215 , B01J19/0013 , B01J2219/00087 , B01J2219/00103 , B01J2219/00108 , B01J2219/0011 , B01J2219/00126 , B01J2219/00128 , C07C51/252 , C07C57/04
摘要： Chilled coolant is prepared by liquid coolant utilizing the latent heat generated by a gasification of liquefied propylene, for example, and this chilled coolant is used in heat exchangers which are used in a process for production of acrylic acid or acrolein. This method allows effective utilization of the latent heat which used to be discarded and permits a reduction of energy consumption of cooling required separately in the step for production. By recovering the chilled coolant with the liquid coolant, it makes possible to stabilize the gasification of propylene, etc. and consequently stabilize the production of acrylic acid. This invention consists of providing the method for the production of acrylic acid, etc. and the apparatus which make effective use of the latent heat generated in the steps of production.
摘要翻译：例如，通过液化丙烯气化产生的潜热的液体冷却剂制备冷冻冷却剂，并且该冷却的冷却剂用于用于生产丙烯酸或丙烯醛的方法中的热交换器。该方法允许有效利用以前被废弃的潜热，并且可以在生产步骤中单独地降低需要的冷却能量消耗。通过用液体冷却剂回收冷却的冷却剂，可以稳定丙烯等的气化，从而稳定丙烯酸的生产。本发明提供了生产丙烯酸等的方法和有效利用在生产步骤中产生的潜热的装置。

8. 发明授权

US06431261B1 Shell and tube type heat exchanger 有权
公开(公告)号：US06431261B1
公开(公告)日：2002-08-13
申请号：US09733679
申请日：2000-12-08
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Daisuke Nakamura , Masakatsu Mori , Osamu Dodo
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Daisuke Nakamura , Masakatsu Mori , Osamu Dodo
IPC分类号： F28D700
摘要： The temperature distribution in a shell and tube type heat exchanger having an expansion joint is uniformized by improving the circulation efficiency of fluid in the shell side. The uniformization is attained by the heat exchanger having an invasion-preventing plate against the fluid in the shell side attached to the expansion joint installed around the periphery of the shell, and a method of catalytic gas phase oxidation reaction that uses the heat exchanger.

9. 发明授权

US06891061B1 Packed column and polymerizable compound treating method using the same 有权
标题翻译：填充柱和使用其的可聚合化合物处理方法
公开(公告)号：US06891061B1
公开(公告)日：2005-05-10
申请号：US09688169
申请日：2000-10-16
申请人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
发明人： Takeshi Nishimura , Yukihiro Matsumoto , Sei Nakahara , Osamu Dodo
IPC分类号： B01D3/16 , B01D3/14 , B01D3/32 , B01J10/00 , B01J19/30 , B01J19/32 , C07C51/44 , C07C57/07 , C07C67/54 , C07C69/54 , C07C67/48 , C07C51/42
CPC分类号： B01J19/305 , B01D3/324 , B01D3/326 , B01J19/325 , B01J2219/185 , B01J2219/3221 , B01J2219/32213 , B01J2219/32272 , B01J2219/32275 , B01J2219/3325
摘要： Provided are a packed column arranged so as to be capable of effectively preventing polymerization of a polymerizable compound such as a (meth)acrylic acid in treating the compound, and a method for treating a polymerizable compound using the packed column. The packed column, which is provided with a packing support plate and is filled with a packing on the packing support plate, is arranged so as to include a packing layer (B) having a greater percentage of voids than that of a packing layer (A), between the packing support plate and the packing layer (A).
摘要翻译：提供了一种填充柱，其布置成能够有效地防止在处理该化合物时诸如（甲基）丙烯酸之类的可聚合化合物的聚合，以及使用填充柱处理可聚合化合物的方法。填充柱设置有填充支撑板并且填充在填料支撑板上的填料，以包括具有比填充层（A（A））更大百分比的空隙的填充层（B）），在包装支撑板和包装层（A）之间。

10. 发明授权

US07377307B1 Vertical heat exchanger 失效
标题翻译：立式换热器
公开(公告)号：US07377307B1
公开(公告)日：2008-05-27
申请号：US09705351
申请日：2000-11-03
申请人： Yuichi Ijiri , Takeshi Nishimura , Kazuhiko Sakamoto , Osamu Dodo
发明人： Yuichi Ijiri , Takeshi Nishimura , Kazuhiko Sakamoto , Osamu Dodo
IPC分类号： F28F27/00
CPC分类号： F28D7/16 , F28F9/02 , F28F2265/06
摘要： A vertical heat exchanger is described, which allows efficient elimination of the gas generated therein and efficient removal of the sludge accumulated therein. The vertical heat exchanger has at least part of one end of a vent pipe formed of an upper tube sheet part (an upper cover part in the case of a spiral heat exchanger) and the other end thereof connected outside the heat exchanger to an immediately adjacent fluid passing port passing the same fluid as the vent and/or at least part of one end of a drain pipe formed of a lower tube sheet part (a lower cover part in the case of a spiral heat exchanger) and the other end thereof connected outside the heat exchanger to an immediately adjacent fluid passing port passing the same fluid as the drain.
摘要翻译：描述了一种立式热交换器，其允许有效地消除其中产生的气体并有效地去除积聚在其中的污泥。立式热交换器具有由上管板部（在螺旋形热交换器的情况下为上盖部）形成的排气管的一端的至少一部分，另一端与热交换器外侧连接，流体通过口通过与排气管相同的流体和/或由下管板部分（在螺旋式热交换器的情况下为下盖部分）形成的排水管的至少一部分，并且其另一端连接在热交换器外面，与通过与排水管相同的流体的紧邻的流体通过口。

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