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1. 发明授权

US07858667B2 Alcohol synthesis from CO or CO2 有权
标题翻译：来自CO或CO 2的酒精合成
公开(公告)号：US07858667B2
公开(公告)日：2010-12-28
申请号：US11611160
申请日：2006-12-15
申请人： Jianli Hu , Robert A. Dagle , Jamelyn D. Holladay , Chunshe Cao , Yong Wang , James F. White , Douglas C. Elliott , Don J. Stevens
发明人： Jianli Hu , Robert A. Dagle , Jamelyn D. Holladay , Chunshe Cao , Yong Wang , James F. White , Douglas C. Elliott , Don J. Stevens
IPC分类号： C07C27/00
CPC分类号： C07C29/152 , B01J19/0093 , B01J2219/00835 , B01J2219/00873 , B01J2219/00961 , B01J2219/00984 , C07C29/157 , Y02P20/52 , C07C31/04 , C07C31/08 , C07C31/02
摘要： Methods for producing alcohols from CO or CO2 and H2 utilizing a palladium-zinc on alumina catalyst are described. Methods of synthesizing alcohols over various catalysts in microchannels are also described. Ethanol, higher alcohols, and other C2+ oxygenates can produced utilizing Rh—Mn or a Fisher-Tropsch catalyst.
摘要翻译：描述了使用氧化铝催化剂上的钯 - 锌从CO或CO 2和H 2生产醇的方法。还描述了在微通道中在各种催化剂上合成醇的方法。可以使用Rh-Mn或Fisher-Tropsch催化剂生产乙醇，高级醇和其他C2 +含氧化合物。

2. 发明授权

US07708955B2 Staged alkylation in microchannels 有权
标题翻译：微通道分阶段烷基化
公开(公告)号：US07708955B2
公开(公告)日：2010-05-04
申请号：US11973447
申请日：2007-10-09
申请人： Yong Wang , James F. White
发明人： Yong Wang , James F. White
IPC分类号： B01J8/04 , B01J10/00
CPC分类号： C10G29/205 , B01J19/0093 , B01J2219/00835 , B01J2219/00844 , B01J2219/00873 , B01J2219/00894 , C10G2300/1081 , C10G2300/1088 , C10G2300/1096 , C10G2300/4081 , C10G2400/02
摘要： The invention provides methods and systems for alkylating a paraffinic feed stream in a microchannel utilizing the staged addition of olefin.
摘要翻译：本发明提供了利用分阶段加入烯烃在微通道中烷基化进入石蜡原料流的方法和系统。

3. 发明申请

US20080017291A1 Structured inorganic materials and method for making and using same 审中-公开
标题翻译：结构化无机材料及其制造和使用方法
公开(公告)号：US20080017291A1
公开(公告)日：2008-01-24
申请号：US11488351
申请日：2006-07-18
申请人： Yongsoon Shin , James F. White , Gregory J. Exarhos , Yong Wang
发明人： Yongsoon Shin , James F. White , Gregory J. Exarhos , Yong Wang
IPC分类号： B31B1/60
CPC分类号： C04B38/0032 , B01J27/22 , B01J27/224 , B01J35/002 , B01J37/0018 , B01J37/08 , C04B35/46 , C04B35/5603 , C04B35/5611 , C04B35/5622 , C04B35/573 , C04B35/62209 , C04B2111/0081 , C04B2235/3232 , C04B2235/3239 , C04B2235/3244 , C04B2235/3251 , C04B2235/3256 , C04B2235/3418 , C04B2235/449 , C04B2235/48 , C04B2235/483 , C04B2235/5409 , C04B2235/6028 , C04B2235/656 , C04B2235/6562 , C04B2235/761 , C04B2235/762 , C04B2235/80 , C04B35/565 , C04B38/0067
摘要： The invention relates generally to hierarchical inorganic materials and a method for making and using same. The materials of the invention have a controlled hardness, porosity, and surface area ideally suited for use as, e.g., durable catalyst supports for reactions conducted in severe and/or hydrothermal environments. The materials of the invention are prepared by infusing hierarchical templates of suitably shaped sized cellulosic or lignocellulosic particles (e.g., from wood, bamboo, and the like) with soluble transition-metal and/or ceramic precursors. Infused templates are heated in a gaseous atmosphere until volatile chemical components are removed. After drying, the infused templates are heated under flowing argon, helium, or air atmosphere for several hours to remove volatiles and convert all or part of the transition-metal and/or ceramic precursors to respective carbide, oxycarbide, or other chemical forms.
摘要翻译：本发明一般涉及层状无机材料及其制造和使用方法。本发明的材料具有受控的硬度，孔隙率和表面积，理想地适用于例如用于在严重和/或水热环境中进行反应的耐久性催化剂载体。本发明的材料通过将合适尺寸的纤维素或木质纤维素颗粒（例如，来自木材，竹子等）与可溶性过渡金属和/或陶瓷前体进行分层模板的注入而制备。将注入的模板在气态气氛中加热直至除去挥发性化学成分。干燥后，将输入的模板在流动的氩气，氦气或空气气氛下加热数小时以除去挥发物并将全部或部分过渡金属和/或陶瓷前体转化为相应的碳化物，碳氧化物或其它化学形式。

4. 发明申请

US20080152555A1 Staged alkylation in microchannels 有权
标题翻译：微通道分阶段烷基化
公开(公告)号：US20080152555A1
公开(公告)日：2008-06-26
申请号：US11973447
申请日：2007-10-09
申请人： Yong Wang , James F. White
发明人： Yong Wang , James F. White
IPC分类号： B01J8/04
CPC分类号： C10G29/205 , B01J19/0093 , B01J2219/00835 , B01J2219/00844 , B01J2219/00873 , B01J2219/00894 , C10G2300/1081 , C10G2300/1088 , C10G2300/1096 , C10G2300/4081 , C10G2400/02
摘要： The invention provides methods and systems for alkylating a paraffinic feed stream in a microchannel utilizing the staged addition of olefin.
摘要翻译：本发明提供了利用分阶段加入烯烃在微通道中烷基化链烷烃进料流的方法和系统。

5. 发明授权

US07304198B2 Staged alkylation in microchannels 有权
标题翻译：微通道分阶段烷基化
公开(公告)号：US07304198B2
公开(公告)日：2007-12-04
申请号：US10846830
申请日：2004-05-14
申请人： Yong Wang , James F. White
发明人： Yong Wang , James F. White
IPC分类号： C07C2/58
CPC分类号： C10G29/205 , B01J19/0093 , B01J2219/00835 , B01J2219/00844 , B01J2219/00873 , B01J2219/00894 , C10G2300/1081 , C10G2300/1088 , C10G2300/1096 , C10G2300/4081 , C10G2400/02
摘要： The invention provides methods and systems for alkylating a paraffinic feed stream in a microchannel utilizing the staged addition of olefin.
摘要翻译：本发明提供了利用分阶段加入烯烃在微通道中烷基化进入石蜡原料流的方法和系统。

6. 发明授权

US09260403B2 Methods for preparing 2,5-furandicarboxylic acid 有权
标题翻译：制备2,5-呋喃二羧酸的方法
公开(公告)号：US09260403B2
公开(公告)日：2016-02-16
申请号：US14229388
申请日：2014-03-28
申请人： Yasuo Yoshikuni , Susan R. Cooper , Adam J. Wargacki , Leo E. Manzer , James F. White , Lou Kapicak , Dennis J. Miller , Lars Peereboom
发明人： Yasuo Yoshikuni , Susan R. Cooper , Adam J. Wargacki , Leo E. Manzer , James F. White , Lou Kapicak , Dennis J. Miller , Lars Peereboom
IPC分类号： C07D307/68
CPC分类号： C07D307/68
摘要： Provided are methods of producing 2,5-furandicarboxylic acid (FDCA) from renewable sources such as seaweed, alginate, oligoalginate, pectin, oligopectin, polygalacturonate, galacturonate, and/or oligogalacturonate. The sugars in the renewable sources can be converted into one or more intermediates such as 4-deoxy-L-erythro-5-hexoseulose uronate (DEHU), 4-deoxy-L-threo-5-hexosulose uronate (DTHU), 5-hydroxymethyl furfural (HMF), 2,5-dihydroxymethyl furan (DHMF), and 5-formyl-2-furancarboxylic acid (FFA), which can be converted into FDCA by dehydration and cyclization to produce 5-formyl-2-furancarboxylic acid (FFA), followed by oxidation to produce FDCA. DEHU or DTHU may also be converted into FDCA by oxidation to produce 2,3-dihydroxy-5-oxohexanedioic acid (DOHA), which then undergoes dehydration and cyclization to produce FDCA.
摘要翻译：提供从可再生来源例如海藻，藻酸盐，低聚海藻酸盐，果胶，寡聚糖蛋白，聚半乳糖醛酸盐，半乳糖醛酸盐和/或寡聚半乳糖醛酸盐生产2,5-呋喃二羧酸（FDCA）的方法。可再生资源中的糖可以转化为一种或多种中间体，例如4-脱氧-L-赤式5-己糖糖酸糖（DEHU），4-脱氧-L-苏糖-5-己糖糖酸糖（DTHU），5- 羟基甲基糠醛（HMF），2,5-二羟甲基呋喃（DHMF）和5-甲酰基-2-呋喃甲酸（FFA），其可以通过脱水和环化转化成FDCA以产生5-甲酰基-2-呋喃甲酸（ FFA），然后氧化生成FDCA。 DEHU或DTHU也可以通过氧化转化成FDCA，生成2,3-二羟基-5-氧代己二酸（DOHA），然后进行脱水和环化以产生FDCA。

7. 发明授权

US07872158B2 Chemical production processes, systems, and catalyst compositions 有权
标题翻译：化学生产过程，系统和催化剂组合物
公开(公告)号：US07872158B2
公开(公告)日：2011-01-18
申请号：US11895414
申请日：2007-08-24
申请人： Thomas H. Peterson , Alan H. Zacher , Michel J. Gray , James F. White , Todd A. Werpy
发明人： Thomas H. Peterson , Alan H. Zacher , Michel J. Gray , James F. White , Todd A. Werpy
IPC分类号： C07C45/51 , C07C45/52
CPC分类号： B01J27/186 , B01J8/025 , B01J23/96 , B01J27/1856 , B01J27/285 , B01J37/03 , B01J38/12 , B01J2208/00212 , B01J2208/00256 , B01J2219/00247 , C07C45/52 , Y02P20/584 , C07C47/22 , C07C49/17
摘要： Chemical production processes are provided that can include exposing a reactant composition to a catalyst composition to form a product composition. The reactant composition can include a multihydric alcohol compound and the product composition can include a carbonyl compound. The catalyst composition can include a metal effective to facilitate catalyst activation. Processes disclosed also include supplementing a dehydration catalyst with a promoter, and activating the supplemented catalyst in the presence of oxygen. Processes also include providing a supplemented dehydration catalyst to within a reactor, and exposing a multihydric alcohol compound to the dehydration catalyst, with the exposing forming coke within the reactor. Oxygen can be provided to the reactor to remove at least a portion of the coke.
摘要翻译：提供化学生产方法，其可以包括将反应物组合物暴露于催化剂组合物以形成产物组合物。反应物组合物可以包括多元醇化合物，并且产物组合物可以包括羰基化合物。催化剂组合物可以包括有效促进催化剂活化的金属。所公开的方法还包括用助催化剂补充脱水催化剂，并在氧的存在下活化补充的催化剂。方法还包括向反应器内部提供补充的脱水催化剂，并将多元醇化合物暴露于脱水催化剂中，同时在反应器内形成曝光的焦炭。可以将氧气提供给反应器以除去至少一部分焦炭。

8. 发明申请

US20100256187A1 COMPOSITION OF 2,4,6- TRIFLUORO-N-[6-(1-METHYL-PIPERIDIN-4-CARBONYL)-PYRIDIN-2-YL]-BENZAMIDE 审中-公开
标题翻译： 2,4,6-三氟-N- [6-（1-甲基 - 哌啶-4-羰基） - 吡啶-2-基] - 苯甲酰胺的组合物
公开(公告)号：US20100256187A1
公开(公告)日：2010-10-07
申请号：US12753489
申请日：2010-04-02
申请人： Alison Pilgrim , James F. White , Nadia M.J. Rupniak
发明人： Alison Pilgrim , James F. White , Nadia M.J. Rupniak
IPC分类号： A61K31/4545 , A61P25/06
CPC分类号： A61K31/4545
摘要： The present invention relates to discloses a pharmaceutical composition of 2,4,6-trifluoro-N-[6-(1-methyl-piperidin-4-ylcarbonyl)-pyridin-2-yl]-benzamide and a pharmaceutically acceptable carrier.
摘要翻译：本发明涉及2,4,6-三氟-N- [6-（1-甲基 - 哌啶-4-基羰基） - 吡啶-2-基] - 苯甲酰胺和药学上可接受的载体的药物组合物。

9. 发明授权

US07700788B2 Hydroxymethyl furfural oxidation methods 有权
标题翻译：羟甲基糠醛氧化法
公开(公告)号：US07700788B2
公开(公告)日：2010-04-20
申请号：US11932436
申请日：2007-10-31
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/44
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中将包含HMF的原料提供到反应器中。将空气和O2中的至少一个提供到反应器中。起始材料与包含Pt的催化剂在载体材料上接触，其中接触在约50℃至约200℃的反应器温度下进行。制备其中提供ZrO 2并被煅烧的氧化催化剂的方法。将ZrO 2与乙酰丙酮化铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2的流量下钝化。

10. 发明授权

US07674916B2 Process for producing cyclic compounds 有权
标题翻译：环状化合物的制备方法
公开(公告)号：US07674916B2
公开(公告)日：2010-03-09
申请号：US11688022
申请日：2007-03-19
申请人： Todd A. Werpy , John G. Frey, Jr. , James F. White , Johnathan E. Holladay , Alan H. Zacher
发明人： Todd A. Werpy , John G. Frey, Jr. , James F. White , Johnathan E. Holladay , Alan H. Zacher
IPC分类号： C07D207/267 , C07D213/63
CPC分类号： C07D207/404
摘要： The invention includes methods of processing an initial di-carbonyl compound by conversion to a cyclic compound. The cyclic compound is reacted with an alkylating agent to form a derivative having an alkylated ring nitrogen. The invention encompasses a method of producing an N-alkyl product. Ammonia content of a solution is adjusted to produce a ratio of ammonia to di-carboxylate compound of from about 1:1 to about 1.5:1. An alkylating agent is added and the initial compound is alkylated and cyclized. The invention includes methods of making N-methyl pyrrolidinone (NMP). Aqueous ammonia and succinate is introduced into a vessel and ammonia is adjusted to provide a ratio of ammonia to succinate of less than 2:1. A methylating agent is reacted with succinate at a temperature of from greater than 100° C. to about 400° C. to produce N-methyl succinimide which is purified and hydrogenated to form NMP.
摘要翻译：本发明包括通过转化为环状化合物来处理初始二羰基化合物的方法。环状化合物与烷基化剂反应形成具有烷基化环氮的衍生物。本发明包括生产N-烷基产物的方法。调节溶液的氨含量以产生约1：1至约1.5：1的氨与二羧酸酯化合物的比例。加入烷基化剂并将该初始化合物烷基化并环化。本发明包括制备N-甲基吡咯烷酮（NMP）的方法。将氨水和琥珀酸钠引入容器中，并调节氨以提供小于2:1的氨与琥珀酸的比例。甲基化剂与琥珀酸酯在大于100℃至约400℃的温度下反应，生成N-甲基琥珀酰亚胺，将其纯化并氢化形成NMP。

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