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1. 发明申请

US20120245281A1 URETHANE RESIN PARTICLES FOR SLUSH MOLDING 有权
标题翻译：用于成型的URETHANE树脂颗粒
公开(公告)号：US20120245281A1
公开(公告)日：2012-09-27
申请号：US13514190
申请日：2010-12-10
申请人： Yasuhiro Tsudo , Masaki Inaba , Koichi Saito , Hideaki Saito , Takanori Yamamoto
发明人： Yasuhiro Tsudo , Masaki Inaba , Koichi Saito , Hideaki Saito , Takanori Yamamoto
IPC分类号： C08L75/04 , C08L75/12
CPC分类号： C08J3/203 , B29C41/18 , B29K2075/00 , C08G18/10 , C08G18/12 , C08G18/42 , C08G18/73 , C08J3/12 , C08J3/20 , C08J2375/00 , C08J2375/04
摘要： Provided are urethane resin particles for slush molding which make it possible that inconveniences based on the slip-down of a pigment, on the aggregation of particles of the pigment, and on other causes are removed although this coloring is coloring onto the resin particle surfaces. The present invention is urethane resin particles for slush mold which contain a urethane resin and an additive, wherein the particles have a shape factor SF1 of 101 to 200, a shape factor SF2 of 120 to 240, and a central particle diameter of 20 to 500 μm. It is preferred that the urethane resin has a concentration of urea groups of 0.5 to 10% by weight, a total of the concentration of urethane groups and that of the urea groups of 4 to 20% by weight, a melting point of 160 to 260° C. and a glass transition temperature of −65 to 0° C.
摘要翻译：提供了用于搪塑的聚氨酯树脂颗粒，这使得可能除去颜料着色到树脂颗粒表面上以来，基于颜料的滑落，颜料的颗粒聚集和其它原因的不便。本发明是含有聚氨酯树脂和添加剂的用于糊模的聚氨酯树脂颗粒，其中颗粒的形状因子SF1为101〜200，形状因子SF2为120〜240，中心粒径为20〜500 μm。优选的是，所述聚氨酯树脂的尿素基浓度为0.5〜10重量％，氨基甲酸酯基和尿素基的浓度的总和为4〜20重量％，熔点为160〜260 ℃，玻璃化转变温度为-65℃至0℃。

2. 发明授权

US08912281B2 Urethane resin particles for slush molding 有权
标题翻译：用于搪塑的聚氨酯树脂颗粒
公开(公告)号：US08912281B2
公开(公告)日：2014-12-16
申请号：US13514190
申请日：2010-12-09
申请人： Yasuhiro Tsudo , Masaki Inaba , Koichi Saito , Hideaki Saito , Takanori Yamamoto
发明人： Yasuhiro Tsudo , Masaki Inaba , Koichi Saito , Hideaki Saito , Takanori Yamamoto
IPC分类号： C08G18/08 , B29C41/18 , C08J3/20 , C08G18/73 , C08G18/10 , C08G18/12 , C08G18/42 , B29K75/00
CPC分类号： C08J3/203 , B29C41/18 , B29K2075/00 , C08G18/10 , C08G18/12 , C08G18/42 , C08G18/73 , C08J3/12 , C08J3/20 , C08J2375/00 , C08J2375/04
摘要： Provided are urethane resin particles for slush molding which make it possible that inconveniences based on the slip-down of a pigment, on the aggregation of particles of the pigment, and on other causes are removed although this coloring is coloring onto the resin particle surfaces. The present invention is urethane resin particles for slush mold which contain a urethane resin and an additive, wherein the particles have a shape factor SF1 of 101 to 200, a shape factor SF2 of 120 to 240, and a central particle diameter of 20 to 500 μm. It is preferred that the urethane resin has a concentration of urea groups of 0.5 to 10% by weight, a total of the concentration of urethane groups and that of the urea groups of 4 to 20% by weight, a melting point of 160 to 260° C. and a glass transition temperature of −65 to 0° C.
摘要翻译：提供了用于搪塑的聚氨酯树脂颗粒，这使得可能除去颜料着色到树脂颗粒表面上以来，基于颜料的滑落，颜料的颗粒聚集和其它原因的不便。本发明是含有聚氨酯树脂和添加剂的用于糊模的聚氨酯树脂颗粒，其中颗粒的形状因子SF1为101〜200，形状因子SF2为120〜240，中心粒径为20〜500 μm。优选的是，所述聚氨酯树脂的尿素基浓度为0.5〜10重量％，氨基甲酸酯基和尿素基的浓度的总和为4〜20重量％，熔点为160〜260 ℃，玻璃化转变温度为-65℃至0℃。

3. 发明申请

US20130237664A1 URETHANE RESIN PARTICLES 有权
标题翻译： URETHANE树脂颗粒
公开(公告)号：US20130237664A1
公开(公告)日：2013-09-12
申请号：US13884771
申请日：2011-11-09
申请人： Shinji Watanabe , Yasuhiro Tsudo , Masaki Inaba , Jun Takeuchi , Yuko Matsumoto
发明人： Shinji Watanabe , Yasuhiro Tsudo , Masaki Inaba , Jun Takeuchi , Yuko Matsumoto
IPC分类号： C08G18/83 , C08K5/04 , C08L75/12
CPC分类号： C08G18/831 , B29C41/003 , B29C41/18 , B29K2075/00 , C08G18/12 , C08G18/2815 , C08G18/2825 , C08G18/3215 , C08G18/345 , C08G18/346 , C08G18/42 , C08G18/4202 , C08G18/4208 , C08G18/6659 , C08G18/73 , C08G18/8064 , C08G2140/00 , C08K5/04 , C08K5/092 , C08K5/103 , C08L75/12 , C08L75/06
摘要： Provided is a slush molding material which exhibits excellent low-temperature meltability and heat resistance and which can yield a molded product having excellent tensile strength and elongation. The present invention is urethane resin particles (D1) comprising a urethane or urethane-urea resin (U1) that has residues (j) bonded thereto covalently, said residues (j) being residues derived from an at least trivalent aromatic polycarboxylic acid by removing hydroxyl groups, or urethane resin particles (D2) comprising a urethane resin composition (S2) which comprises both a urethane or urethane-urea resin (U2) and a compound (E) that has a residue (j) derived from an at least trivalent aromatic polycarboxylic acid by removing hydroxyl groups, said compound (E) being represented by general formula (1), wherein the residues (j) are linked respectively to urethane or urea groups (u) of the resin (U1) or (U2) by hydrogen bonds.
摘要翻译：提供一种具有优异的低温熔融性和耐热性的搪塑成型材料，并且可以得到具有优异的拉伸强度和伸长率的成型体。本发明是包含具有共价键合的残基（j）的氨基甲酸酯或氨基甲酸酯 - 尿素树脂（U1）的聚氨酯树脂颗粒（D1），所述残基（j）是通过除去羟基从至少三价芳族多元羧酸衍生的残基基团或聚氨酯树脂颗粒（D2），其包含氨基甲酸酯或氨基甲酸酯 - 脲树脂（U2）和具有衍生自至少三价芳族化合物的残基（j）的化合物（E）的聚氨酯树脂组合物（S2）通过除去羟基的多元羧酸，所述化合物（E）由通式（1）表示，其中残基（j）分别通过氢气与树脂（U1）或（U2）的氨基甲酸酯基或脲基（u）连接债券。

4. 发明申请

US20120245280A1 THERMOPLASTIC URETHANE RESIN 审中-公开
标题翻译：热塑性URETHANE树脂
公开(公告)号：US20120245280A1
公开(公告)日：2012-09-27
申请号：US13514113
申请日：2010-12-03
申请人： Yasuhiro Tsudo , Masaki Inaba , Shinji Watanabe
发明人： Yasuhiro Tsudo , Masaki Inaba , Shinji Watanabe
IPC分类号： C08G18/42 , C08G18/66 , C08L75/06
CPC分类号： C08G18/4018 , C08G18/12 , C08G18/2825 , C08G18/4202 , C08G18/4211 , C08G18/4216 , C08G18/73 , C08G2140/00 , C08G2170/20 , C08G18/3275
摘要： An object is to provide a material for slush molding that is excellent in low-temperature meltability, and gives a molded body excellent in both of tensile strength and elongation. The present invention is a thermoplastic urethane resin (D) for thermal molding, which is a thermoplastic urethane resin yielded by causing high molecular weight diols (A) to react with a diisocyanate (B), wherein the high molecular weight diols (A) comprise a polyester diol (A1) having a glass transition temperature of 0 to 70° C., and a high molecular weight diol (A2) having a solubility parameter lower than that of the (A1) by 1.2 to 3.0 and further having a glass transition temperature of −40 to −75° C.
摘要翻译：本发明的目的是提供一种低温熔融性优异的用于搪塑的材料，并且具有优异的拉伸强度和伸长率的成型体。本发明是一种用于热成型的热塑性聚氨酯树脂（D），其是通过使高分子量二醇（A）与二异氰酸酯（B）反应而产生的热塑性聚氨酯树脂，其中高分子量二醇（A）包含玻璃化转变温度为0〜70℃的聚酯二醇（A1）和比（A1）的溶解度参数低1.2〜3.0的高分子量二醇（A2），还具有玻璃化转变温度为-40〜-75℃

5. 发明授权

US09023941B2 Urethane resin particles 有权
标题翻译：聚氨酯树脂颗粒
公开(公告)号：US09023941B2
公开(公告)日：2015-05-05
申请号：US13884771
申请日：2011-11-09
申请人： Shinji Watanabe , Yasuhiro Tsudo , Masaki Inaba , Jun Takeuchi , Yuko Matsumoto
发明人： Shinji Watanabe , Yasuhiro Tsudo , Masaki Inaba , Jun Takeuchi , Yuko Matsumoto
IPC分类号： C08G18/83 , C08G18/42 , C08K5/092 , C08K5/103 , C08G18/80 , C08G18/32 , C08L75/06 , B29C41/00 , B29C41/18 , C08G18/66 , C08G18/73 , C08G18/12 , C08G18/28 , C08G18/34 , C08K5/04 , C08L75/12 , B29K75/00
CPC分类号： C08G18/831 , B29C41/003 , B29C41/18 , B29K2075/00 , C08G18/12 , C08G18/2815 , C08G18/2825 , C08G18/3215 , C08G18/345 , C08G18/346 , C08G18/42 , C08G18/4202 , C08G18/4208 , C08G18/6659 , C08G18/73 , C08G18/8064 , C08G2140/00 , C08K5/04 , C08K5/092 , C08K5/103 , C08L75/12 , C08L75/06
摘要： Provided is a slush molding material which exhibits excellent low-temperature meltability and heat resistance and which can yield a molded product having excellent tensile strength and elongation. The present invention is urethane resin particles (D1) comprising a urethane or urethane-urea resin (U1) that has residues (j) bonded thereto covalently, said residues (j) being residues derived from an at least trivalent aromatic polycarboxylic acid by removing hydroxyl groups, or urethane resin particles (D2) comprising a urethane resin composition (S2) which comprises both a urethane or urethane-urea resin (U2) and a compound (E) that has a residue (j) derived from an at least trivalent aromatic polycarboxylic acid by removing hydroxyl groups, said compound (E) being represented by general formula (1), wherein the residues (j) are linked respectively to urethane or urea groups (u) of the resin (U1) or (U2) by hydrogen bonds.
摘要翻译：提供一种具有优异的低温熔融性和耐热性的搪塑成型材料，并且可以得到具有优异的拉伸强度和伸长率的成型体。本发明是包含具有共价键合的残基（j）的氨基甲酸酯或氨基甲酸酯 - 尿素树脂（U1）的聚氨酯树脂颗粒（D1），所述残基（j）是通过除去羟基从至少三价芳族多元羧酸衍生的残基基团或聚氨酯树脂颗粒（D2），其包含氨基甲酸酯或氨基甲酸酯 - 脲树脂（U2）和具有衍生自至少三价芳族化合物的残基（j）的化合物（E）的聚氨酯树脂组合物（S2）通过除去羟基的多元羧酸，所述化合物（E）由通式（1）表示，其中残基（j）分别通过氢气与树脂（U1）或（U2）的氨基甲酸酯基或脲基（u）连接债券。

6. 发明申请

US20140179864A1 POWDERED POLYURETHANE UREA RESIN COMPOSITION FOR SLUSH MOLDING AND MANUFACTURING PROCESS THEREFOR 有权
标题翻译：粉末状聚氨酯尿素树脂组合物，用于其模塑和制造工艺
公开(公告)号：US20140179864A1
公开(公告)日：2014-06-26
申请号：US14236495
申请日：2012-07-30
申请人： Koichi Saito , Ko Kawasaki , Kakuhiro Kawaguchi , Yasuhiro Tsudo
发明人： Koichi Saito , Ko Kawasaki , Kakuhiro Kawaguchi , Yasuhiro Tsudo
IPC分类号： C08K3/04
CPC分类号： C08K3/04 , B29B9/12 , B29B9/16 , B29B2009/125 , B29B2009/161 , B29B2009/163 , B29B2009/166 , B29C39/00 , B29C41/16 , B29C41/18 , B29C67/02 , B29C67/06 , B29C67/24 , C08G18/00 , C08G18/06 , C08G18/08 , C08G18/0847 , C08G18/0852 , C08G18/0866 , C08G18/10 , C08G18/12 , C08G18/28 , C08G18/2805 , C08G18/2815 , C08G18/282 , C08G18/2825 , C08G18/4202 , C08G18/4211 , C08G18/4213 , C08G18/4238 , C08G18/73 , C08G2140/00 , C08J3/00 , C08J3/12 , C08K3/00 , C08K5/00 , C08L75/02 , C08G18/3228
摘要： Provided are: a powdered material for slush molding; and a manufacturing process therefor. The powdered material is less odorous, exhibits excellent powder fluidity, and does not suffer from troubles resulting from the sliding-down or agglomeration of a pigment even when the resin particles have been pigmented on the surfaces thereof. Thus, the powdered material ensures high productivity. The powdered material is a powdered polyurethane urea resin composition which comprises (D) a polyurethane urea resin that has a total content of bimolecular condensate of acetone, bimolecular condensate of methyl ethyl ketone, and bimolecular condensate of methyl isobutyl ketone of 1,000 ppm or less and (N) an additive, wherein the polyurethane urea resin (D) takes the form of thermoplastic polyurethane urea resin particles (P) that have a volume-mean particle diameter of 20 to 500 μm and that have protrusions and recesses on the surfaces. The powdered polyurethane urea resin composition is manufactured by a manufacturing process which includes a step of mixing (A) an isocyanato-terminated urethane prepolymer with (B) an alicyclic diamine and/or an aliphatic diamine in an aqueous medium by stirring to form the resin particles (P).
摘要翻译：提供：用于搪塑的粉状材料; 及其制造工艺。该粉末状材料的气味较少，表现出优异的粉末流动性，并且即使树脂颗粒在其表面上着色时也不会由于颜料的滑落或凝聚而产生麻烦。因此，粉末材料确保高生产率。粉末状材料是粉末状聚氨酯脲树脂组合物，其包含（D）聚丙烯酸脲树脂，其具有丙酮的双分子缩合物，甲基乙基酮的双分子缩合物和甲基异丁基酮的双分子缩合物的总含量为1,000ppm以下，（N）添加剂，其中，所述聚氨酯脲树脂（D）为体积平均粒径为20〜500μm的热塑性聚氨酯脲树脂粒子（P）的形式，在所述表面具有突起和凹部。粉末状聚氨酯脲树脂组合物通过制造方法制造，其包括通过搅拌将（A）异氰酸酯基封端的氨基甲酸酯预聚物与（B）脂环族二胺和/或脂族二胺混合以形成树脂的步骤颗粒（P）。

7. 发明授权

US09550874B2 Powdered polyurethane urea resin composition for slush molding and manufacturing process therefor 有权
标题翻译：用于搪塑的粉状聚氨酯脲树脂组合物及其制造方法
公开(公告)号：US09550874B2
公开(公告)日：2017-01-24
申请号：US14236495
申请日：2012-07-30
申请人： Koichi Saito , Ko Kawasaki , Kakuhiro Kawaguchi , Yasuhiro Tsudo
发明人： Koichi Saito , Ko Kawasaki , Kakuhiro Kawaguchi , Yasuhiro Tsudo
IPC分类号： B29B9/12 , B29B9/16 , B29C39/00 , B29C41/16 , B29C41/18 , B29C67/02 , B29C67/06 , B29C67/24 , C08K3/04 , C08G18/00 , C08G18/06 , C08G18/08 , C08G18/10 , C08G18/12 , C08G18/28 , C08G18/42 , C08G18/73
CPC分类号： C08K3/04 , B29B9/12 , B29B9/16 , B29B2009/125 , B29B2009/161 , B29B2009/163 , B29B2009/166 , B29C39/00 , B29C41/16 , B29C41/18 , B29C67/02 , B29C67/06 , B29C67/24 , C08G18/00 , C08G18/06 , C08G18/08 , C08G18/0847 , C08G18/0852 , C08G18/0866 , C08G18/10 , C08G18/12 , C08G18/28 , C08G18/2805 , C08G18/2815 , C08G18/282 , C08G18/2825 , C08G18/4202 , C08G18/4211 , C08G18/4213 , C08G18/4238 , C08G18/73 , C08G2140/00 , C08J3/00 , C08J3/12 , C08K3/00 , C08K5/00 , C08L75/02 , C08G18/3228
摘要： Provided are: a powdered material for slush molding; and a manufacturing process therefor. The powdered material is less odorous, exhibits excellent powder fluidity, and does not suffer from troubles resulting from the sliding-down or agglomeration of a pigment even when the resin particles have been pigmented on the surfaces thereof. Thus, the powdered material ensures high productivity. The powdered material is a powdered polyurethane urea resin composition which comprises (D) a polyurethane urea resin that has a total content of bimolecular condensate of acetone, bimolecular condensate of methyl ethyl ketone, and bimolecular condensate of methyl isobutyl ketone of 1,000 ppm or less and (N) an additive, wherein the polyurethane urea resin (D) takes the form of thermoplastic polyurethane urea resin particles (P) that have a volume-mean particle diameter of 20 to 500 μm and that have protrusions and recesses on the surfaces. The powdered polyurethane urea resin composition is manufactured by a manufacturing process which includes a step of mixing (A) an isocyanato-terminated urethane prepolymer with (B) an alicyclic diamine and/or an aliphatic diamine in an aqueous medium by stirring to form the resin particles (P).
摘要翻译：提供：用于搪塑的粉末材料; 及其制造工艺。该粉末状材料的气味较少，表现出优异的粉末流动性，并且即使树脂颗粒在其表面上着色时也不会由于颜料的滑落或凝聚而产生麻烦。因此，粉末材料确保高生产率。粉末状材料是粉末状聚氨酯脲树脂组合物，其包含（D）聚丙烯酸脲树脂，其具有丙酮的双分子缩合物，甲基乙基酮的双分子缩合物和甲基异丁基酮的双分子缩合物的总含量为1,000ppm以下，（N）添加剂，其中，所述聚氨酯脲树脂（D）为体积平均粒径为20〜500μm的热塑性聚氨酯脲树脂粒子（P）的形式，在所述表面具有突起和凹部。粉末状聚氨酯脲树脂组合物通过制造方法制造，其包括通过搅拌将（A）异氰酸酯基封端的氨基甲酸酯预聚物与（B）脂环族二胺和/或脂族二胺混合以形成树脂的步骤颗粒（P）。

8. 发明授权

US09125315B2 Conductive film and method for its production 有权
标题翻译：导电膜及其生产方法
公开(公告)号：US09125315B2
公开(公告)日：2015-09-01
申请号：US13574073
申请日：2011-01-18
申请人： Ko Higashitani , Yasuhiro Tsudo , Masaki Nakayama , Shinji Kake
发明人： Ko Higashitani , Yasuhiro Tsudo , Masaki Nakayama , Shinji Kake
IPC分类号： H05K1/09 , H05K3/12 , H05K9/00 , H01B1/02
CPC分类号： H05K3/1216 , H01B1/02 , H05K1/092 , H05K1/097 , H05K9/0094
摘要： To provide a method for producing a conductive film with excellent transparency and conductivity by a simple method suitable for large-area production.A method for producing a conductive film comprising a step of placing a template (B), having openings in a mesh structure running from the side that is to contact a substrate (A) through to the back side, on the surface of the substrate (A), and spreading a dispersion (D) of conductive particles (P) on the surface of the substrate (A) on which the template (B) has been placed, and drying it, thereby forming a mesh-like structure (C) of the conductive particles (P) near the points of contact between the substrate (A) and the template (B), and then removing the template (B) from the substrate (A) to form a mesh-like structure (C) of the conductive particles (P) on the surface of the substrate (A).
摘要翻译：提供一种适用于大面积生产的简单方法制备具有优异透明性和导电性的导电膜的方法。一种导电膜的制造方法，其特征在于，在基板表面上设置具有开口的模板（B），所述模板（B）具有从所述基板（A）的与所述背面接触的一侧的网状结构的开口 A），并且在已经放置了模板（B）的基板（A）的表面上铺展导电颗粒（P）的分散体（D）并干燥，从而形成网状结构（C）在基板（A）和模板（B）之间的接触点附近的导电粒子（P）之间，然后从基板（A）去除模板（B），以形成网状结构（C）在基板（A）的表面上的导电粒子（P）。

9. 发明申请

US20120325545A1 CONDUCTIVE FILM AND METHOD FOR ITS PRODUCTION 有权
标题翻译：导电膜及其生产方法
公开(公告)号：US20120325545A1
公开(公告)日：2012-12-27
申请号：US13574073
申请日：2011-01-18
申请人： Ko Higashitani , Yasuhiro Tsudo , Masaki Nakayama , Shinji Kake
发明人： Ko Higashitani , Yasuhiro Tsudo , Masaki Nakayama , Shinji Kake
IPC分类号： H05K1/02 , C25D15/00 , B05D5/12
CPC分类号： H05K3/1216 , H01B1/02 , H05K1/092 , H05K1/097 , H05K9/0094
摘要： To provide a method for producing a conductive film with excellent transparency and conductivity by a simple method suitable for large-area production.A method for producing a conductive film comprising a step of placing a template (B), having openings in a mesh structure running from the side that is to contact a substrate (A) through to the back side, on the surface of the substrate (A), and spreading a dispersion (D) of conductive particles (P) on the surface of the substrate (A) on which the template (B) has been placed, and drying it, thereby forming a mesh-like structure (C) of the conductive particles (P) near the points of contact between the substrate (A) and the template (B), and then removing the template (B) from the substrate (A) to form a mesh-like structure (C) of the conductive particles (P) on the surface of the substrate (A).
摘要翻译：提供一种适用于大面积生产的简单方法制备具有优异透明性和导电性的导电膜的方法。一种导电膜的制造方法，其特征在于，在基板表面上设置具有开口的模板（B），所述模板（B）具有从所述基板（A）的与所述背面接触的一侧的网状结构的开口 A），并且在已经放置了模板（B）的基板（A）的表面上铺展导电颗粒（P）的分散体（D）并干燥，从而形成网状结构（C）在基板（A）和模板（B）之间的接触点附近的导电粒子（P）之间，然后从基板（A）去除模板（B），以形成网状结构（C）在基板（A）的表面上的导电粒子（P）。

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