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1. 发明授权

US06291535B1 Silica-magnesium fluoride hydrate composite sols and process for their preparation 失效
标题翻译：二氧化硅 - 氟化镁水合物复合溶胶及其制备方法
公开(公告)号：US06291535B1
公开(公告)日：2001-09-18
申请号：US09455928
申请日：1999-12-07
申请人： Yoshitane Watanabe , Keitaro Suzuki , Osamu Tanegashima , Yoshinari Koyama
发明人： Yoshitane Watanabe , Keitaro Suzuki , Osamu Tanegashima , Yoshinari Koyama
IPC分类号： B01F312
CPC分类号： B82Y30/00 , C01B33/14 , C01F5/28 , C01P2004/50 , C01P2004/64
摘要： A sol comprising silica-magnesium fluoride hydrate composite colloidal particles used in an anti-reflection coating material for forming an anti-reflection coating and a process for its preparation are provided. A sol comprising silica-magnesium fluoride hydrate composite colloidal particles having a ratio of silica to magnesium fluoride hydrate MgF2.nH2O, n being in the range between 0.25 and 0.5, in terms of a SiO2/MgF2 weight ratio of from 0.01 to 5 and a primary particle size of 5 to 50 nm. A process for the preparation of an aqueous sol comprising silica-magnesium fluoride hydrate composite colloidal particles which comprises the steps of adding an aqueous fluoride solution to a mixture liquid of a silica sol and an aqueous magnesium salt solution to produce a slurry of an agglomerate comprising silica-magnesium fluoride hydrate composite colloidal particles and removing the salts formed as by-products. A process for the preparation of an organosol further comprising the step of replacing water in the aqueous sol with an organic solvent.
摘要翻译：提供一种包含用于形成抗反射涂层的防反射涂层材料中的二氧化硅 - 氟化镁水合物复合胶体颗粒及其制备方法。包含二氧化硅 - 氟化镁水合物复合胶体粒子的溶胶，SiO 2 / MgF 2重量比为0.01〜5，二氧化硅与氟化镁水合物的比例为MgF 2·nH 2 O，n为0.25〜0.5的范围，一次粒径为5〜50nm。一种制备包含二氧化硅 - 氟化镁水合物复合胶体颗粒的水性溶胶的方法，包括以下步骤：向二氧化硅溶胶和镁盐水溶液的混合液中加入氟化钠水溶液，以产生附聚物的浆料，其包含二氧化硅 - 氟化镁水合物复合胶体颗粒并除去作为副产物形成的盐。一种制备有机溶胶的方法，还包括用有机溶剂代替水溶胶中的水的步骤。

2. 发明授权

US5906679A Coating compositions employing zinc antimonate anhydride particles 失效
标题翻译：使用锑酸锌酸酐颗粒的涂料组合物
公开(公告)号：US5906679A
公开(公告)日：1999-05-25
申请号：US939202
申请日：1997-09-29
申请人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama
发明人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama
IPC分类号： C01G30/02 , C09K3/16 , C09K21/02 , C09D1/00 , C08K3/10 , C09D5/18 , C09K21/00
CPC分类号： B82Y30/00 , C01G30/02 , C09K21/02 , C09K3/16 , C01P2002/72 , C01P2004/04 , C01P2004/10 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/22 , C01P2006/40 , C01P2006/60 , C01P2006/82 , Y10S524/911
摘要： The invention relates to coating compositions employing zinc antimonate anhydride comprising zinc antimonate anhydride particles and a liquid of a part-hydrolyzed silane coupling agent, a liquid of hydrolyzed ethylsilicate, a liquid of hydrolyzed methylsilicate, or a resin emulsion. The zinc antimonate anhydride particle having a ZnO/Sb.sub.2 O.sub.5 molar ratio in a range of from 0.8 to 1.2, a crystal structure of zinc antimonate anhydride (Zn Sb.sub.2 0.sub.5), and a primary particle size in a range of from 5 to 500 nm. The particle production method comprises the steps of mixing a zinc compound with a colloidal antimony oxide at a ZnO/Sb.sub.2 O.sub.5 molar rate in a range of from 0.8 to 1.2, followed by calcining the mixture within a temperature range of from 500 to 1100.degree. C. The particles are applicable as a flame retardant for plastics, a smoke suppressant, antistatic agent for plastics and glasses, and resistor.
摘要翻译：本发明涉及使用包含锑酸锌酸酐颗粒和部分水解的硅烷偶联剂的液体，水解的硅酸乙酯的液体，水解的甲基硅酸的液体或树脂乳液的锑酸锌酸酐的涂料组合物。 ZnO / Sb 2 O 5摩尔比为0.8〜1.2的锑酸锌酸酐粒子，锑酸锌酸酐（Zn Sb 2 O 5）的结晶结构，一次粒径为5〜500nm。粒子的制造方法包括以0.5〜1.2的ZnO / Sb 2 O 5摩尔比混合锌化合物和胶态氧化锑，然后在500〜1100℃的温度范围内煅烧。该颗粒可用作塑料阻燃剂，防烟剂，塑料和眼镜用抗静电剂和电阻剂。

3. 发明授权

US5861112A Electro-conductive oxide particle and processes for its production 失效
标题翻译：导电氧化物颗粒及其生产方法
公开(公告)号：US5861112A
公开(公告)日：1999-01-19
申请号：US977668
申请日：1997-11-24
申请人： Yoshitane Watanabe , Keitaro Suzuki , Motoko Iijima
发明人： Yoshitane Watanabe , Keitaro Suzuki , Motoko Iijima
IPC分类号： C01G15/00 , C01G30/00 , C01G30/02 , H01B1/08 , H01B1/20 , B32B9/00
CPC分类号： B82Y30/00 , C01G30/02 , H01B1/08 , C01P2002/72 , C01P2002/88 , C01P2004/04 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C01P2004/82 , C01P2006/10 , C01P2006/12 , C01P2006/22 , C01P2006/40 , C01P2006/80 , Y10T428/25 , Y10T428/26 , Y10T428/261 , Y10T428/2982
摘要： An electro-conductive oxide particle comprising indium atoms, antimony atoms and oxygen atoms in a molar ratio of In:Sb:O being 1:0.02-1.25:1.55-4.63 and having a primary particle diameter of from 5 to 500 nm.
摘要翻译： In：Sb：O的摩尔比为铟原子，锑原子和氧原子的导电性氧化物粒子为1：0.02〜1.25：1.55〜4.63，初级粒径为5〜500nm。

4. 发明授权

US5756009A Process for the production of an electro-conductive oxide particle 失效
标题翻译：用于生产导电氧化物颗粒的方法
公开(公告)号：US5756009A
公开(公告)日：1998-05-26
申请号：US615957
申请日：1996-03-14
申请人： Yoshitane Watanabe , Keitaro Suzuki , Motoko Iijima
发明人： Yoshitane Watanabe , Keitaro Suzuki , Motoko Iijima
IPC分类号： C01G15/00 , C01G30/00 , C01G30/02 , H01B1/08
CPC分类号： B82Y30/00 , C01G30/02 , H01B1/08 , C01P2002/72 , C01P2002/88 , C01P2004/04 , C01P2004/32 , C01P2004/62 , C01P2004/64 , C01P2004/82 , C01P2006/10 , C01P2006/12 , C01P2006/22 , C01P2006/40 , C01P2006/80 , Y10T428/25 , Y10T428/26 , Y10T428/261 , Y10T428/2982
摘要： An electro-conductive oxide particle comprising indium atoms, antimony atoms and oxygen atoms in a molar ratio of In:Sb:O being 1:0.02-1.25:1.55-4.63 and having a primary particle diameter of from 5 to 500 nm.
摘要翻译： In：Sb：O的摩尔比为铟原子，锑原子和氧原子的导电性氧化物粒子为1：0.02〜1.25：1.55〜4.63，初级粒径为5〜500nm。

5. 发明授权

US5188667A Tungstic oxide-stannic oxide composite sol and method of preparing the same 失效
标题翻译：氧化钨 - 氧化锡复合溶胶及其制备方法
公开(公告)号：US5188667A
公开(公告)日：1993-02-23
申请号：US795678
申请日：1991-11-21
申请人： Yoshitane Watanabe , Keitaro Suzuki
发明人： Yoshitane Watanabe , Keitaro Suzuki
IPC分类号： C01B13/14 , C01G19/02 , C01G25/02 , C01G30/00 , C01G41/00 , C03C17/23 , C03C25/42 , C04B41/50 , C04B41/87 , C09D7/12 , D06M11/46 , D06M11/48 , D06P1/673 , D21H17/67 , D21H19/38 , D21H21/22 , D21H21/34 , G02B1/10
CPC分类号： B82Y30/00 , C01B13/145 , C01G19/02 , C01G25/02 , C01G30/005 , C01G41/00 , C03C17/23 , C03C25/42 , C04B41/5025 , C04B41/87 , C09D7/1216 , C09D7/1266 , D06M11/46 , D06M11/48 , D06P1/67341 , D21H17/675 , D21H19/385 , D21H21/22 , D21H21/34 , G02B1/105 , C01P2004/52 , C01P2004/64 , C01P2004/82 , C01P2006/10 , C01P2006/12 , C01P2006/22 , C01P2006/60 , C01P2006/80 , C03C2217/23 , C03C2218/113 , C08K3/22
摘要： An aqueous sol of colloidal particles of tungstic oxide (WO.sub.3)-stannic oxide (SnO.sub.2) composite having a particle size of from 2 to 7 millimicrons is prepared by blending an aqueous solution of tungstic acid and an aqueous solution of an stannate in a weight ratio of from 0.5 to 100 as WO.sub.3 /SnO.sub.2. Where the WO.sub.3 -SnO.sub.2 composite sol in an amount of from 2 to 100 parts by weight as the total of WO.sub.3 and SnO.sub.2 is blended with a sol of a 3- to 5 valent metal oxide having a particle size of from 4 to 50 millimicrons in an amount of 100 parts by weight as the metal oxide, a modified metal oxide sol of colloidal particles having a size of 4.5 to 60 millimicrons as surface-coated with the tungstic oxide (WO.sub.3)-stannic oxide (SnO.sub.5) composite colloidal particles is prepared.
摘要翻译：通过将钨酸水溶液和锡酸盐水溶液以重量比混合，制备粒径为2至7毫微米的氧化钨（WO3） - 氧化锡（SnO 3）复合物的胶体颗粒的水溶胶为0.5〜100作为WO 3 / SnO 2。其中作为WO 3和SnO 2的总量的2〜100重量份的WO 3-SnO 2复合溶胶与3〜5价的粒度为4〜50毫微子的金属氧化物的溶胶共混，作为金属氧化物的量为100重量份，制备表面涂覆有氧化钨（WO3） - 氧化锡（SnO5）复合胶体粒子的尺寸为4.5〜60毫微米的胶体粒子的改性金属氧化物溶胶。

6. 发明授权

US06296943B1 Method for producing composite sol, coating composition, and optical element 有权
标题翻译：复合溶胶，涂料组合物和光学元件的制备方法
公开(公告)号：US06296943B1
公开(公告)日：2001-10-02
申请号：US09380403
申请日：1999-09-01
申请人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama , Motoko Iijima
发明人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama , Motoko Iijima
IPC分类号： B32B904
CPC分类号： B82Y30/00 , C01G23/00 , C01G23/002 , C01G25/006 , C01P2004/64 , C01P2006/22 , C01P2006/40 , C01P2006/60 , C01P2006/64 , C01P2006/90 , C03C17/256 , C03C2217/212 , C03C2217/23 , C03C2218/113 , Y10T428/31612 , Y10T428/31663
摘要： The present invention relates to a method for producing titanium oxide (TiO2)-tin oxide (SnO2) composite sol, a titanium oxide (TiO2)-zirconium oxide (ZrO2)-tin oxide (SnO2) composite sol, and a titanium oxide (TiO2)-cerium oxide (CeO2)-tin oxide (SnO2) composite sol. Further, the present invention relates to a coating composition containing any of the above-mentioned composite sols for forming coating films that are excellent in marring resistance, surface hardness, wearing resistance, transparency, heat resistance, light-resistant, weatherability, or water resistance on optical elements such as lenses for glasses and cameras, automotive windowpane, or optical filters attached to liquid-crystal displays, plasma displays, etc. and to optical elements having a cured film of the coating composition on the surfaces.
摘要翻译：本发明涉及氧化钛（TiO 2） - 氧化锡（SnO 2）复合溶胶，氧化钛（TiO 2） - 氧化锆（ZrO 2） - 氧化锡（SnO 2）复合溶胶和氧化钛（TiO 2）的制造方法） - 氧化铈（CeO2） - 氧化锡（SnO2）复合溶胶。此外，本发明涉及一种涂料组合物，其含有上述用于形成耐损伤性，表面硬度，耐磨性，透明性，耐热性，耐光性，耐候性或耐水性优异的涂膜的上述复合溶胶在诸如用于眼镜和相机的透镜，汽车窗玻璃或附着到液晶显示器的光学滤光器，等离子体显示器等的光学元件上，以及具有表面上的涂层组合物的固化膜的光学元件。

7. 发明授权

US5891362A Hydrated zinc stannate sols, coating compositions and optical elements 失效
公开(公告)号：US5891362A
公开(公告)日：1999-04-06
申请号：US659371
申请日：1996-06-06
申请人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama , Motoko Iijima
发明人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama , Motoko Iijima
IPC分类号： C01G19/00 , G02B1/10 , C04B35/624 , C04B35/628
CPC分类号： G02B1/105 , C01G19/00 , Y10T428/2949 , Y10T428/2991
摘要： A sol having dispersed in a liquid medium particles of a hydrated zinc stannate having a primary particle diameter of from 2 to 200 nm and represented by the formula xZnO.ySnO.sub.2.zH.sub.2 O wherein the molar ratio of x:y:z is 1:0.83 to 1.43:1.00 to 5.00.

8. 发明授权

US5667725A Sol and fine powder of sodium magnesium fluoride and processes for their production 失效
标题翻译：溶胶和氟化镁的细粉末及其生产工艺
公开(公告)号：US5667725A
公开(公告)日：1997-09-16
申请号：US618816
申请日：1996-03-20
申请人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama , Motoko Iijima
发明人： Yoshitane Watanabe , Keitaro Suzuki , Yoshinari Koyama , Motoko Iijima
IPC分类号： B01J13/00 , C01F5/00 , C01F5/28 , C03C17/22 , C01B9/08
CPC分类号： B82Y30/00 , B01J13/0008 , C01F5/00 , C03C17/22 , C01P2004/64 , C03C2217/241 , C03C2217/285 , C03C2218/113 , Y10S516/928 , Y10T428/256
摘要： A sol comprising colloidal particles of sodium magnesium fluoride (NaF.MgF.sub.2) having an average particle diameter of from 10 to 100 nm.
摘要翻译：包含平均粒径为10〜100nm的氟化钠（NaF.MgF 2）的胶体粒子的溶胶。

9. 发明授权

US5472797A Optical elements having cured coating film 失效
标题翻译：具有固化涂膜的光学元件
公开(公告)号：US5472797A
公开(公告)日：1995-12-05
申请号：US86801
申请日：1993-07-07
申请人： Eiichi Yajima , Yoshitane Watanabe , Keitaro Suzuki , Tetsunori Matsukura
发明人： Eiichi Yajima , Yoshitane Watanabe , Keitaro Suzuki , Tetsunori Matsukura
IPC分类号： C08K9/02 , C08L83/04 , C09D183/04 , G02B1/10 , G02B1/115 , G02B1/14 , B32B9/00
CPC分类号： G02B1/105 , Y10T428/2991 , Y10T428/2993
摘要： An optional element having a cured coating film on optical base material wherein the cured coating film is prepared with a coating composition comprising an organosilicon compound and modified stannic oxide-zirconium oxide composite colloidal particles which are obtained by partially or fully coating the surface of stannic oxide-zirconium oxide composite colloidal particles with tungstic oxide-stannic oxide composite colloidal particles. The formed cured coating film is excellent in hot water resistance, and light-resistance and weathering resistance are not impaired even when the antireflection film made by vepor deposition of inorganic oxides is applied on the cured coating film.
摘要翻译：在光学基材上具有固化涂膜的可选元件，其中固化涂膜由包含有机硅化合物和修饰的氧化锡 - 氧化锆复合胶体颗粒的涂料组合物制备，所述胶体颗粒通过部分或全部涂覆氧化锡表面而获得氧化锆复合胶体颗粒与氧化钨 - 氧化锡复合胶体颗粒。形成的固化涂膜具有优异的耐热水性，并且即使在固化涂膜上施加由无机氧化物形成的防反射膜的情况下也不会损害耐光性和耐候性。

10. 发明授权

US5460738A Modified stannic oxide-zirconium oxide composite sol and process for preparing the same 失效
标题翻译：改性氧化锡 - 氧化锆复合溶胶及其制备方法
公开(公告)号：US5460738A
公开(公告)日：1995-10-24
申请号：US86878
申请日：1993-07-07
申请人： Yoshitane Watanabe , Keitaro Suzuki , Tetsunori Matsukura
发明人： Yoshitane Watanabe , Keitaro Suzuki , Tetsunori Matsukura
IPC分类号： B01J13/00 , C01G19/02 , C01G25/00 , C01G41/00 , G02B1/04 , G02B1/10 , G02B1/14
CPC分类号： B82Y30/00 , C01G25/00 , C01G41/006 , C01P2004/64 , C01P2004/82 , C01P2006/12 , C01P2006/22 , C01P2006/60 , C01P2006/80
摘要： A stable sol which comprises colloidal particles of modified stannic oxide-zirconium oxide composite having a particle size of from 4.5 to 60 nm, said colloidal particles consisting essentially of, as nuclei, colloidal particles of stannic oxide-zirconium oxide composite having a particle size of from 4 to 50 nm and having a structure in which colloidal particles of stannic oxide and colloidal particles of zirconium oxide are bonded to each other in a ratio, by weight of these oxides, of from 0.02 to 1.0 as ZrO.sub.2 /SnO.sub.2, and, as a coating on the surface of the nuclei, colloidal particles of tungstic oxide-stannic oxide composite having a particles size of from 2 to 7 nm and a WO.sub.3 /SnO.sub.2 weight ratio of from 0.5 to 100, and which has a total content of metal oxides of from 2 to 50 wt %.
摘要翻译：一种稳定的溶胶，其包含粒径为4.5〜60nm的改性氧化锡 - 氧化锆复合体的胶体粒子，所述胶体粒子主要由作为核的氧化锡 - 氧化锆复合体的胶体粒子组成，其粒径为 4〜50nm，其结果是氧化锡的胶态粒子和氧化锆的胶体粒子以这些氧化物的重量比例以ZrO2 / SnO2为0.02〜1.0的比例相互结合，作为核表面上的涂层，粒径为2〜7nm，WO3 / SnO2重量比为0.5〜100的钨氧化物 - 锡氧化物复合体的胶体粒子，金属氧化物的总含量为2〜50重量％。

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