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    • 1. 发明授权
    • Process for preparing methyl tertiary-butyl ether
    • 制备甲基叔丁基醚的方法
    • US4404409A
    • 1983-09-13
    • US125655
    • 1980-02-28
    • Yasuo FujiwaraTetsuya Takezono
    • Yasuo FujiwaraTetsuya Takezono
    • C07C43/04B01J31/00C07B61/00C07C41/06C07C41/00
    • C07C41/06
    • A process for continuously preparing methyl tertiary-butyl ether with high yield involves reacting an isobutylene-containing/hydrocarbon and methanol by continuously passing the isobutylene and methanol, in a molar ratio of isobutylene to methanol of 1 to 0.6-1.4 at a temperature of 60.degree.-100.degree. C. at a liquid space velocity of 0.1-50 l/hour and at a pressure of 1-50 atmospheres, through a first reactor filled with strong acid type cation exchange resin particles having an average particle diameter of 0.2-10 mm; dividing the mixture of the reaction products in two streams, the flow rate of the first stream being 3-15 times the flow rate of the second stream; recycling the first stream to the first reactor; passing the second stream, at a temperature of 20.degree.-55.degree. C. at a liquid space velocity of 0.1-50 l/hour and at a pressure of 1-50 atmospheres, through a second reactor filled with strong acid type cation exchange resin particles having an average particle diameter of 0.2-10 mm; passing the stream from the second reactor through a fixed bed filled with a water-insoluble solid particulate acid neutralizing agent having an average particle diameter of 0.1-10 mm at a temperature of about 0.degree.-55.degree. C.; passing the resulting reaction mixture into a flashing tower whereby the unreacted hydrocarbon is removed; and recovering a mixture containing MTBE from the bottom of the flashing tower.
    • 以高产率连续制备甲基叔丁基醚的方法包括使异丁烯/烃和甲醇通过连续使异丁烯和甲醇以异丁烯与甲醇的摩尔比在1至0.6-1.4的温度下反应,温度为60℃ 以0.1-50升/小时的液体空间速度和1-50大气压的压力,通过填充有强酸型阳离子交换树脂颗粒的平均粒径为0.2-10的第一反应器 毫米 将反应产物的混合物分成两股,第一流的流量为第二料流的流量的3-15倍; 将第一流回收到第一反应器; 在20〜-5℃的温度下以0.1-50升/小时的液体空间速度和1-50大气压的压力,通过填充有强酸型阳离子交换树脂的第二反应器 平均粒径为0.2-10mm的颗粒; 使来自第二反应器的物流在约0-55℃的温度下通过填充有平均粒径为0.1-10mm的水不溶性固体颗粒酸中和剂的固定床; 将所得反应混合物通入闪蒸塔,除去未反应的烃; 并从闪光塔的底部回收含有MTBE的混合物。
    • 9. 发明授权
    • Developer container, process cartridge, developer sealing member and
sealing method
    • 显影剂容器,处理盒,显影剂密封件和密封方法
    • US6097907A
    • 2000-08-01
    • US939678
    • 1997-09-29
    • Yasuo Fujiwara
    • Yasuo Fujiwara
    • G03G15/08B65D83/06C09J7/02C09J201/00G09F3/04
    • G03G15/0894G03G15/0882G03G15/0884G03G2215/00987G03G2221/183
    • A developer container having an opening for discharging a developer contained therein and a sealing surface portion surrounding the opening, is sealed with a sealing member having a sealant layer and applied onto the sealing surface portion of the developer container with the sealant layer. The sealant layer contains a dispersed material therein and the sealing surface portion of the developer container contains a dispersed material, which is mutually soluble with the dispersed material in the sealant layer. The dispersed material in the sealant layer preferably includes a thermoplastic elastomer. The resultant sealed developer container may be provided with a sound seal structure even at a relatively low sealing pressure causing a smaller sealing surface depression of the developer container, which allows re-sealing of the container.
    • 具有用于排出其中包含的显影剂的开口的开口容器和围绕开口的密封表面部分用具有密封剂层的密封构件密封并且用密封剂层施加到显影剂容器的密封表面部分上。 密封剂层包含分散的材料,显影剂容器的密封表面部分含有与分散材料在密封层中相互溶解的分散材料。 密封剂层中的分散材料优选包括热塑性弹性体。 所得密封的显影剂容器即使在相对低的密封压力下也可以设置声音密封结构,导致显影剂容器的较小的密封表面下压,这允许容器的再次密封。