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1. 发明授权

US4734479A Room temperature-curable organopolysiloxane composition 失效
标题翻译：室温可固化的有机聚硅氧烷组合物
公开(公告)号：US4734479A
公开(公告)日：1988-03-29
申请号：US27263
申请日：1987-03-18
申请人： Yoshio Inoue , Masatoshi Arai , Koji Yokoo
发明人： Yoshio Inoue , Masatoshi Arai , Koji Yokoo
IPC分类号： C08K5/00 , C08K3/00 , C08K5/05 , C08K5/5425 , C08K5/5465 , C08K5/57 , C08L1/00 , C08L23/00 , C08L27/00 , C08L83/04 , C08L83/06 , C08L83/07 , C08L101/00 , C08G77/06
CPC分类号： C08K5/5465 , C08L83/04 , C08G77/16 , C08G77/18 , C08G77/26 , Y10S528/901
摘要： The essential components in the inventive room temperature-curable organopolysiloxane composition are: (A-1) a diorganopolysiloxane of which each terminal silicon atom has a silanolic hydroxy group or two alkoxy groups; (A-2) a filler; (A-3) an alkenyloxy silane, e.g. methyl tri)isopropenyloxy)silane; (A-4) a guanidino-containing organosilicon compound, e.g. 3-(tetramethylguanidino)propyl trimethoxy silane; (A-5) an alcohol, e.g. methyl or ethyl alcohol; (B) an organosilicon compound having a silicon-bonded hydrogen atom; and (C) an organic tin compound as a catalyst. By virtue of the unique formulation above, the composition is very stable in storage in a moisture-free condition for a long period of time without losing the high curability when exposed to a moisture-containing atmosphere.
摘要翻译：本发明的室温可固化的有机基聚硅氧烷组合物中的主要成分是：（A-1）每个末端硅原子具有硅烷醇羟基或两个烷氧基的二有机聚硅氧烷; （A-2）填料; （A-3）烯氧基硅烷，例如甲基三）异丙烯氧基）硅烷; （A-4）含胍基的有机硅化合物，例如 3-（四甲基胍基）丙基三甲氧基硅烷; （A-5）醇，例如甲基或乙醇; （B）具有硅键合氢原子的有机硅化合物; 和（C）有机锡化合物作为催化剂。由于上述独特的配方，组合物在无水条件下长期储存时非常稳定，而在暴露于含湿气氛时不会损失高固化性。

2. 发明授权

US4721765A Room temperature-curable organopolysiloxane composition 失效
标题翻译：室温可固化的有机聚硅氧烷组合物
公开(公告)号：US4721765A
公开(公告)日：1988-01-26
申请号：US30693
申请日：1987-03-25
申请人： Yoshio Inoue , Masatoshi Arai , Koji Yokoo
发明人： Yoshio Inoue , Masatoshi Arai , Koji Yokoo
IPC分类号： C08K5/00 , C08K5/05 , C08K5/5419 , C08K5/5425 , C08K5/544 , C08K5/5465 , C08K5/57 , C08L1/00 , C08L23/00 , C08L27/00 , C08L83/04 , C08L83/06 , C08L101/00 , C08G77/06
CPC分类号： C08K5/5465 , C08L83/04 , C08G77/16 , C08G77/18 , C08G77/26
摘要： The invention provides a room temperature-curable organopolysiloxane composition curable into a rubbery elastomer, which has excellent storage stability under a moisture-free condition without losing high curability. The composition comprises, in addition to the conventional essential ingredients of a hydroxy- or alkoxy-terminated diorganopolysiloxane, filler, triisopropenyloxy silane compound as a crosslinking agent and a guanidino-containing organosilicon compound as a curing aid, an amino-containing silane compound such as MeSi[NH--C.sub.3 H.sub.6 --Si(OEt).sub.3 ].sub.3 and MeSi[NH--C.sub.2 H.sub.4 NHC.sub.3 H.sub.6 --Si(OMe).sub.3 ].sub.3.
摘要翻译：本发明提供可固化到橡胶弹性体中的室温可固化的有机基聚硅氧烷组合物，其在无湿度条件下具有优异的储存稳定性，而不损失高固化性。除了作为交联剂的填充剂，作为交联剂的三异丙烯基氧基硅烷化合物和作为固化助剂的含胍基的有机硅化合物的常规必需成分之外，还包含含氨基的硅烷化合物，例如 MeSi [NH-C3H6-Si（OEt）3] 3和MeSi [NH-C2H4NHC3H6-Si（OMe）3] 3。

3. 发明授权

US4695617A Room temperature-curable organopolysiloxane composition 失效
标题翻译：室温可固化的有机聚硅氧烷组合物
公开(公告)号：US4695617A
公开(公告)日：1987-09-22
申请号：US837588
申请日：1986-03-07
申请人： Yoshio Inoue , Masatoshi Arai , Shinichi Sato , Koji Yokoo
发明人： Yoshio Inoue , Masatoshi Arai , Shinichi Sato , Koji Yokoo
IPC分类号： C08L83/00 , C08K5/5425 , C08K5/5465 , C08L83/04 , C08L83/06 , H01B3/46 , C08G77/20
CPC分类号： C08K5/5465 , C08K5/54 , C08G77/14 , C08G77/16 , C08G77/20 , C08G77/26 , Y10S528/901
摘要： The room temperature-curable organopolysiloxane composition of the invention capable of giving a cured rubber can be used advantageously as an insulating material in electric and electronic instruments without causing troubles in contact points which is unavoidable with conventional compositions. The inventive composition is formulated with (a) a diorganopolysiloxane terminated at the molecule molecular chain ends each with a silanolic hydroxy group, (b) an alkenyloxy, e.g. isopropenyloxy, containing silane and (c) a guanidino-substituted organosilicon compound and these components are specified either by the upper limit of the content of low molecular constituents having a specified vapor pressure or higher or the upper limit of the vapor pressure of the compound per se so that the electric contact points near the insulation with the composition are free from exposure to the vapor of organosilicon compounds which may be deposited as an oxide of silicon by sparks.
摘要翻译：能够提供固化橡胶的本发明的室温可固化的有机基聚硅氧烷组合物可以有利地用作电气和电子仪器中的绝缘材料，而不会在常规组合物中不可避免地引起接触点的麻烦。本发明的组合物配制成（a）在分子分子链处终止的二有机聚硅氧烷，每个末端具有硅烷醇羟基，（b）链烯氧基，例如，含有硅烷的异丙烯氧基和（c）胍基取代的有机硅化合物，并且这些组分由具有特定蒸气压或更高的低分子量成分的含量的上限或化合物的蒸气压的上限规定使得与组合物绝缘附近的电接触点不会暴露于有机硅化合物的蒸气中，有机硅化合物可以通过火花作为硅的氧化物沉积。

4. 发明授权

US4721766A Room temperature-curable organopolysiloxane composition 失效
标题翻译：室温可固化的有机聚硅氧烷组合物
公开(公告)号：US4721766A
公开(公告)日：1988-01-26
申请号：US894857
申请日：1986-08-08
申请人： Yoshio Inoue , Masatoshi Arai , Koji Yokoo
发明人： Yoshio Inoue , Masatoshi Arai , Koji Yokoo
IPC分类号： C08L83/00 , C08K5/5419 , C08K5/5425 , C08K5/5465 , C08L1/00 , C08L23/00 , C08L27/00 , C08L83/04 , C08L83/06 , C08L101/00 , C08G77/06
CPC分类号： C08K5/5465 , C08L83/04 , C08G77/16 , C08G77/18 , Y10S528/901
摘要： The room temperature-curable organopolysiloxane composition of the invention is imparted with greatly improved stability in prolonged storage without being affected in respect of the curability. The composition is formulated, in addition to the base ingredients of a silanol- or alkoxy-terminated diorganopolysiloxane and a filler, with an alkenyloxy-containing silane compound in an amount of at least equimolar to the silanol groups and water in the base ingredients and a guanidino-containing organosilane compound in a limited amount.
摘要翻译：本发明的室温可固化的有机基聚硅氧烷组合物在长期保存中赋予了极大的改进的稳定性，而不会影响固化性。除了硅烷醇或烷氧基封端的二有机聚硅氧烷和填料的基础成分之外，配合含有至少等摩尔量的含烯氧基的硅烷化合物与基础成分中的硅烷醇基和水，以及含胍基的有机硅烷化合物。

5. 发明授权

US5039735A Room temperature vulcanizable organopolysiloxane composition for masking electric or electronic parts 失效
标题翻译：室温可硫化的有机聚硅氧烷组合物，用于掩蔽电气或电子部件
公开(公告)号：US5039735A
公开(公告)日：1991-08-13
申请号：US351303
申请日：1989-05-09
申请人： Masatoshi Arai , Koji Yokoo , Yoshifumi Kurihara
发明人： Masatoshi Arai , Koji Yokoo , Yoshifumi Kurihara
IPC分类号： C08L83/06 , C08K5/20 , C08K5/5425 , C08K5/5465 , C08K13/02 , C08L83/04 , C08L101/02 , C09D5/20 , H05K3/28 , H05K3/34
CPC分类号： C08K5/5465 , C08K5/20 , C08K5/5425 , C08L83/04 , C08G77/16 , C08G77/18 , C08G77/20 , Y10S528/901
摘要： A room temperature vulcanizable organopolysiloxane composition comprising a diorganopolysiloxane blocked with a hydroxyl group at opposite ends of the molecular chain of the diorganopolysiloxane, a silane or siloxane compound having at least three hydrolyzable groups in the molecule, a filler, and a curing catalyst. The composition further comprises a specific type of amide compound whereby the composition is readily released from electric or electronic parts after having been vulcanized and dipped in a hot soldering bath.
摘要翻译：一种室温可硫化的有机聚硅氧烷组合物，其包含在二有机聚硅氧烷的分子链的相对端用羟基封端的二有机聚硅氧烷，在分子中具有至少三个可水解基团的硅烷或硅氧烷化合物，填料和固化催化剂。组合物还包含特定类型的酰胺化合物，由此组合物在硫化并浸渍在热焊浴中后容易从电子或电子部件释放。

6. 发明授权

US4629775A Room temperature-curable organopolysiloxane composition 失效
标题翻译：室温可固化的有机聚硅氧烷组合物
公开(公告)号：US4629775A
公开(公告)日：1986-12-16
申请号：US758164
申请日：1985-07-23
申请人： Masatoshi Arai , Takeo Inoue , Koji Yokoo
发明人： Masatoshi Arai , Takeo Inoue , Koji Yokoo
IPC分类号： C08L83/00 , C07F7/18 , C08K5/00 , C08K5/548 , C08L83/04 , C08L83/06 , C08G77/06
CPC分类号： C08K5/0091 , C07F7/1836 , C07F7/184 , C08L83/04 , C08G77/16
摘要： The room temperature-curable organopolysiloxane composition of the invention can be cured into a rubbery elastomer which exhibits strong adhesion to the surface of a substrate made of, for example, a plastic resin even without the use of a primer or other adhesion aid. The composition comprises, in addition to the conventional ingredients of a silanolic hydroxy-terminated diorganopolysiloxane and alkoxy-containing organosilicon compound, a special organosilicon compound having, in a molecule, at least one group of the formula(R.sup.1 O).sub.3-n (Me).sub.n Si--C.sub.3 H.sub.6 --S--CO--NH--,in which Me is a methyl group, R.sup.1 is a methyl or an ethyl group and n is zero or 1, and a titanium chelate compound represented by the general formula ##STR1## in which Q is a divalent organosilicon-containing group, R.sup.2 is an alkyl group having 1 to 3 carbon atoms and R.sup.3 is the same as R.sup.2 or R.sup.2 O.
摘要翻译：本发明的室温可固化的有机基聚硅氧烷组合物可以固化成即使不使用底漆或其它粘合助剂也能显示出对由例如塑料树脂制成的基材表面的强粘合性的橡胶状弹性体。除了硅烷醇羟基封端的二有机聚硅氧烷和含烷氧基的有机硅化合物的常规成分之外，组合物还包含在分子中具有至少一个式（R 1）3-n（Me）的基团的特殊有机硅化合物， nSi-C 3 H 6 -S-CO-NH-，其中Me是甲基，R 1是甲基或乙基，n是0或1，和由通式“IMAGE”表示的钛螯合物，其中Q 是含二价含有机硅基团，R 2为碳原子数为1〜3的烷基，R 3为与R 2或R 2 O相同的基团。

7. 发明授权

US4987155A Foamable organopolysiloxane composition 失效
标题翻译：可发泡有机聚硅氧烷组合物
公开(公告)号：US4987155A
公开(公告)日：1991-01-22
申请号：US557824
申请日：1990-07-26
申请人： Yoshio Inoue , Masatoshi Arai , Tsuneo Kimura
发明人： Yoshio Inoue , Masatoshi Arai , Tsuneo Kimura
IPC分类号： C08J9/02 , C08L83/04
CPC分类号： C08J9/02 , C08L83/04 , C08G77/045 , C08G77/12 , C08G77/16 , C08G77/62 , C08J2383/04
摘要： The invention provides a foamable organopolysiloxane composition capable of giving, by foaming and curing at room temperature, a silicone rubber foam of high foaming expansion having very uniform and dense cellular structure. The composition is prepared by a process comprising the steps of: (A) compounding an .alpha.,.omega.-dihydroxy dimethylpolysiloxane with a reinforcing silica filler, hexamethyl disilazane and water as the hydrolysis agent of the silazane to give a compound; (B) removing ammonia in the compound formed by the hydrolysis of the silazane compound as completely as possible; and (C) compounding the compound with a polyhydroxy methylpolysiloxane, an organohydrogenpolysiloxane and a platinum compound as a catalyst for the dehydrogenation reaction between the silanolic hydroxy groups and the silicon-bonded hydrogen atoms to produce hydrogen as the foaming gas.
摘要翻译：本发明提供一种可发泡的有机聚硅氧烷组合物，其能够通过在室温下发泡和固化得到具有非常均匀且致密的细胞结构的高发泡膨胀的硅橡胶泡沫。通过包括以下步骤的方法制备组合物：（A）将α，ω-二羟基二甲基聚硅氧烷与增强二氧化硅填料，六甲基二硅氮烷和水混合，作为硅氮烷的水解试剂，得到化合物; （B）通过尽可能完全地水解硅氮烷化合物形成的化合物中除去氨; 和（C）将化合物与多羟基甲基聚硅氧烷，有机氢聚硅氧烷和铂化合物混合，作为硅烷醇羟基与硅键合的氢原子之间的脱氢反应的催化剂，以产生氢作为发泡气体。

8. 发明授权

US5357023A Organopolysiloxanes having silethylene linkages and a curable composition comprising the same 失效
标题翻译：具有亚乙烯基键的有机聚硅氧烷和包含它们的可固化组合物
公开(公告)号：US5357023A
公开(公告)日：1994-10-18
申请号：US83387
申请日：1993-06-29
申请人： Yoshio Inoue , Masatoshi Arai , Kazutoshi Fujioka , Tsuneo Kimura
发明人： Yoshio Inoue , Masatoshi Arai , Kazutoshi Fujioka , Tsuneo Kimura
IPC分类号： C08G77/50 , C08L83/14 , C08G77/20
CPC分类号： C08L83/14 , C08G77/50
摘要： A novel organopolysiloxane compound having, in a molecule, at least one silyl-substituted ethyl group of the general formula ##STR1## in which R.sup.1 is a hydrogen atom or a methyl group, R is a monovalent hydrocarbon group and the subscripts a is 2 or and b is 1, 2 or 3, or a linear organopolysiloxane having, at each molecular chain end, at least one of such a group, can be prepared by first reacting a vinyl-containing organopolysiloxane with a hydrogen chlorosilane compound to effect the hydrosilation reaction between the silicon-bonded vinyl groups and the silicon-bonded hydrogen atoms and then the silicon-bonded chlorine atoms are subjected to a dehydrochlorination reaction with a silanol compound of the general formula ##STR2## A composition comprising the organopolysiloxane and a photopolymerization initiator is highly sensitive to light and readily cured into a rubbery elastomer by irradiation with ultraviolet light.
摘要翻译：一种新的有机聚硅氧烷化合物，其在分子中具有至少一个通式为“IMAGE”的甲硅烷基取代的乙基，其中R 1为氢原子或甲基，R为单价烃基，下标a为2或并且b为1,2或3，或者在各分子链末端具有这种基团中的至少一个的线性有机聚硅氧烷可以通过首先使含乙烯基的有机聚硅氧烷与氢氯硅烷化合物反应来进行氢化硅烷化反应硅键合的乙烯基和与硅键合的氢原子之间，然后与硅键合的氯原子与通式为的硅烷醇化合物进行脱氯化氢反应。包含有机聚硅氧烷和光聚合引发剂的组合物是高度的对光敏感，并通过紫外线照射容易地固化成橡胶状弹性体。

9. 发明授权

US5244938A Room temperature curable organopolysiloxane composition 失效
标题翻译：室温可固化有机硅氧烷组合物
公开(公告)号：US5244938A
公开(公告)日：1993-09-14
申请号：US806342
申请日：1991-12-13
申请人： Masatoshi Arai , Yoshifumi Inoue , Yoshio Inoue
发明人： Masatoshi Arai , Yoshifumi Inoue , Yoshio Inoue
IPC分类号： C08K3/00 , C08K5/5419 , C08K5/57 , C08L83/04 , C08L83/06 , C08L83/08
CPC分类号： C08K5/5419 , C08L83/04 , C08L83/08 , C08G77/16 , C08G77/18 , C08G77/24 , Y10S528/901
摘要： The present invention is characterized by adding and mixing an organosilicon compound having alkoxy, groups and an ester linkage in the molecule represented by the following formula: ##STR1## in an amount of 1 to 20 parts by weight per 100 parts by weight of a trifluoropropylalkylpolysiloxane. Said organosilicon compound has a function as a storage stabilizer as well as a curing agent and, according to the present invention, an RTV fluorosilicone composition that has hitherto been difficult to be applied as an adhesive for electric and electronic parts has been made possible to be used in the particular field.

10. 发明授权

US4695603A Room temperature curable silicone rubber composition 失效
标题翻译：室温可固化硅橡胶组合物
公开(公告)号：US4695603A
公开(公告)日：1987-09-22
申请号：US739421
申请日：1985-05-30
申请人： Yoshio Inoue , Masatoshi Arai , Takeo Inoue
发明人： Yoshio Inoue , Masatoshi Arai , Takeo Inoue
IPC分类号： C09K3/10 , C08K3/00 , C08K5/00 , C08K5/54 , C08K5/5455 , C08K5/549 , C08L83/00 , C08L83/04 , C08L83/06 , C08L83/08
CPC分类号： C08K5/0008 , C08K5/5455
摘要： The room temperature curable silicone rubber composition of the invention is outstandingly free from the problem of surface stain when a cured elastomer thereof used, for example, in building works is prolongedly exposed to the atmosphere with very durable stain-preventing effect by the formulation of a surface active agent having at least one fluorine atom in a molecule and a specific organosilicon compound of the formula R.sup.1 --CO--NR.sup.2 --CH.sub.2).sub.b SiR.sup.3.sub.a O.sub.(3-a)/2, in which R.sup.1 and R.sup.2 are each a hydrogen atom or a monovalent hydrocarbon group, R.sup.3 is a hydrogen atom, or monovalent hydrocarbon group, a is 0-3 and b is a positive integer not larger than 10, in addition to the usual components of conventional room temperature curable silicone rubber compositions.
摘要翻译：当本发明的室温可固化硅橡胶组合物在其用于例如建筑工程中的固化弹性体长期暴露于大气中时，其表面污渍的问题显着地不会受到非常耐用的防污染作用，分子中具有至少一个氟原子的表面活性剂和式R 1 -CO-NR 2 -CH 2）b SiR 3 a O（3-a）/ 2的特定有机硅化合物，其中R 1和R 2各自为氢原子或一价烃基，R3为氢原子或一价烃基，a为0-3，b为不大于10的正整数，除常规的室温可固化硅橡胶组合物的组分外。

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