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1. 发明授权

US07151197B2 Processes for purifying chlorofluorinated compounds and processes for purifying CF3CFHCF3 失效
标题翻译：纯化氟氯化合物的方法和纯化CF3CFHCF3的方法
公开(公告)号：US07151197B2
公开(公告)日：2006-12-19
申请号：US10698579
申请日：2003-10-31
申请人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
发明人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
IPC分类号： C07C17/383 , C07C17/38 , C07C17/386 , C07C17/395 , C07C17/389
CPC分类号： C07C17/383 , B01J23/44 , B01J23/8926 , B01J27/128 , B01J27/132 , C07C17/10 , C07C17/206 , C07C17/23 , C07C17/38 , C07C17/395 , Y02P20/582 , C07C19/10 , C07C19/08
摘要： Methods and materials are provided for the production of essentially isomerically pure perhalogenated and partially halogenated compounds. One embodiment of the present invention provides a process for the production of essentially isomerically pure CFC-216aa. Other embodiments include processes for the production of CFC-217ba and HFC-227ea. Particular embodiments of the present invention provide separation techniques for the separation of chlorofluorocarbons from HF, from other chlorofluorocarbons, and the separation of isomers of halogenated compounds. Still other embodiments of the present invention provide catalytic synthetic techniques that demonstrate extended catalyst lifetime. In other embodiments, the present invention provides catalytic techniques for the purification of isomeric mixtures.
摘要翻译：提供了用于生产基本上异构纯的全卤代和部分卤代化合物的方法和材料。本发明的一个实施方案提供了生产基本上异构纯的CFC-216aa的方法。其它实施方案包括生产CFC-217ba和HFC-227ea的方法。本发明的具体实施方案提供了将氯氟烃与其它氯氟烃分开的分离技术以及卤代化合物异构体的分离。本发明的其它实施方案提供催化合成技术，其显示延长的催化剂寿命。在其它实施方案中，本发明提供用于纯化异构体混合物的催化技术。

2. 发明授权

US07348461B2 Processes for halogenating compounds 失效
标题翻译：卤化化合物的方法
公开(公告)号：US07348461B2
公开(公告)日：2008-03-25
申请号：US10698731
申请日：2003-10-31
申请人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
发明人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
IPC分类号： C07C17/06 , C07C17/013
CPC分类号： C07C17/383 , B01J23/44 , B01J23/8926 , B01J27/128 , B01J27/132 , C07C17/10 , C07C17/206 , C07C17/23 , C07C17/38 , C07C17/395 , Y02P20/582 , C07C19/10 , C07C19/08
摘要： Methods and materials are provided for the production of essentially isomerically pure perhalogenated and partially halogenated compounds. One embodiment of the present invention provides a process for the production of essentially isomerically pure CFC-216aa. Other embodiments include processes for the production of CFC-217ba and HFC-227ea. Particular embodiments of the present invention provide separation techniques for the separation of chlorofluorocarbons from HF, from other chlorofluorocarbons, and the separation of isomers of halogenated compounds. Still other embodiments of the present invention provide catalytic synthetic techniques that demonstrate extended catalyst lifetime. In other embodiments, the present invention provides catalytic techniques for the purification of isomeric mixtures.
摘要翻译：提供了用于生产基本上异构纯的全卤代和部分卤代化合物的方法和材料。本发明的一个实施方案提供了生产基本上异构纯的CFC-216aa的方法。其它实施方案包括生产CFC-217ba和HFC-227ea的方法。本发明的具体实施方案提供了将氯氟烃与其它氯氟烃分开的分离技术以及卤代化合物异构体的分离。本发明的其它实施方案提供催化合成技术，其显示延长的催化剂寿命。在其它实施方案中，本发明提供用于纯化异构体混合物的催化技术。

3. 发明授权

US07335805B2 Processes for purifying reaction products and processes for separating chlorofluorinated compounds 失效
标题翻译：用于纯化反应产物的方法和用于分离氯氟化合物的方法
公开(公告)号：US07335805B2
公开(公告)日：2008-02-26
申请号：US10699491
申请日：2003-10-31
申请人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
发明人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
IPC分类号： C07C17/38
CPC分类号： C07C17/383 , B01J23/44 , B01J23/8926 , B01J27/128 , B01J27/132 , C07C17/10 , C07C17/206 , C07C17/23 , C07C17/38 , C07C17/395 , Y02P20/582 , C07C19/10 , C07C19/08
摘要： Methods and materials are provided for the production of essentially isomerically pure perhalogenated and partially halogenated compounds. One embodiment of the present invention provides a process for the production of essentially isomerically pure CFC-216aa. Other embodiments include processes for the production of CFC-217ba and HFC-227ea. Particular embodiments of the present invention provide separation techniques for the separation of chlorofluorocarbons from HF, from other chlorofluorocarbons, and the separation of isomers of halogenated compounds. Still other embodiments of the present invention provide catalytic synthetic techniques that demonstrate extended catalyst lifetime. In other embodiments, the present invention provides catalytic techniques for the purification of isomeric mixtures.
摘要翻译：提供了用于生产基本上异构纯的全卤代和部分卤代化合物的方法和材料。本发明的一个实施方案提供了生产基本上异构纯的CFC-216aa的方法。其它实施方案包括生产CFC-217ba和HFC-227ea的方法。本发明的具体实施方案提供了将氯氟烃与其它氯氟烃分开的分离技术以及卤代化合物异构体的分离。本发明的其它实施方案提供催化合成技术，其显示延长的催化剂寿命。在其它实施方案中，本发明提供用于纯化异构体混合物的催化技术。

4. 发明授权

US07332635B2 Processes for purifying chlorofluorinated compounds 失效
标题翻译：氯氟化合物的净化方法
公开(公告)号：US07332635B2
公开(公告)日：2008-02-19
申请号：US10698730
申请日：2003-10-31
申请人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
发明人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Qian , Julie Sacarias
IPC分类号： C07C17/00 , C07C17/35 , C07C17/38
CPC分类号： C07C17/383 , B01J23/44 , B01J23/8926 , B01J27/128 , B01J27/132 , C07C17/10 , C07C17/206 , C07C17/23 , C07C17/38 , C07C17/395 , Y02P20/582 , C07C19/10 , C07C19/08
摘要： Methods and materials are provided for the production of essentially isomerically pure perhalogenated and partially halogenated compounds. One embodiment of the present invention provides a process for the production of essentially isomerically pure CFC-216aa. Other embodiments include processes for the production of CFC-217ba and HFC-227ea. Particular embodiments of the present invention provide separation techniques for the separation of chlorofluorocarbons from HF, from other chlorofluorocarbons, and the separation of isomers of halogenated compounds. Still other embodiments of the present invention provide catalytic synthetic techniques that demonstrate extended catalyst lifetime. In other embodiments, the present invention provides catalytic techniques for the purification of isomeric mixtures.
摘要翻译：提供了用于生产基本上异构纯的全卤代和部分卤代化合物的方法和材料。本发明的一个实施方案提供了生产基本上异构纯的CFC-216aa的方法。其它实施方案包括生产CFC-217ba和HFC-227ea的方法。本发明的具体实施方案提供了将氯氟烃与其它氯氟烃分开的分离技术以及卤代化合物异构体的分离。本发明的其它实施方案提供催化合成技术，其显示延长的催化剂寿命。在其它实施方案中，本发明提供用于纯化异构体混合物的催化技术。

5. 发明授权

US07329786B2 Processes for producing CF3CFHCF3 失效
标题翻译：生产CF3CFHCF3的方法
公开(公告)号：US07329786B2
公开(公告)日：2008-02-12
申请号：US09966158
申请日：2001-09-28
申请人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Chengping Chien , Julie Sacarias , Vimal Sharma
发明人： Yuichi Iikubo , Stephen Owens , Mitchel Cohn , Stephan M. Brandstadter , Vicki E. Hedrick , Janet K. Boggs , John Chengping Chien , Julie Sacarias , Vimal Sharma
IPC分类号： C07C17/013 , C07C17/093 , C07C17/10 , C07C17/35 , C07C19/08
CPC分类号： C07C17/383 , B01J23/44 , B01J23/8926 , B01J27/128 , B01J27/132 , C07C17/10 , C07C17/206 , C07C17/23 , C07C17/38 , C07C17/395 , Y02P20/582 , C07C19/10 , C07C19/08
摘要： Methods and materials are provided for the production of essentially isomerically pure perhalogenated and partially halogenated compounds. One embodiment of the present invention provides a process for the production of essentially isomerically pure CFC-216aa. Other embodiments include processes for the production of CFC-217ba and HFC-227ea. Particular embodiments of the present invention provide separation techniques for the separation of chlorofluorocarbons from HF, from other chlorofluorocarbons, and the separation of isomers of halogenated compounds. Still other embodiments of the present invention provide catalytic synthetic techniques that demonstrate extended catalyst lifetime. In other embodiments, the present invention provides catalytic techniques for the purification of isomeric mixtures.
摘要翻译：提供了用于生产基本上异构纯的全卤代和部分卤代化合物的方法和材料。本发明的一个实施方案提供了生产基本上异构纯的CFC-216aa的方法。其它实施方案包括生产CFC-217ba和HFC-227ea的方法。本发明的具体实施方案提供了将氯氟烃与其它氯氟烃分开的分离技术以及卤代化合物异构体的分离。本发明的其它实施方案提供催化合成技术，其显示延长的催化剂寿命。在其它实施方案中，本发明提供用于纯化异构体混合物的催化技术。

6. 发明授权

US07368089B2 Systems and methods for producing fluorocarbons 失效
标题翻译：碳氟化合物的制备方法
公开(公告)号：US07368089B2
公开(公告)日：2008-05-06
申请号：US11069180
申请日：2005-02-28
申请人： Vicki E. Hedrick , Janet K. Boggs , Stephen M. Brandstadter , Mitchel Cohn
发明人： Vicki E. Hedrick , Janet K. Boggs , Stephen M. Brandstadter , Mitchel Cohn
IPC分类号： B01J19/00
CPC分类号： C07C17/354 , B01J23/8926 , B01J27/08 , B01J27/128 , B01J27/13 , B01J35/0006 , C07C17/23 , C07C19/08 , C07C21/18 , C07C19/10
摘要： Systems and methods for producing fluorocarbons are provided that include contacting a saturated halogenated fluorocarbon with hydrogen and catalyst to produce a saturated hydrofluorocarbon and an unsaturated fluorocarbon. Aspects of the present invention describe systems and methods for contacting saturated halogenated fluorocarbons such as CF3CClFCF3 and/or CF3CCl2CF3 with hydrogen and catalyst. Systems and methods of the present invention also describe contacting saturated halogenated fluorocarbons with catalysts having one or more of K, Zr, Na, Ni, Cu, Ni, Zn, Fe, Mn, Co, Ti, and Pd. Aspects of the present invention also describe contacting saturated halogenated fluorocarbons with hydrogen under pressure. Saturated hydroflourocarbons and unsaturated fluorocarbons produced in accordance with the systems and methods of the present invention can include one or more of CF3CFHCF3, CF3CH2CF3, CF3CHClCF3, CF3CF═CF2, CF3CH═CF2, and CF3CCl═CF2.
摘要翻译：提供了制备碳氟化合物的系统和方法，包括使饱和卤代碳氟化合物与氢气和催化剂接触以产生饱和氢氟碳化合物和不饱和氟碳化合物。本发明的方面描述了用于使饱和卤代碳氟化合物如CF 3 CClFC 3 3和/或CF 3 CCl 3和/ 2 CO 3与氢气和催化剂反应。本发明的系统和方法还描述了使饱和卤代碳氟化合物与具有一种或多种K，Zr，Na，Ni，Cu，Ni，Zn，Fe，Mn，Co，Ti和Pd的催化剂接触。本发明的方面还描述了在压力下使饱和卤代碳氟化合物与氢接触。根据本发明的系统和方法生产的饱和氢氟烃和不饱和碳氟可以包括一种或多种CF 3 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3 CF 3，CF 3，CF 3 CF 3，CF 3 CF 3，CF 3，CF 3 CF 3， CF 2，CF 3，CH-CF 2，CF 3，CCl-CF 2， SUB>。

7. 发明申请

US20060161029A1 Production and purification processes 审中-公开
标题翻译：生产和净化过程
公开(公告)号：US20060161029A1
公开(公告)日：2006-07-20
申请号：US11323365
申请日：2005-12-29
申请人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Qian , Julia Sacarias , Yuichi Iikubo
发明人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Qian , Julia Sacarias , Yuichi Iikubo
IPC分类号： C07C17/32 , C07C17/26
CPC分类号： C07C19/08 , C07C17/00 , C07C17/21 , C07C17/25 , C07C17/278 , C07C17/38 , C07C17/383 , C07C17/386 , C07C21/18 , C07C21/04 , C07C19/01
摘要： Methods and materials are provided for the production and purification of halogenated compounds and intermediates in the production of 1,1,1,3,3-pentafluoropropane. In a preferred embodiment, the process steps include: (1) reacting carbon tetrachloride with vinyl chloride to produce 1,1,1,3,3-pentachloropropane; (2) dehydrochlorinating the 1,1,1,3,3-pentachloropropane with a Lewis acid catalyst to produce 1,1,3,3-tetrachloropropene; (3) fluorinating the 1,1,3,3-tetrachloroprope-ne to produce 1-chloro-3,3,3-trifluoropropene; (4) fluorinating the 1-chloro-3,3,3-trifluoropropene to produce a product mixture containing 1,1,1,3,3-pentafluoropropane; and (5) separating 1,1,1,3,3-pentafluoropro-pane from by-products.
摘要翻译：提供了生产和提纯卤代化合物和中间产物1,1,1,3,3-五氟丙烷的方法和材料。在优选的实施方案中，方法步骤包括：（1）使四氯化碳与氯乙烯反应，生成1,1,1,3,3-五氯丙烷; （2）用路易斯酸催化剂对1,1,1,3,3-五氯丙烷进行脱氯化氢以制备1,1,3,3-四氯丙烯; （3）使1,1,3,3-四氯丙炔氟化，生成1-氯-3,3,3-三氟丙烯; （4）氟化1-氯-3,3,3-三氟丙烯以制备含有1,1,1,3,3-五氟丙烷的产物混合物; 和（5）从副产物中分离1,1,1,3,3-五氟平板。

8. 发明申请

US20050101810A1 Processes for separating 1,1,1,3,3-pentafluoropropane from a mixture comprising 1,1,1,3,3-pentafluoropropane and 1-chloro-3,3,3-trifluoropropene 审中-公开
标题翻译：从1,1,1,3,3-五氟丙烷和1-氯-3,3,3-三氟丙烯的混合物中分离1,1,1,3,3-五氟丙烷的方法
公开(公告)号：US20050101810A1
公开(公告)日：2005-05-12
申请号：US11006987
申请日：2004-12-08
申请人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Qian , Julia Sacarias , Yuichi Iikubo
发明人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Qian , Julia Sacarias , Yuichi Iikubo
IPC分类号： C07C17/00 , C07C17/21 , C07C17/25 , C07C17/278 , C07C17/38 , C07C17/383 , C07C17/386 , C07C19/08
CPC分类号： C07C19/08 , C07C17/00 , C07C17/21 , C07C17/25 , C07C17/278 , C07C17/38 , C07C17/383 , C07C17/386 , C07C21/18 , C07C21/04 , C07C19/01
摘要： Methods and materials are provided for the production and purification of halogenated compounds and intermediates in the production of 1,1,1,3,3-pentafluoropropane. In a preferred embodiment, the process steps include: (1) reacting carbon tetrachloride with vinyl chloride to produce 1,1,1,3,3-pentachloropropane; (2) dehydrochlorinating the 1,1,1,3,3 -pentachloropropane with a Lewis acid catalyst to produce 1,1,3,3-tetrachloropropene; (3) fluorinating the 1,1,3,3-tetrachloropropene to produce 1-chloro-3,3,3-trifluoropropene; (4) fluorinating the 1-chloro-3,3,3-trifluoropropene to produce a product mixture containing 1,1,1,3,3 -pentafluoropropane; and (5) separating 1,1,1,3,3-pentafluoropropane from by-products.
摘要翻译：提供了生产和提纯卤代化合物和中间产物1,1,1,3,3-五氟丙烷的方法和材料。在优选的实施方案中，方法步骤包括：（1）使四氯化碳与氯乙烯反应，生成1,1,1,3,3-五氯丙烷; （2）用路易斯酸催化剂对1,1,1,3,3-三氯丙烷进行脱氯化氢，得到1,1,3,3-四氯丙烯; （3）使1,1,3,3-四氯丙烯氟化，得到1-氯-3,3,3-三氟丙烯; （4）氟化1-氯-3,3,3-三氟丙烯以制备含有1,1,1,3,3-五氟丙烷的产物混合物; 和（5）从副产物中分离1,1,1,3,3-五氟丙烷。

9. 发明授权

US07094936B1 Process for preparing halogenated alkanes 失效
标题翻译：制备卤代烷烃的方法
公开(公告)号：US07094936B1
公开(公告)日：2006-08-22
申请号：US10688230
申请日：2003-10-16
申请人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Cheng-Ping Qian , Julia Ann Sacarias , Yuichi Iikubo
发明人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Cheng-Ping Qian , Julia Ann Sacarias , Yuichi Iikubo
IPC分类号： C07C17/278 , C07C17/272 , C07C17/26
CPC分类号： C07C19/08 , C07C17/00 , C07C17/21 , C07C17/25 , C07C17/278 , C07C17/38 , C07C17/383 , C07C17/386 , C07C21/18 , C07C21/04 , C07C19/01
摘要： Methods and materials are provided for the production and purification of halogenated compounds and intermediates in the production of 1,1,1,3,3-pentafluoropropane. In a preferred embodiment, the process steps include: (1) reacting carbon tetrachloride with vinyl chloride to produce 1,1,1,3,3-pentachloropropane; (2) dehydrochlorinating the 1,1,1,3,3-pentachloropropane with a Lewis acid catalyst to produce 1,1,3,3-tetrachloropropene; (3) fluorinating the 1,1,3,3-tetrachloropropene to produce 1-chloro-3,3,3-trifluoropropene; (4) fluorinating the 1-chloro-3,3,3-trifluoropropene to produce a product mixture containing 1,1,1,3,3-pentafluoropropane; and (5) separating 1,1,1,3,3-pentafluoropropane from by-products.
摘要翻译：提供了生产和提纯卤代化合物和中间产物1,1,1,3,3-五氟丙烷的方法和材料。在优选的实施方案中，方法步骤包括：（1）使四氯化碳与氯乙烯反应，生成1,1,1,3,3-五氯丙烷; （2）用路易斯酸催化剂对1,1,1,3,3-五氯丙烷进行脱氯化氢以制备1,1,3,3-四氯丙烯; （3）使1,1,3,3-四氯丙烯氟化，得到1-氯-3,3,3-三氟丙烯; （4）氟化1-氯-3,3,3-三氟丙烯以制备含有1,1,1,3,3-五氟丙烷的产物混合物; 和（5）从副产物中分离1,1,1,3,3-五氟丙烷。

10. 发明申请

US20080154072A1 Production Vessel Mixtures 审中-公开
标题翻译：生产容器混合物
公开(公告)号：US20080154072A1
公开(公告)日：2008-06-26
申请号：US11950611
申请日：2007-12-05
申请人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Cheng-Ping Qian , Julia Ann Sacarias , Yuichi Iikubo
发明人： Stephen Owens , Andrew Jackson , Vimal Sharma , Mitchel Cohn , John Cheng-Ping Qian , Julia Ann Sacarias , Yuichi Iikubo
IPC分类号： C07C19/08
CPC分类号： C07C19/08 , C07C17/00 , C07C17/21 , C07C17/25 , C07C17/278 , C07C17/38 , C07C17/383 , C07C17/386 , C07C21/18 , C07C21/04 , C07C19/01
摘要： Methods and materials are provided for the production and purification of halogenated compounds and intermediates in the production of 1,1,1,3,3-pentafluoropropane. In a preferred embodiment, the process steps include: (1) reacting carbon tetrachloride with vinyl chloride to produce 1,1,1,3,3-pentachloropropane; (2) dehydrochlorinating the 1,1,1,3,3-pentachloropropane with a Lewis acid catalyst to produce 1,1,3,3-tetrachloropropene; (3) fluorinating the 1,1,3,3-tetrachloropropene to produce 1-chloro-3,3,3-trifluoropropene; (4) fluorinating the 1-chloro-3,3,3-trifluoropropene to produce a product mixture containing 1,1,1,3,3-pentafluoropropane; and (5) separating 1,1,1,3,3-pentafluoropro-pane from by-products.
摘要翻译：提供了生产和提纯卤代化合物和中间产物1,1,1,3,3-五氟丙烷的方法和材料。在优选的实施方案中，方法步骤包括：（1）使四氯化碳与氯乙烯反应，生成1,1,1,3,3-五氯丙烷; （2）用路易斯酸催化剂对1,1,1,3,3-五氯丙烷进行脱氯化氢以制备1,1,3,3-四氯丙烯; （3）使1,1,3,3-四氯丙烯氟化，得到1-氯-3,3,3-三氟丙烯; （4）氟化1-氯-3,3,3-三氟丙烯以制备含有1,1,1,3,3-五氟丙烷的产物混合物; 和（5）从副产物中分离1,1,1,3,3-五氟平板。

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