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1. 发明授权

US09394212B2 Process for the cooligomerization of olefins 有权
标题翻译：烯烃低聚异构化方法
公开(公告)号：US09394212B2
公开(公告)日：2016-07-19
申请号：US13159761
申请日：2011-06-14
申请人： Wolfgang Rohde , Qiang Miao , Stefan Bitterlich , Gauthier Luc Maurice Averlant , Hans-Guenter Wagner , Beatrice Röβler-Feigel
发明人： Wolfgang Rohde , Qiang Miao , Stefan Bitterlich , Gauthier Luc Maurice Averlant , Hans-Guenter Wagner , Beatrice Röβler-Feigel
IPC分类号： C07C2/00 , C07C2/12
CPC分类号： C07C2/12 , C07C2523/755 , C07C2529/072 , C07C2529/70 , Y02P20/582 , C07C11/02
摘要： In a process for the cooligomerization of olefins, an olefin starting material comprising olefins having n carbon atoms and olefins having 2n carbon atoms is reacted over an olefin oligomerization catalyst to give a reaction product. The process is carried out under such conditions that the conversion of olefins having 2n carbon atoms is less than 10%. Both the cooligomer having 3n carbon atoms and the olefin having 2n carbon atoms which has been separated off from the reaction product have a high hydroformylatability.
摘要翻译：在烯烃冷却反应的方法中，将包含具有n个碳原子的烯烃和具有2n个碳原子的烯烃的烯烃原料在烯烃低聚催化剂上反应得到反应产物。该方法在具有2n个碳原子的烯烃的转化率小于10％的条件下进行。具有3n个碳原子的冷聚物和已经从反应产物中分离的具有2n个碳原子的烯烃都具有高的加氢甲酰化性。

2. 发明申请

US20110306812A1 PROCESS FOR THE COOLIGOMERIZATION OF OLEFINS 有权
标题翻译：烯烃冷却过程
公开(公告)号：US20110306812A1
公开(公告)日：2011-12-15
申请号：US13159761
申请日：2011-06-14
申请人： Wolfgang Rohde , Qiang Miao , Stefan Bitterlich , Gauthier Luc Maurice Averlant , Hans-Guenter Wagner , Beatrice Rößler-Feigel
发明人： Wolfgang Rohde , Qiang Miao , Stefan Bitterlich , Gauthier Luc Maurice Averlant , Hans-Guenter Wagner , Beatrice Rößler-Feigel
IPC分类号： C07C2/00
CPC分类号： C07C2/12 , C07C2523/755 , C07C2529/072 , C07C2529/70 , Y02P20/582 , C07C11/02
摘要： In a process for the cooligomerization of olefins, an olefin starting material comprising olefins having n carbon atoms and olefins having 2n carbon atoms is reacted over an olefin oligomerization catalyst to give a reaction product. The process is carried out under such conditions that the conversion of olefins having 2n carbon atoms is less than 10%. Both the cooligomer having 3n carbon atoms and the olefin having 2n carbon atoms which has been separated off from the reaction product have a high hydroformylatability.
摘要翻译：在烯烃冷却反应的方法中，将包含具有n个碳原子的烯烃和具有2n个碳原子的烯烃的烯烃原料在烯烃低聚催化剂上反应得到反应产物。该方法在具有2n个碳原子的烯烃的转化率小于10％的条件下进行。具有3n个碳原子的冷聚物和已经从反应产物中分离的具有2n个碳原子的烯烃都具有高的加氢甲酰化性。

3. 发明授权

US07750194B2 Process for preparing isopropanol and 2-butanol from the corresponding alkanes 失效
标题翻译：从相应的烷烃制备异丙醇和2-丁醇的方法
公开(公告)号：US07750194B2
公开(公告)日：2010-07-06
申请号：US12374351
申请日：2007-07-16
申请人： Georg Degen , Sven Crone , Ralf Boehling , Ansgar Gereon Altenhoff , Wolfgang Rohde , Jochen Buerkle , Goetz-Peter Schindler , Thomas Holtmann , Markus Schmitt
发明人： Georg Degen , Sven Crone , Ralf Boehling , Ansgar Gereon Altenhoff , Wolfgang Rohde , Jochen Buerkle , Goetz-Peter Schindler , Thomas Holtmann , Markus Schmitt
IPC分类号： C07C29/09
CPC分类号： C07C67/04 , C07C29/095 , Y02P20/127 , C07C31/10 , C07C31/12 , C07C69/06 , C07C69/14
摘要： A process for preparing alkanols (I) selected from the group consisting of isopropanol and 2-butanol from the corresponding alkanes (II) selected from the group consisting of propane and n-butane, comprising the steps of: A) providing a starting gas stream a comprising the alkane (II); B) feeding the starting gas stream a comprising the alkane (II) into a dehydrogenation zone and subjecting the alkane (II) to a dehydrogenation to the alkene (III) to obtain a product gas stream b comprising the alkene (III) and unconverted alkane (II), with or without high boilers, steam, hydrogen and low boilers; C) at least compressing product gas stream b, optionally separating product gas stream b into an aqueous phase c1, a phase c2 comprising the alkene (III) and the alkane (II), with or without high boilers, and a gas phase c3 comprising hydrogen and low boilers; D) reacting product gas stream b or the phase c2 comprising alkene (III) and alkane (II) with an organic acid (IV) in an esterification zone to obtain a product mixture d comprising the corresponding alkyl ester (V) of the organic acid and the unconverted alkane (II); E) removing from product mixture d a gas stream e1 which comprises an alkane (II) and is recycled into the dehydrogenation zone if appropriate, and a product mixture e2 comprising the alkyl ester; F) reacting the product mixture e2 comprising the alkyl ester with water in an ester hydrolysis zone to give a product mixture f comprising the alkanol (I) and the organic acid (IV); G) removing the alkanol (I) and the organic acid (IV) from product mixture f and, if appropriate, recycling the organic acid into the esterification zone.
摘要翻译：从选自丙烷和正丁烷的相应的烷烃（II）制备选自异丙醇和2-丁醇的链烷醇（I）的方法，包括以下步骤：A）提供起始气流 a包含烷烃（II）; B）将包含烷烃（II）的起始气体流（a）进料到脱氢区中并使烷烃（II）脱氢至烯烃（III），得到包含烯烃（III）和未转化烷烃的产物气流b （II），有或没有高锅炉，蒸汽，氢气和低锅炉; C）至少压缩产物气流b，任选地将产物气流b分离成水相c1，包含烯烃（III）和烷烃（II）的阶段c2，具有或不具有高锅炉，以及气相c3，其包含氢和低锅炉; D）使产物气流b或包含烯烃（III）和烷烃（II）的相c与酯化区中的有机酸（IV）反应，得到包含相应的有机酸烷基酯（V）的产物混合物d 和未转化的烷烃（II）; E）从产物混合物d除去包含烷烃（II）的气流e1，并且如果合适的话再循环到脱氢区中，以及包含烷基酯的产物混合物e2; F）在酯水解区中使包含烷基酯的产物混合物e2与水反应，得到包含链烷醇（I）和有机酸（IV）的产物混合物f; G）从产物混合物f中除去链烷醇（I）和有机酸（IV），如果合适，将有机酸再循环到酯化区。

4. 发明授权

US07556489B2 Guiding of a cut-open parison 失效
标题翻译：指导一个切开的型坯
公开(公告)号：US07556489B2
公开(公告)日：2009-07-07
申请号：US10520537
申请日：2003-07-09
申请人： Wolfgang Rohde , Jörg Meyer , Rainer Sattel , Jörg Schnorr , Bernhard Springholz , Roger Weinlein , Andreas Wüst
发明人： Wolfgang Rohde , Jörg Meyer , Rainer Sattel , Jörg Schnorr , Bernhard Springholz , Roger Weinlein , Andreas Wüst
IPC分类号： B28B11/14
CPC分类号： B29C49/42 , B29C47/0023 , B29C47/0026 , B29C47/0054 , B29C47/0066 , B29C49/0047 , B29C49/0073 , B29C49/04 , B29C49/4247 , B29C2793/0063 , B29C2793/0081 , B29K2995/0082
摘要： The invention relates to a device for partitioning the plastic parisons to give at least one semifinished open-surface product (6), where the device encompasses at least one means of partitioning (3) the plastic parison and one means of drive (2). The means of drive may be composed of one, but preferably of two, driven rolls. It has been found that use of the device of the invention can reduce or prevent the production of creasing and irregularity at the margins, i.e. at the cut edges, of the partitioned parisons, i.e. of the resultant semifinished sheets.
摘要翻译：本发明涉及一种用于分隔塑料型坯以提供至少一种半成品的开放式表面产品（6）的装置，其中该装置包括至少一种分隔（3）塑料型坯和一种驱动装置（2）的装置。驱动装置可由一个驱动辊组成，但优选由两个驱动辊组成。已经发现，使用本发明的装置可以减少或防止在分割的型坯，即所得的半成品片材的边缘，即在切割边缘处产生褶皱和不规则性。

5. 再颁专利

USRE40140E1 Polymerization catalyst used for producing polyolefins that have excellent combined properties 有权
标题翻译：用于生产具有优异组合性能的聚烯烃的聚合催化剂
公开(公告)号：USRE40140E1
公开(公告)日：2008-03-04
申请号：US11541519
申请日：2001-05-14
申请人： Shahram Mihan , Martin Lux , Wolfgang Rohde , Andreas Deckers , Peter Kölle , Heinz Vogt
发明人： Shahram Mihan , Martin Lux , Wolfgang Rohde , Andreas Deckers , Peter Kölle , Heinz Vogt
IPC分类号： B01J27/06 , B01J21/08 , B01J35/08 , B01J13/00 , C01B33/12
CPC分类号： C08F10/02 , C08F4/24
摘要： The invention relates to a process for preparing a catalyst for the polymerization of olefins, which comprises: a) preparation of a finely divided silica xerogel, b) loading of the xerogel with chromium from a solution of chromium trioxide or a chromium compound which is converted into chromium trioxide under the conditions of step c), and c) activation of the resulting product at from 400 to 1100° C. in a water-free gas stream comprising oxygen in a concentration of above 10% by volume, wherein a fluoride doping with a fluorinating agent is carried out in step b) or in step c). Furthermore, the invention relates to a catalyst for the polymerization of olefins which is obtainable by the process of the invention and to a process for the polymerization of olefins in which an olefin or an olefin mixture is polymerized in the presence of a catalyst according to the invention.
摘要翻译：本发明涉及一种制备烯烃聚合催化剂的方法，该方法包括：a）制备细碎的二氧化硅干凝胶，b）用铬从三氧化铬溶液或铬化合物的溶液中加载干凝胶，在步骤c）的条件下转化为三氧化铬，和c）在含有浓度高于10体积％的氧的无水气流中，在400至1100℃下活化所得产物，其中氟化物掺杂在步骤b）或步骤c）中进行氟化剂。此外，本发明涉及可通过本发明的方法获得的烯烃聚合催化剂和烯烃聚合方法，其中烯烃或烯烃混合物在催化剂存在下聚合，根据发明。

6. 发明授权

US07059163B2 Roll stand comprising a crown-variable-control (CVC) roll pair 有权
标题翻译：辊架包括冠状变量控制（CVC）辊对
公开(公告)号：US07059163B2
公开(公告)日：2006-06-13
申请号：US10344054
申请日：2001-07-25
申请人： Hans Georg Hartung , Klaus Klamma , Wolfgang Rohde , Jürgen Seidel
发明人： Hans Georg Hartung , Klaus Klamma , Wolfgang Rohde , Jürgen Seidel
IPC分类号： B21B39/20
CPC分类号： B21B27/02 , B21B13/142
摘要： The invention relates to a roll stand comprising a crown-variable-control (CVC) roll pair, preferably a CVC working roll pair and a back-up roll pair, which comprise a contact area (B cont) in which a horizontally active torque (M) acts that leads to a twisting of the rolls and thus to axial forces in the roll bearings. In order to keep the axial forces in the roll bearings as small as possible, the torque (M) is minimized by an appropriate CVC grinding.
摘要翻译：本发明涉及一种辊架，其包括冠状可变控制（CVC）辊对，优选CVC工作辊对和支撑辊对，其包括接触区域（B cont），其中水平有效转矩（ M）作用导致辊的扭转，从而导致滚动轴承中的轴向力。为了保持滚动轴承中的轴向力尽可能小，通过适当的CVC磨削使扭矩（M）最小化。

7. 发明申请

US20060122340A1 Selection of polymerization catalysts and apparatus for carrying this out 失效
标题翻译：聚合催化剂的选择和携带这一点的装置
公开(公告)号：US20060122340A1
公开(公告)日：2006-06-08
申请号：US10528268
申请日：2003-09-16
申请人： Wolfgang Rohde , Marc Kristen , Dieter Lilge
发明人： Wolfgang Rohde , Marc Kristen , Dieter Lilge
IPC分类号： C08G85/00 , B01J19/00
CPC分类号： C40B40/18 , B01J8/1836 , B01J19/0013 , B01J19/0046 , B01J31/143 , B01J31/2295 , B01J2208/00061 , B01J2208/00203 , B01J2219/00283 , B01J2219/00286 , B01J2219/00306 , B01J2219/00333 , B01J2219/00353 , B01J2219/00367 , B01J2219/00423 , B01J2219/00493 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00698 , B01J2219/00722 , B01J2219/00745 , B01J2219/00747 , C08F10/00 , C40B30/08 , C40B40/14 , C40B60/14 , C08F4/24 , C08F4/69
摘要： In a method of selecting polymerization catalysts, in particular Phillips catalysts for the polymerization of olefins, from a multiplicity of catalysts on the basis of their catalytic properties, a multiplicity of catalyst precursors or catalyst supports are converted in parallel into polymerization catalysts in a pretreatment step in an array of reactors, where the pretreatment comprises at least one thermal treatment step at from 250 to 1200° C. Furthermore, at least one starting material is converted with the aid of the respective polymerization catalysts under prescribed polymerization conditions into at least one polymer product in a polymerization step and, finally, analysis of the polymer product or products is carried out to determine its composition and/or chosen properties. This makes it possible to carry out a thermal pretreatment of polymerization catalysts quickly under defined conditions which can be varied.
摘要翻译：在选择聚合催化剂，特别是用于烯烃聚合的菲利普斯催化剂的方法中，从多种催化剂的催化性能基础上选择多个催化剂前体或催化剂载体在预处理步骤中并行转化为聚合催化剂在一系列反应器中，其中预处理包括在250-1200℃下的至少一个热处理步骤。此外，在规定的聚合条件下，将至少一种起始原料借助于相应的聚合催化剂转化成至少一种聚合物产物在聚合步骤中，最后进行聚合物产物的分析以确定其组成和/或所选择的性质。这使得可以在可以改变的限定条件下快速进行聚合催化剂的热预处理。

8. 发明授权

US06548580B1 Use of sterically hindered amines or stabilised ethylene polymers in the production of plastic bodies for storage and transport of vegetable oil esters 有权
标题翻译：在制造用于储存和运输植物油酯的塑料体中使用空间位阻胺或稳定的乙烯聚合物
公开(公告)号：US06548580B1
公开(公告)日：2003-04-15
申请号：US09555873
申请日：2000-06-08
申请人： Wolfgang Rohde , Laurent Deloux
发明人： Wolfgang Rohde , Laurent Deloux
IPC分类号： C08K534
CPC分类号： C08K5/3435 , C08L23/04
摘要： Ethylene homo- and copolymers stabilized by sterically hindered amines or by N-hydroxy or N-oxyl derivatives are used to produce articles of plastic and components for the storage and transport of vegetable oil esters.
摘要翻译：通过空间位阻胺或N-羟基或N-氧基衍生物稳定的乙烯均聚物和共聚物用于生产塑料制品和用于储存和运输植物油酯的成分。

9. 发明授权

US06180731B2 Polymerisates of ethylene with a high degree of resistance to stress crack, and a catalyst system for the production thereof 失效
标题翻译：具有高抗应力裂纹性的乙烯的聚合物，以及用于制备它的催化剂体系
公开(公告)号：US06180731B2
公开(公告)日：2001-01-30
申请号：US09000011
申请日：1997-01-22
申请人： Wolfgang Rohde , Roland Saive , Dieter Lilge , Martin Lux , Peter Bauer
发明人： Wolfgang Rohde , Roland Saive , Dieter Lilge , Martin Lux , Peter Bauer
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F4/61904 , C08F4/61912 , C08F4/61925 , C08F210/16 , Y10S526/943 , C08F210/14 , C08F2500/13 , C08F2500/12 , C08F2500/07 , C08F2500/26 , C08F4/63904 , C08F4/69
摘要： Polymers of ethylene are obtainable by polymerization of ethylene and, if desired, further comonomers in the presence of a catalyst system comprising as active constituents I) a Phillips catalyst, II) a solid which is different from I) and comprises a component which is derived from the metallocene complexes of the formula (A) in which the substituents and indices have the following meanings: R1 to R10 are hydrogen, C1-C10-alkyl, 5-to 7-membered cycloalkyl which may in turn bear C1-C6-alkyl groups as substituents, C6-C15-aryl or aryalkyl, where two adjacent radicals may also together form a cyclic group having from 4 to 15 carbon atoms, or Si(R11)3, where R11 is C1-C10-alkyl, C6-C15-aryl or C3-C10-cycloalkyl, or the radicals R4 and R9 together form a group —[Y(R12R13)]m—, where Y is silicon, germanium, tin or carbon, and R12, R13 are hydrogen C1-C10-alky, C3-C10-cycloalyl or C6-C15-aryl, M is a metal of transition groups IV to VIII or a metal of the lanthanide series, Z1, Z2 are fluorine, chlorine, bromine, iodine, hydrogen, C1-C20-alkyl or aryl, —OR14, —OOCR14, where R14 is hydrogen or C1-C20-alkyl; R15 is C1-C20-alkyl; m is 1,2,3 or 4; n is 0, or 2; r is 0, 1 or 2; the sum n+r is likewise 0, 1 or 2, and, if desired, III) an organometallic component selected from groups IA, IIA, IIB and IIIA of the Periodic Table of the Elements.
摘要翻译：乙烯的聚合物可以通过在包含作为活性成分的催化剂体系的存在下乙烯和如果需要的情况下进一步的共聚单体获得。I）菲利普斯催化剂，II）与I）不同的固体，并且包含衍生自式（A）的金属茂络合物，其中取代基和指数具有以下含义：R 1至R 10是氢，C 1 -C 10 - 烷基，5-至7-元环烷基，其也可以含有C 1 -C 6 - 烷基作为取代基，其中两个相邻基团也可以一起形成具有4至15个碳原子的环状基团的C 6 -C 15 - 芳基或芳烷基，或其中R 11是C 1 -C 10 - 烷基，C 6 -C 15 - 芳基或C 3 -C 10 - 环烷基，或基团R 4和R 9一起形成 - [Y（R 12 R 13）] m - 基团，其中Y是硅，锗，锡或碳，R 12，R 13是氢C1-C10-烷基 C 3 -C 10 - 环烷基或C 6 -C 15 - 芳基，M为Ⅳ〜Ⅷ族金属或镧系金属，Z 1，Z 2为氟，氯，溴，碘，氢，C 1 -C 20烷基或芳基，-OR 14，-OOCR 14，其中R 14是氢或C 1 -C 20烷基; R 15是C 1 -C 20 - 烷基; m为1,2,3或4; n为0或2; r为0,1或2; 总和n + r同样为0,1或2，如果需要，III）选自元素周期表的IA，IIA，IIB和IIIA族的有机金属组分。

10. 发明授权

US5771731A Hot strip production plant for ferritic rolling and method of producing ferritic rolled strip 失效
标题翻译：用于铁素体轧制的热轧板生产设备和生产铁素体轧制钢带的方法
公开(公告)号：US5771731A
公开(公告)日：1998-06-30
申请号：US704005
申请日：1996-08-22
申请人： Wolfgang Rohde , Manfred Albedyhl
发明人： Wolfgang Rohde , Manfred Albedyhl
IPC分类号： B21B27/02 , B21B1/26 , B21B1/28 , B21B1/46 , B21B13/14 , C21D9/52 , B21B27/06 , B21B1/00
CPC分类号： B21B1/26 , B21B1/28 , B21B1/466 , B21B2201/04
摘要： A production plant for producing hot-rolled flat products includes a rolling train composed of a plurality of roll stands, a run-out table with devices for cooling the hot strip, and subsequently arranged coiling machines for coiling the strip. A compact deformation stage in the form of a rolling train with one to four roll stands is arranged following the reeling unit of a conventionally constructed hot-rolled wide strip train. This rolling train is specifically constructed for the deformation in the ferritic range.
摘要翻译：用于生产热轧扁平产品的生产设备包括由多个辊架组成的轧制组，具有用于冷却热轧带材的装置的排出台，以及随后布置的用于卷绕带材的卷取机。按照常规构造的热轧宽带系列的卷取单元布置具有一至四个辊架的轧制机形式的紧凑变形阶段。该轧制列车是专门为铁素体系变形而构造的。

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