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1. 发明授权

US08575277B2 Process for production of nucleus-hydrogenated aromatic vinyl/(meth)acrylate copolymers 有权
标题翻译：核 - 氢化芳族乙烯基/（甲基）丙烯酸酯共聚物的生产方法
公开(公告)号：US08575277B2
公开(公告)日：2013-11-05
申请号：US12672152
申请日：2008-08-04
申请人： Yasuhiro Kushida , Yuuichi Sugano , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
发明人： Yasuhiro Kushida , Yuuichi Sugano , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
IPC分类号： C08F8/04
CPC分类号： G11B7/2533 , B01J21/06 , B01J21/066 , B01J23/44 , B01J35/0066 , B01J37/0203 , C08F8/04 , C08F212/08 , C08F220/18 , C08F2800/10 , C08F2810/50 , C08F220/14
摘要： A safe and stable production method of a hydrogenated polymer having high transparency, which is a production method of a hydrogenated polymer by hydrogenating aromatic rings of an aromatic vinyl compound-(meth)acrylate copolymer, in which (1) a solvent solution of the copolymer is added to a reactor, which has a solvent and a supported palladium catalyst charged therein, under a hydrogen atmosphere at a rate of from 0.01 to 15 g/hour in terms of the copolymer per unit mass (g) of the supported palladium catalyst, thereby performing hydrogenation reaction, and then such an operation is performed repeatedly that (2) a hydrogenated polymer is obtained from 30 to 90% by mass of the resulting reaction mixed solution, and a fresh solvent solution of the copolymer is added to the reactor, in which the residual reaction mixed solution is left, or to which the residual reaction mixed solution is returned, at a rate of from 0.01 to 15 g/hour in terms of the copolymer per unit mass (g) of the supported palladium catalyst, thereby performing hydrogenation reaction.
摘要翻译：通过氢化芳香族乙烯基化合物 - （甲基）丙烯酸酯共聚物的芳香环，是氢化聚合物的制造方法的高透明性的安全稳定的制造方法，其中（1）共聚物的溶剂溶液加入到反应器中，其中，在氢气氛下，以负载的钯催化剂的单位质量（g）的共聚物为0.01〜15g /小时，加入溶剂和负载的钯催化剂，进行氢化反应，然后重复进行这样的操作：（2）得到的反应混合溶液的氢化聚合物的质量为30〜90质量％，将共聚物的新鲜溶剂溶液加入到反应器中，残留的反应混合溶液返回残余反应混合溶液，以每单位质量（g）的共聚物计，为0.01〜15g /小时报告钯催化剂，从而进行氢化反应。

2. 发明申请

US20110269912A1 PROCESS FOR PRODUCTION OF NUCLEUS-HYDROGENATED AROMATIC VINYL/(METH)ACRYLATE COPOLYMERS 有权
标题翻译：生产氢化羟基乙酸/（甲基）丙烯酸酯共聚物的方法
公开(公告)号：US20110269912A1
公开(公告)日：2011-11-03
申请号：US12672152
申请日：2008-08-04
申请人： Yasuhiro Kushida , Yuuichi Sugano , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
发明人： Yasuhiro Kushida , Yuuichi Sugano , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
IPC分类号： C08F8/04 , C08F220/18
CPC分类号： G11B7/2533 , B01J21/06 , B01J21/066 , B01J23/44 , B01J35/0066 , B01J37/0203 , C08F8/04 , C08F212/08 , C08F220/18 , C08F2800/10 , C08F2810/50 , C08F220/14
摘要： A safe and stable production method of a hydrogenated polymer having high transparency, which is a production method of a hydrogenated polymer by hydrogenating aromatic rings of an aromatic vinyl compound-(meth)acrylate copolymer, in which (1) a solvent solution of the copolymer is added to a reactor, which has a solvent and a supported palladium catalyst charged therein, under a hydrogen atmosphere at a rate of from 0.01 to 15 g/hour in terms of the copolymer per unit mass (g) of the supported palladium catalyst, thereby performing hydrogenation reaction, and then such an operation is performed repeatedly that (2) a hydrogenated polymer is obtained from 30 to 90% by mass of the resulting reaction mixed solution, and a fresh solvent solution of the copolymer is added to the reactor, in which the residual reaction mixed solution is left, or to which the residual reaction mixed solution is returned, at a rate of from 0.01 to 15 g/hour in terms of the copolymer per unit mass (g) of the supported palladium catalyst, thereby performing hydrogenation reaction.
摘要翻译：通过氢化芳香族乙烯基化合物 - （甲基）丙烯酸酯共聚物的芳香环，是氢化聚合物的制造方法的高透明性的安全稳定的制造方法，其中（1）共聚物的溶剂溶液加入到反应器中，其中，在氢气氛下，以负载的钯催化剂的单位质量（g）的共聚物为0.01〜15g /小时，加入溶剂和负载的钯催化剂，进行氢化反应，然后重复进行这样的操作：（2）得到的反应混合溶液的氢化聚合物的质量为30〜90质量％，将共聚物的新鲜溶剂溶液加入到反应器中，残留的反应混合溶液返回残余反应混合溶液，以每单位质量（g）的共聚物计，为0.01〜15g /小时报告钯催化剂，从而进行氢化反应。

3. 发明申请

US20070185277A1 PROCESS FOR PRODUCING HYDROGENATED POLYMERS 有权
标题翻译：生产氢化聚合物的方法
公开(公告)号：US20070185277A1
公开(公告)日：2007-08-09
申请号：US11679222
申请日：2007-02-27
申请人： Yuuichi Sugano , Yasuhiro Kushida , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
发明人： Yuuichi Sugano , Yasuhiro Kushida , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
IPC分类号： C08F265/04
CPC分类号： C08F8/04 , C08F212/08
摘要： A process for producing a hydrogenated polymer, which includes a step of hydrogenating aromatic rings of an aromatic vinyl compound—(meth)acrylate copolymer. In the process, the copolymer having a ratio, A/B, of from 0.25 to 4.0 (A is a molar number of constitutional units derived from the (meth)acrylate monomer, and B is a molar number of constitutional units derived from the aromatic vinyl monomer) is hydrogenated in a solvent in the presence of a catalyst which is composed of zirconium oxide supporting palladium. By the process, a highly transparent, hydrogenated polymer is stably and rapidly produced for a long period of time or repeatedly.
摘要翻译：一种氢化聚合物的制造方法，其包括使芳香族乙烯基化合物 - （甲基）丙烯酸酯共聚物的芳香环氢化的工序。在该方法中，A / B比为0.25〜4.0（A为来自（甲基）丙烯酸酯单体的结构单元的摩尔数），B为衍生自芳香族化合物的结构单元的摩尔数乙烯基单体）在溶剂中在由氧化锆担载钯组成的催化剂存在下氢化。通过该方法，高度透明的氢化聚合物长时间或重复地稳定且快速地生产。

4. 发明授权

US07488782B2 Process for producing hydrogenated polymers 有权
标题翻译：生产氢化聚合物的方法
公开(公告)号：US07488782B2
公开(公告)日：2009-02-10
申请号：US11679222
申请日：2007-02-27
申请人： Yuuichi Sugano , Yasuhiro Kushida , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
发明人： Yuuichi Sugano , Yasuhiro Kushida , Tatsuya Yamauchi , Hideyuki Sato , Yoshikazu Shima
IPC分类号： C08C19/02 , C08F220/18 , C08F12/08
CPC分类号： C08F8/04 , C08F212/08
摘要： A process for producing a hydrogenated polymer, which includes a step of hydrogenating aromatic rings of an aromatic vinyl compound—(meth)acrylate copolymer. In the process, the copolymer having a ratio, A/B, of from 0.25 to 4.0 (A is a molar number of constitutional units derived from the (meth)acrylate monomer, and B is a molar number of constitutional units derived from the aromatic vinyl monomer) is hydrogenated in a solvent in the presence of a catalyst which is composed of zirconium oxide supporting palladium. By the process, a highly transparent, hydrogenated polymer is stably and rapidly produced for a long period of time or repeatedly.
摘要翻译：一种氢化聚合物的制造方法，其包括使芳香族乙烯基化合物 - （甲基）丙烯酸酯共聚物的芳香环氢化的工序。在该方法中，A / B比为0.25〜4.0（A为来自（甲基）丙烯酸酯单体的结构单元的摩尔数），B为衍生自芳香族化合物的结构单元的摩尔数乙烯基单体）在溶剂中在由氧化锆担载钯组成的催化剂存在下氢化。通过该方法，高度透明的氢化聚合物长时间或重复地稳定且快速地生产。

5. 发明授权

US07446152B2 Method of producing hydrogenated polymers 有权
标题翻译：生产氢化聚合物的方法
公开(公告)号：US07446152B2
公开(公告)日：2008-11-04
申请号：US11374068
申请日：2006-03-14
申请人： Tatsuya Yamauchi , Yasuhiro Kushida , Yuuichi Sugano , Yoshikazu Shima
发明人： Tatsuya Yamauchi , Yasuhiro Kushida , Yuuichi Sugano , Yoshikazu Shima
IPC分类号： C08F8/04
CPC分类号： C08F220/14 , B01J23/40 , B01J23/755 , C08F8/04 , C08F2800/10 , C08F2810/50 , G02B1/041 , G11B7/253 , C08F212/08 , C08L33/10
摘要： In the production of a nuclear-hydrogenated polymer, the hydrogenation of an aromatic vinyl compound—(meth)acrylate copolymer is conducted in a mixed solvent comprising an ester compound and an alcohol compound in the presence of a catalyst. By this method, a highly transparent nuclear-hydrogenated polymer is produced safely, stably and quickly, even when the degree of nuclear-hydrogenation is low.
摘要翻译：在制备核氢化聚合物中，芳族乙烯基化合物 - （甲基）丙烯酸酯共聚物的氢化在包含酯化合物和醇化合物的混合溶剂中在催化剂存在下进行。通过该方法，即使核氢化程度低，安全，稳定，快速地制造高度透明的核氢化聚合物。

6. 发明申请

US20060205886A1 Method of producing hydrogenated polymers 有权
标题翻译：生产氢化聚合物的方法
公开(公告)号：US20060205886A1
公开(公告)日：2006-09-14
申请号：US11374068
申请日：2006-03-14
申请人： Tatsuya Yamauchi , Yasuhiro Kushida , Yuuichi Sugano , Yoshikazu Shima
发明人： Tatsuya Yamauchi , Yasuhiro Kushida , Yuuichi Sugano , Yoshikazu Shima
IPC分类号： C08F297/00
CPC分类号： C08F220/14 , B01J23/40 , B01J23/755 , C08F8/04 , C08F2800/10 , C08F2810/50 , G02B1/041 , G11B7/253 , C08F212/08 , C08L33/10
摘要： In the production of a nuclear-hydrogenated polymer, the hydrogenation of an aromatic vinyl compound—(meth)acrylate copolymer is conducted in a mixed solvent comprising an ester compound and an alcohol compound in the presence of a catalyst. By this method, a highly transparent nuclear-hydrogenated polymer is produced safely, stably and quickly, even when the degree of nuclear-hydrogenation is low.
摘要翻译：在制备核氢化聚合物中，芳族乙烯基化合物 - （甲基）丙烯酸酯共聚物的氢化在包含酯化合物和醇化合物的混合溶剂中在催化剂存在下进行。通过该方法，即使核氢化程度低，安全，稳定，快速地制造高度透明的核氢化聚合物。

7. 发明授权

US6069388A Semiconductor device and production method thereof 失效
标题翻译：半导体装置及其制造方法
公开(公告)号：US6069388A
公开(公告)日：2000-05-30
申请号：US984144
申请日：1997-12-03
申请人： Yoshihiro Okusa , Tatsuya Yamauchi
发明人： Yoshihiro Okusa , Tatsuya Yamauchi
IPC分类号： H01L21/02 , H01L21/28 , H01L21/336 , H01L29/04 , H01L29/786 , H01G4/06
CPC分类号： H01L28/40 , H01L21/28158 , H01L29/045 , H01L29/66757 , H01L29/78675
摘要： On a silicon substrate 1 is provided a silicon oxide film 2, on which a polycrystalline silicon film 3 is formed by a low pressure CVD method at a monosilane partial pressure of no more than 10 Pa and a film formation temperature of no lower than 600.degree. C. The polycrystalline silicon film is doped with an impurity such as phosphorus in a concentration of 1.times.10.sup.20 atoms/cm.sup.3 to 1.times.10.sup.21 atoms/cm.sup.3 to form a phosphosilicate glass film 6, and after removing it, the polycrystalline silicon film is thermally oxidized in an oxidative atmosphere to form a dielectric film 5 on the surface. A polycrystalline silicon film 4 is formed on the dielectric film 5, which is treated as the oriented polycrystalline silicon film 3a to form an oriented polycrystalline silicon film 4a. The oriented polycrystalline silicon film 4a as an upper electrode and the oriented polycrystalline silicon film 3a as a lower electrode are wired to obtain a semiconductor device having a capacitor. Further, a thin film transistor of a high dielectric strength can be produced in a short time on the polycrystalline silicon which is oriented in a short time.
摘要翻译：在硅基板1上设置氧化硅膜2，通过低压CVD法在不超过10Pa的单硅烷分压和不低于600°的成膜温度下形成多晶硅膜3 C.多晶硅膜掺杂浓度为1×10 20原子/ cm 3至1×10 21原子/ cm 3的磷等杂质，形成磷硅玻璃膜6，去除后，多晶硅膜氧化成氧化在表面形成电介质膜5。在作为取向多晶硅膜3a的电介质膜5上形成多晶硅膜4，形成取向多晶硅膜4a。将作为上电极的定向多晶硅膜4a和作为下电极的取向多晶硅膜3a布线以获得具有电容器的半导体器件。此外，可以在短时间内在短时间取向的多晶硅上制造高介电强度的薄膜晶体管。

8. 发明授权

US06316339B1 Semiconductor device and production method thereof 有权
标题翻译：半导体装置及其制造方法
公开(公告)号：US06316339B1
公开(公告)日：2001-11-13
申请号：US09513343
申请日：2000-02-25
申请人： Yoshihiro Okusa , Tatsuya Yamauchi
发明人： Yoshihiro Okusa , Tatsuya Yamauchi
IPC分类号： H01L2120
CPC分类号： H01L28/40 , H01L21/28158 , H01L29/045 , H01L29/66757 , H01L29/78675
摘要： On a silicon substrate 1 is provided a silicon oxide film 2, on which a polycrystalline silicon film 3 is formed by a low pressure CVD method at a monosilane partial pressure of no more than 10 Pa and a film formation temperature of no lower than 600° C. The polycrystalline silicon film is doped with an impurity such as phosphorus in a concentration of 1×1020 atoms/cm3 to 1×1021 atoms/cm3 to form a phosphosilicate glass film 6, and after removing it, the polycrystalline silicon film is thermally oxidized in an oxidative atmosphere to form a dielectric film 5 on the surface. A polycrystalline silicon film 4 is formed on the dielectric film 5, which is treated as the oriented polycrystalline silicon film 3a to form an oriented polycrystalline silicon film 4a. The oriented polycrystalline silicon film 4a as an upper electrode and the oriented polycrystalline silicon film 3a as a lower electrode are wired to obtain a semiconductor device having a capacitor. Further, a thin film transistor of a high dielectric strength can be produced in a short time on the polycrystalline silicon which is oriented in a short time.
摘要翻译：在硅基板1上设置氧化硅膜2，通过低压CVD法在不超过10Pa的单硅烷分压和不低于600°的成膜温度下形成多晶硅膜3 C.多晶硅膜掺杂浓度为1×10 20原子/ cm 3至1×10 21原子/ cm 3的磷等杂质，形成磷硅玻璃膜6，去除后，多晶硅膜氧化成氧化在表面形成电介质膜5。在作为取向多晶硅膜3a的电介质膜5上形成多晶硅膜4，形成取向多晶硅膜4a。将作为上电极的定向多晶硅膜4a和作为下电极的取向多晶硅膜3a布线以获得具有电容器的半导体器件。此外，可以在短时间内在短时间取向的多晶硅上制造高介电强度的薄膜晶体管。

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