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1. 发明授权

US5952439A Epoxy group-containing silicone resin and compositions based thereon 失效
标题翻译：含环氧基的硅氧烷树脂及其组合物
公开(公告)号：US5952439A
公开(公告)日：1999-09-14
申请号：US226539
申请日：1994-04-12
申请人： Yoshitsugu Morita , Junji Nakanishi , Ken Tanaka , Toshio Saruyama
发明人： Yoshitsugu Morita , Junji Nakanishi , Ken Tanaka , Toshio Saruyama
IPC分类号： C08G59/32 , C08G77/14 , C08L61/06 , C08L63/00 , C08L79/08 , C08L83/06 , C08L101/00 , C08G77/00 , C08L283/00
CPC分类号： C08L61/06 , C08G59/3254 , C08G77/14 , C08L101/00 , C08L79/08 , C08L83/06 , C08L63/00
摘要： There is disclosed a curable resin composition that has an excellent fluidity prior to curing and that cures to form a molding resin that is flexible, highly moisture resistant, and strongly resistant to heat shock, said composition comprising(A) 100 weight parts of a curable resin; and(B) 0.1 to 500 weight parts of an epoxy group-containing silicone resin that has the general formula(R.sup.1 SiO.sub.3/2).sub.a (R.sup.2 R.sup.3 SiO.sub.2/2).sub.b (SiO.sub.4/2).sub.cwherein R.sup.1, R.sup.2 and R.sup.3 each represents a group selected from the group consisting of an epoxy group-containing organic group and a monovalent hydrocarbon group with the proviso that said epoxy group-containing organic groups comprise 0.1 to 40 mole percent of the total silicon-bonded organic groups in said silicone resin (B), a is a positive number, b is zero or a positive number, c is zero or a positive number, b/a has a value of zero to 10, c/(a+b+c) has a value of zero to 0.3 and said silicone resin (B) has a glass-transition temperature of -90.degree. C. to 150.degree. C.
摘要翻译：公开了一种固化性树脂组合物，其在固化前具有优异的流动性，并且可固化形成柔性，高度防潮并且耐热冲击性强的模制树脂，所述组合物包含（A）100重量份的可固化树脂; 和（B）0.1〜500重量份具有通式（R1SiO3 / 2）a（R2R3SiO2 / 2）b（SiO4 / 2）c的含环氧基的有机硅树脂，其中R1，R2和R3各自表示基团选自含有环氧基的有机基团和一价烃基，条件是所述含环氧基的有机基团包含所述有机硅树脂（B）中的总硅键合有机基团的0.1至40摩尔％，a为正数，b为零或正数，c为零或正数，b / a的值为零至10，c /（a + b + c）的值为零至0.3 所述有机硅树脂（B）的玻璃化转变温度为-90℃〜150℃。

2. 发明授权

US5516858A Epoxy group-containing silicone resin and compositions based thereon 失效
公开(公告)号：US5516858A
公开(公告)日：1996-05-14
申请号：US419685
申请日：1995-04-10
申请人： Yoshitsugu Morita , Junji Nakanishi , Ken Tanaka , Toshio Saruyama
发明人： Yoshitsugu Morita , Junji Nakanishi , Ken Tanaka , Toshio Saruyama
IPC分类号： C08G59/32 , C08G77/14 , C08L61/06 , C08L63/00 , C08L79/08 , C08L83/06 , C08L101/00 , C08F283/00 , C08G77/00
CPC分类号： C08L61/06 , C08G59/3254 , C08G77/14 , C08L101/00 , C08L79/08 , C08L83/06 , C08L63/00
摘要： There is disclosed a curable resin composition that has an excellent fluidity prior to curing and that cures to form a molding resin that is flexible, highly moisture resistant, and strongly resistant to heat shock, said composition comprising(A) 100 weight parts of a curable resin; and(B) 0.1 to 500 weight parts of an epoxy group-containing silicone resin that has the general formula(R.sup.1 SiO.sub.3/2).sub.a (R.sup.2 R.sup.3 SiO.sub.2/2).sub.b (SiO.sub.4/2).sub.cwherein R.sup.1, R.sup.2 and R.sup.3 each represents a group selected from the group consisting of an epoxy group-containing organic group and a monovalent hydrocarbon group with the proviso that said epoxy group-containing organic groups comprise 0.1 to 40 mole percent of the total silicon-bonded organic groups in said silicone resin (B), a is a positive number, b is zero or a positive number, c is zero or a positive number, b/a has a value of zero to 10, c/(a+b+c) has a value of zero to 0.3 and said silicone resin (B) has a glass-transition temperature of -90.degree. C. to 150.degree. C.

3. 发明授权

US06710124B2 Water base coating material composition and production process 有权
标题翻译：水基涂料组成及生产工艺
公开(公告)号：US06710124B2
公开(公告)日：2004-03-23
申请号：US09940314
申请日：2001-08-27
申请人： Yoshitsugu Morita , Kazuo Kobayashi , Ken Tanaka
发明人： Yoshitsugu Morita , Kazuo Kobayashi , Ken Tanaka
IPC分类号： C08L8304
CPC分类号： C09D183/04 , C08L83/04 , C09D7/65 , C09D7/68 , C09D7/69
摘要： Water base coating material compositions form coating films of superior flat finish properties. They contain silicone particles with at least two kinds of different average particle size. According to the method of making the composition, a water base coating material composition can be formed by adding an aqueous suspension of silicone particles to a water base coating material composition where the aqueous suspension contains at least two kinds of silicone particles with different average particle size.
摘要翻译：水性涂料组合物形成具有优异平整性的涂膜。它们含有至少两种不同平均粒径的硅氧烷颗粒。根据制备组合物的方法，可以通过向水性涂料组合物中加入硅氧烷颗粒的水性悬浮液形成水性涂料组合物，其中水性悬浮液含有至少两种平均粒度不同的硅氧烷颗粒。

4. 发明授权

US06433041B1 Method for producing water based coating compositions 有权
公开(公告)号：US06433041B1
公开(公告)日：2002-08-13
申请号：US09753843
申请日：2001-01-03
申请人： Kazuo Kobayashi , Yoshitsugu Morita , Ken Tanaka
发明人： Kazuo Kobayashi , Yoshitsugu Morita , Ken Tanaka
IPC分类号： C08D18304
摘要： An efficient method is provided for producing water based coating compositions that are capable of forming highly scratch and abrasion resistant matte coatings in which crosslinked silicone particles are well dispersed. The method involves addition to a water based coating composition of a waterborne suspension of crosslinked silicone particles having an average diameter of 0.1-200 &mgr;m. The method is characterized in that the suspension is a waterborne crosslinked silicone particle suspension provided by effecting crosslinking of a condensation reaction crosslinkable silicone composition comprising (A) an organopolysiloxane containing at least two silanol groups in each molecule, (B) a crosslinker, and (C) a condensation reaction catalyst. The crosslinking is effected in the emulsified composition in an aqueous solution of an anionic surfactant.

5. 发明授权

US08217122B2 Silicone rubber powder and method of manufacturing thereof 有权
标题翻译：硅橡胶粉及其制造方法
公开(公告)号：US08217122B2
公开(公告)日：2012-07-10
申请号：US12675508
申请日：2008-08-19
申请人： Yoshitsugu Morita , Kazuo Kobayashi , Ken Tanaka
发明人： Yoshitsugu Morita , Kazuo Kobayashi , Ken Tanaka
IPC分类号： C08J3/24 , C08G77/12
CPC分类号： C08K5/5435 , C08G77/12 , C08G77/16 , C08J3/24 , C08J3/26 , C08J2383/04 , C08K5/57 , C08L83/04 , C08L83/00
摘要： A silicone rubber powder obtained by curing a condensation-curable silicone rubber composition in a dispersed state in water, having an epoxy equivalent measured by a titration method equal to or lower than 3,000 and an average particle size in the range of 0.1 to 100 μm; and a method of manufacturing a silicone rubber powder comprising the steps of dispersing in water a silicone rubber composition comprising at least components (A) through (C) listed below; adding component (D); and curing the mixture: (A) a diorganopolysiloxane capped at both molecular terminals with silanol groups and having in one molecule 30 or less silicon atoms; (B) an organopolysiloxane having in one molecule at least two silicon-bonded hydrogen atoms; (C) an epoxy-containing alkoxysilane; and (D) a condensation-reaction catalyst. The silicone rubber powder has low epoxy equivalent and possesses excellent dispersibility in organic resins, and the method is efficient in manufacturing of the aforementioned powder.
摘要翻译：将分散状态的可缩合固化硅橡胶组合物在水中固化，通过滴定法测定的环氧当量为3000以下，平均粒径为0.1〜100μm的方法得到的硅橡胶粉末; 和一种制造硅橡胶粉末的方法，包括以下步骤：在水中分散包含至少包含以下列出的组分（A）至（C）的硅橡胶组合物; 添加组分（D）; 并固化该混合物：（A）在两个分子末端用硅烷醇基封端并且在一个分子中具有30个或更少硅原子的二有机聚硅氧烷; （B）在一个分子中具有至少两个与硅键合的氢原子的有机聚硅氧烷; （C）含环氧基的烷氧基硅烷; 和（D）缩合反应催化剂。硅橡胶粉末具有低环氧当量，并且在有机树脂中具有优异的分散性，并且该方法在制备上述粉末中是有效的。

6. 发明申请

US20100216952A1 Silicone Rubber Powder And Method Of Manufacturing Thereof 有权
标题翻译：硅橡胶粉及其制造方法
公开(公告)号：US20100216952A1
公开(公告)日：2010-08-26
申请号：US12675508
申请日：2008-08-19
申请人： Yoshitsugu Morita , Kazuo Kobayashi , Ken Tanaka
发明人： Yoshitsugu Morita , Kazuo Kobayashi , Ken Tanaka
IPC分类号： C08J3/24 , C08G77/12
CPC分类号： C08K5/5435 , C08G77/12 , C08G77/16 , C08J3/24 , C08J3/26 , C08J2383/04 , C08K5/57 , C08L83/04 , C08L83/00
摘要： A silicone rubber powder obtained by curing a condensation-curable silicone rubber composition in a dispersed state in water, having an epoxy equivalent measured by a titration method equal to or lower than 3,000 and an average particle size in the range of 0.1 to 100 μm; and a method of manufacturing a silicone rubber powder comprising the steps of dispersing in water a silicone rubber composition comprising at least components (A) through (C) listed below; adding component (D); and curing the mixture: (A) a diorganopolysiloxane capped at both molecular terminals with silanol groups and having in one molecule 30 or less silicon atoms; (B) an organopolysiloxane having in one molecule at least two silicon-bonded hydrogen atoms; (C) an epoxy-containing alkoxysilane; and (D) a condensation-reaction catalyst. The silicone rubber powder has low epoxy equivalent and possesses excellent dispersibility in organic resins, and the method is efficient in manufacturing of the aforementioned powder.
摘要翻译：将分散状态的可缩合固化硅橡胶组合物在水中固化，通过滴定法测定的环氧当量为3000以下，平均粒径为0.1〜100μm的方法得到的硅橡胶粉末; 和一种制造硅橡胶粉末的方法，包括以下步骤：在水中分散包含至少包含以下列出的组分（A）至（C）的硅橡胶组合物; 添加组分（D）; 并固化该混合物：（A）在两个分子末端用硅烷醇基封端并且在一个分子中具有30个或更少硅原子的二有机聚硅氧烷; （B）在一个分子中具有至少两个与硅键合的氢原子的有机聚硅氧烷; （C）含环氧基的烷氧基硅烷; 和（D）缩合反应催化剂。硅橡胶粉末具有低环氧当量，并且在有机树脂中具有优异的分散性，并且该方法在制备上述粉末中是有效的。

7. 发明授权

US06437042B2 Method for producing suspension of crosslinked silicone particles 有权
标题翻译：交联硅氧烷颗粒悬浮液的制备方法
公开(公告)号：US06437042B2
公开(公告)日：2002-08-20
申请号：US09753772
申请日：2001-01-03
申请人： Kazuo Kobayashi , Yoshitsugu Morita , Ken Tanaka
发明人： Kazuo Kobayashi , Yoshitsugu Morita , Ken Tanaka
IPC分类号： C08G7708
CPC分类号： C08J3/215 , C08J3/26 , C08J2383/04 , Y10T428/2991 , Y10T428/2995
摘要： A suspension containing crosslinked silicone particles with a lower mean particle diameter and a better dispersion in certain organic resins is prepared by emulsifying a condensation crosslinkable silicone composition containing (A) an organopolysiloxane having at least two silanol groups per molecule and (B) a crosslinker, but no (C) condensation catalyst, in water using a surfactant. A tin (II) salt of an organic acid with no more than ten carbon atoms is then emulsified in water with a surfactant, and added as the component (C) to the emulsion of condensation crosslinkable silicone composition. This crosslinks the emulsion of condensation crosslinkable silicone composition.
摘要翻译：通过乳化含有（A）每分子具有至少两个硅烷醇基团的有机聚硅氧烷和（B）交联剂的缩合交联性硅氧烷组合物，制备含有具有较低平均粒径和较好的分散在某些有机树脂中的交联硅氧烷颗粒的悬浮液，但没有（C）缩合催化剂，在水中使用表面活性剂。然后将具有不超过10个碳原子的有机酸的锡（II）盐与表面活性剂在水中乳化，并作为组分（C）加入到缩合交联性有机硅组合物的乳液中。这使交联聚硅氧烷缩合物的乳液交联。

8. 发明授权

US5422412A Organopolysiloxane and method for the preparation thereof 失效
标题翻译：有机聚硅氧烷及其制备方法
公开(公告)号：US5422412A
公开(公告)日：1995-06-06
申请号：US263589
申请日：1994-06-22
申请人： Yoshitsugu Morita , Ken Tanaka
发明人： Yoshitsugu Morita , Ken Tanaka
IPC分类号： C08G77/38 , C08G77/48 , C08G77/50 , C08G77/08
CPC分类号： C08G77/485 , C08G77/50
摘要： An organopolysiloxane suitable for modifying curable organic and silicone compositions is disclosed, said organopolysiloxane having the general formula ##STR1## wherein each R.sup.1 is a monovalent group independently selected from the group consisting of alkyl radicals having 1 to 5 carbon atoms and phenyl radical; R.sup.2 is a monovalent group independently selected from the group consisting of hydrogen, alkyl radicals having 1 to 5 carbon atoms and phenyl radical; R.sup.3 is selected from the group consisting of alkoxysilylalkyl groups and alkyl groups having at least 6 carbon atoms; a is zero or a positive number; b is a positive number; c is a positive number; a/c has a value of zero to
摘要翻译：公开了适用于改性可固化的有机和有机硅组合物的有机聚硅氧烷，所述有机聚硅氧烷具有通式“IMAGE”，其中每个R 1是独立地选自具有1至5个碳原子的烷基和苯基的一价基团; R2是独立地选自氢，具有1-5个碳原子的烷基和苯基的一价基团; R3选自烷氧基甲硅烷基烷基和具有至少6个碳原子的烷基; a为零或正数; b是正数; c是正数; a / c的值为零至<4; b / c的值为0.05〜4; 和（a + b）/ c的值为0.2至4，条件是所述有机聚硅氧烷在其分子中具有至少一个所述烷氧基甲硅烷基烷基和至少一个所述具有至少6个碳原子的烷基。

9. 发明授权

US09056925B2 Process for production of modified conjugated diene polymers, modified conjugated diene polymers produced by the process, rubber compositions, and tires 有权
标题翻译：改性共轭二烯聚合物的制备方法，通过该方法制备的改性共轭二烯聚合物，橡胶组合物和轮胎
公开(公告)号：US09056925B2
公开(公告)日：2015-06-16
申请号：US12446799
申请日：2007-10-25
申请人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
发明人： Ken Tanaka , Kouji Masaki , Yoichi Ozawa , Eiji Suzuki , Christine M. Rademacher , Terrence E. Hogan , Takuo Sone , Takaomi Matsumoto
IPC分类号： C08L83/00 , C08C19/25 , B60C1/00 , C08C19/44 , C08L15/00 , C08L21/00
CPC分类号： C08C19/25 , B60C1/0016 , B60C1/0025 , C08C19/44 , C08K3/04 , C08K3/36 , C08L9/00 , C08L15/00 , C08L21/00 , C08L2666/08
摘要： A process for producing a modified conjugated diene based polymer includes a step (a) of reacting a silicon compound with a conjugated diene based polymer having an active end so that the reaction takes place at the active end, the silicon compound having a protected primary amino group in the molecule thereof and a silicon atom to which a hydrocarbyloxy group and a reactive group are bonded, to thereby modify the active end, and a step (b) of performing condensation reaction, in the presence of a titanium compound serving as a titanium-based condensation-accelerating agent. A rubber composition contains the modified diene polymer, and a tire is produced from the rubber composition.
摘要翻译：改性共轭二烯系聚合物的制造方法包括使硅化合物与具有活性末端的共轭二烯系聚合物反应以使反应在活性末端进行的工序（a），具有被保护的伯氨基在其分子中具有烃氧基和反应性基团键合的硅原子，从而改变活性末端，以及在用作钛的钛化合物的存在下进行缩合反应的步骤（b）的缩合促进剂。橡胶组合物含有改性二烯聚合物，由橡胶组合物制成轮胎。

10. 发明授权

US08809464B2 Polymers functionalized with halosilanes containing an amino group 有权
标题翻译：用含有氨基的卤代硅烷官能化的聚合物
公开(公告)号：US08809464B2
公开(公告)日：2014-08-19
申请号：US13588033
申请日：2012-08-17
申请人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Junko Matsushita , Ryuji Nakagawa , Eiju Suzuki , Ken Tanaka
发明人： Terrence E. Hogan , Steven Luo , Yoichi Ozawa , Junko Matsushita , Ryuji Nakagawa , Eiju Suzuki , Ken Tanaka
IPC分类号： C08F236/06 , C08F8/32
CPC分类号： C08C19/44 , C08F8/42 , C08L15/00 , C08L19/006 , C08F297/04
摘要： A method for preparing a functionalized polymer, the method comprising the steps of preparing a reactive polymer, and reacting the reactive polymer with a halosilane compound containing an amino group.
摘要翻译：一种制备官能化聚合物的方法，该方法包括如下步骤：制备反应性聚合物，并使反应性聚合物与含有氨基的卤代硅烷化合物反应。

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