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1. 发明授权

US06387314B1 Process for increasing the flame resistance of polyethylene-containing hollowware 失效
标题翻译：提高含聚乙烯的中空件的阻燃性能的方法
公开(公告)号：US06387314B1
公开(公告)日：2002-05-14
申请号：US09456524
申请日：1999-12-08
申请人： Wolfgang Rohde , Günther Pfirrmann , Peter Bauer , Andreas Haufe , Joachim Koch
发明人： Wolfgang Rohde , Günther Pfirrmann , Peter Bauer , Andreas Haufe , Joachim Koch
IPC分类号： B29C7102
CPC分类号： B32B27/08 , B29C49/0005 , B29C71/02 , B29L2031/7172 , B32B1/02 , B32B27/32 , B32B2307/3065 , B32B2323/04 , B32B2439/00
摘要： A process for increasing the flame resistance of polyethylene-containing, single- or multilayer hollowware, in particular plastic fuel tanks, by heat treating the hollowware at 60-135° C.
摘要翻译：一种通过在60-135℃热处理中空件来提高含聚乙烯，单层或多层中空器件，特别是塑料燃料箱的阻燃性能的方法。

2. 发明授权

US06855388B2 Blow moulded containers and moulded parts consisting of synthetic material and having improved antistatic properties 失效
标题翻译：吹塑容器和由合成材料组成的成型部件，具有改进的抗静电性能
公开(公告)号：US06855388B2
公开(公告)日：2005-02-15
申请号：US10221846
申请日：2001-03-07
申请人： Bernhard Springlholz , Wolfgang Rohde , Andreas Haufe
发明人： Bernhard Springlholz , Wolfgang Rohde , Andreas Haufe
IPC分类号： B29C49/00 , B29C49/04 , B29C49/20 , B29C49/26 , B29K105/22 , B29L31/30 , B65D25/38 , B65D90/46 , B29D22/00 , B29D23/00 , B32B1/08
CPC分类号： B29C49/0078 , B29B2911/1434 , B29C49/04 , B29K2995/0013 , B60K2015/03401 , B65D25/385 , B65D90/46 , Y10T428/1352 , Y10T428/1362 , Y10T428/24124 , Y10T428/24174 , Y10T428/24994 , Y10T428/249942 , Y10T428/31855
摘要： The present invention relates to plastic containers or moldings which have been produced by blow molding and have improved antistatic properties. The containers or moldings have an outer wall and an inner wall and contain webs of electrically conducting material running along the inner wall. The invention also relates to a process for the production of the containers or moldings and to their use.
摘要翻译：本发明涉及通过吹塑生产并具有改进的抗静电性能的塑料容器或模制品。容器或模制品具有外壁和内壁，并且包含沿着内壁延伸的导电材料的腹板。本发明还涉及用于生产容器或模制品及其用途的方法。

3. 发明申请

US20060063666A1 Supported chromium catalyst and its use for preparing homopolymers and copolymers of ethylene 有权
标题翻译：负载型铬催化剂及其制备乙烯均聚物和共聚物的用途
公开(公告)号：US20060063666A1
公开(公告)日：2006-03-23
申请号：US10538536
申请日：2003-12-09
申请人： Wolfgang Rohde , Guido Funk , Andreas Haufe , Anke Bold , Neil Nadalin
发明人： Wolfgang Rohde , Guido Funk , Andreas Haufe , Anke Bold , Neil Nadalin
IPC分类号： B01J23/26
CPC分类号： C08F210/16 , C08F4/24 , C08F210/14 , C08F2500/18 , C08F2500/12 , C08F2500/07 , C08F2500/04 , C08F2500/13
摘要： Process for preparing supported, titanized chromium catalysts, which comprises the following steps: A) bringing a support material into contact with a protic medium comprising a titanium compound and a chromium compound, B) optionally removing the solvent, C) optionally calcining the precatalyst obtained after step B) and D) optionally activating the precatalyst obtained after step B) or C) in an oxygen-containing atmosphere at from 400° C. to 1100° C.
摘要翻译：制备负载的钛化铬催化剂的方法，其包括以下步骤：A）使载体材料与包含钛化合物和铬化合物的质子介质接触，B）任选除去溶剂，C）任选地煅烧所获得的预催化剂在步骤B）和D）之后，任选地在步骤B）或C）中在400℃至1100℃的含氧气氛中活化预催化剂。

4. 发明授权

US07803736B2 Supported chromium catalyst and its use for preparing homopolymers and copolymers of ethylene 有权
标题翻译：负载型铬催化剂及其制备乙烯均聚物和共聚物的用途
公开(公告)号：US07803736B2
公开(公告)日：2010-09-28
申请号：US10538536
申请日：2003-12-09
申请人： Wolfgang Rohde , Guido Funk , Andreas Haufe , Anke Bold , Neil Nadalin
发明人： Wolfgang Rohde , Guido Funk , Andreas Haufe , Anke Bold , Neil Nadalin
IPC分类号： B01J23/00 , B01J21/00 , B01J20/00
CPC分类号： C08F210/16 , C08F4/24 , C08F210/14 , C08F2500/18 , C08F2500/12 , C08F2500/07 , C08F2500/04 , C08F2500/13
摘要： A process for preparing supported, titanized chromium catalysts is disclosed. The process comprises A) bringing a support material into contact with a protic medium comprising a titanium compound and a chromium compound; B) optionally removing the solvent; C) optionally calcining the precatalyst obtained after step B); and D) optionally activating the precatalyst obtained after step B) or C) in an oxygen-containing atmosphere at from 400° C. to 1100° C.
摘要翻译：公开了制备负载的钛化铬催化剂的方法。该方法包括：A）使载体材料与包含钛化合物和铬化合物的质子介质接触; B）任选地除去溶剂; C）任选地煅烧在步骤B）之后获得的预催化剂; 和D）任选地在步骤B）或C）中在400℃至1100℃的含氧气氛中活化预催化剂。

5. 发明授权

US06180731B2 Polymerisates of ethylene with a high degree of resistance to stress crack, and a catalyst system for the production thereof 失效
标题翻译：具有高抗应力裂纹性的乙烯的聚合物，以及用于制备它的催化剂体系
公开(公告)号：US06180731B2
公开(公告)日：2001-01-30
申请号：US09000011
申请日：1997-01-22
申请人： Wolfgang Rohde , Roland Saive , Dieter Lilge , Martin Lux , Peter Bauer
发明人： Wolfgang Rohde , Roland Saive , Dieter Lilge , Martin Lux , Peter Bauer
IPC分类号： C08F442
CPC分类号： C08F10/00 , C08F4/61904 , C08F4/61912 , C08F4/61925 , C08F210/16 , Y10S526/943 , C08F210/14 , C08F2500/13 , C08F2500/12 , C08F2500/07 , C08F2500/26 , C08F4/63904 , C08F4/69
摘要： Polymers of ethylene are obtainable by polymerization of ethylene and, if desired, further comonomers in the presence of a catalyst system comprising as active constituents I) a Phillips catalyst, II) a solid which is different from I) and comprises a component which is derived from the metallocene complexes of the formula (A) in which the substituents and indices have the following meanings: R1 to R10 are hydrogen, C1-C10-alkyl, 5-to 7-membered cycloalkyl which may in turn bear C1-C6-alkyl groups as substituents, C6-C15-aryl or aryalkyl, where two adjacent radicals may also together form a cyclic group having from 4 to 15 carbon atoms, or Si(R11)3, where R11 is C1-C10-alkyl, C6-C15-aryl or C3-C10-cycloalkyl, or the radicals R4 and R9 together form a group —[Y(R12R13)]m—, where Y is silicon, germanium, tin or carbon, and R12, R13 are hydrogen C1-C10-alky, C3-C10-cycloalyl or C6-C15-aryl, M is a metal of transition groups IV to VIII or a metal of the lanthanide series, Z1, Z2 are fluorine, chlorine, bromine, iodine, hydrogen, C1-C20-alkyl or aryl, —OR14, —OOCR14, where R14 is hydrogen or C1-C20-alkyl; R15 is C1-C20-alkyl; m is 1,2,3 or 4; n is 0, or 2; r is 0, 1 or 2; the sum n+r is likewise 0, 1 or 2, and, if desired, III) an organometallic component selected from groups IA, IIA, IIB and IIIA of the Periodic Table of the Elements.
摘要翻译：乙烯的聚合物可以通过在包含作为活性成分的催化剂体系的存在下乙烯和如果需要的情况下进一步的共聚单体获得。I）菲利普斯催化剂，II）与I）不同的固体，并且包含衍生自式（A）的金属茂络合物，其中取代基和指数具有以下含义：R 1至R 10是氢，C 1 -C 10 - 烷基，5-至7-元环烷基，其也可以含有C 1 -C 6 - 烷基作为取代基，其中两个相邻基团也可以一起形成具有4至15个碳原子的环状基团的C 6 -C 15 - 芳基或芳烷基，或其中R 11是C 1 -C 10 - 烷基，C 6 -C 15 - 芳基或C 3 -C 10 - 环烷基，或基团R 4和R 9一起形成 - [Y（R 12 R 13）] m - 基团，其中Y是硅，锗，锡或碳，R 12，R 13是氢C1-C10-烷基 C 3 -C 10 - 环烷基或C 6 -C 15 - 芳基，M为Ⅳ〜Ⅷ族金属或镧系金属，Z 1，Z 2为氟，氯，溴，碘，氢，C 1 -C 20烷基或芳基，-OR 14，-OOCR 14，其中R 14是氢或C 1 -C 20烷基; R 15是C 1 -C 20 - 烷基; m为1,2,3或4; n为0或2; r为0,1或2; 总和n + r同样为0,1或2，如果需要，III）选自元素周期表的IA，IIA，IIB和IIIA族的有机金属组分。

6. 发明授权

US06462135B1 Low-odor polyethylene blends 失效
标题翻译：低气味聚乙烯混合物
公开(公告)号：US06462135B1
公开(公告)日：2002-10-08
申请号：US09743923
申请日：2001-01-17
申请人： Wolfgang Rohde , Peter Bauer , Dieter Lilge , Martin Lux , Paulus de Lange , Guido Funk
发明人： Wolfgang Rohde , Peter Bauer , Dieter Lilge , Martin Lux , Paulus de Lange , Guido Funk
IPC分类号： C08L2300
CPC分类号： C08L23/06 , C08L23/0815 , C08L2314/04 , Y10T428/1352 , Y10T428/31855 , C08L2666/04
摘要： In a low-odor polyethylene blend made from a high-molecular-weight ethylene copolymer obtainable by polymerization in the presence of a Ziegler catalyst and from a low-molecular-weight ethylene homopolymer or ethylene copolymer obtainable by polymerization in the presence of a chromocene catalyst on an oxidic support, the Al content of the high-molecular-weight component is from 5 to 60 mg/kg, the Al content of the low-molecular-weight component is from 0 to 5 mg/kg and the Al content of the blend is from 1 to 55 mg/kg. Processes are described for preparing blends of this type. Their use is described for producing moldings, in particular hollow articles and pipes. Moldings, in particular hollow articles and pipes, are produced from low-odor polyethylene blends.
摘要翻译：在由可在齐格勒催化剂存在下聚合得到的高分子量乙烯共聚物和可通过在色烯催化剂存在下聚合得到的低分子量乙烯均聚物或乙烯共聚物制成的低气味聚乙烯共混物在氧化载体上，高分子量成分的Al含量为5〜60mg / kg，低分子量成分的Al含量为0〜5mg / kg，Al 共混物为1至55mg / kg。描述了制备这种类型的共混物的方法。它们的用途描述用于生产模制品，特别是中空制品和管道。木制品，特别是中空制品和管道，由低气味聚乙烯混合物制成。

7. 发明申请

US20120253005A1 CONDITIONING OF DOUBLE METAL CYANIDE CATALYSTS 有权
标题翻译：双金属氰化物催化剂的调节
公开(公告)号：US20120253005A1
公开(公告)日：2012-10-04
申请号：US13502816
申请日：2010-10-01
申请人： Igor Shishkov , Sirus Zarbakhsh , Ronald Adelmann , Wolfgang Rohde , Achim Loeffler
发明人： Igor Shishkov , Sirus Zarbakhsh , Ronald Adelmann , Wolfgang Rohde , Achim Loeffler
IPC分类号： B01J37/08 , C08G59/68 , C08G59/00 , B01J27/26 , C08G63/83
CPC分类号： B01J27/26 , B01J37/10 , C08G65/2609 , C08G65/2663
摘要： The invention relates to a method for conditioning double metal catalysts which are used in the production of polyether polyols. The conditioning enhances the performance of the catalyst, so that lower concentrations of the DMC catalyst can be used in polyether polyol production.
摘要翻译：本发明涉及一种用于制备聚醚多元醇的双金属催化剂的调理方法。该调节提高了催化剂的性能，使得DMC催化剂的较低浓度可用于聚醚多元醇生产。

8. 发明授权

US07737230B2 NMR method of determining and regulating the composition of polymer mixtures in polymerization 有权
标题翻译：确定和调节聚合物中聚合物混合物组成的NMR方法
公开(公告)号：US07737230B2
公开(公告)日：2010-06-15
申请号：US11629542
申请日：2005-06-09
申请人： Shahram Mihan , Dieter Lilge , Wolfgang Rohde
发明人： Shahram Mihan , Dieter Lilge , Wolfgang Rohde
IPC分类号： C08F2/00 , C08F210/00
CPC分类号： G01N24/08 , C08F10/02 , C08F110/02 , C08F210/16 , C08F2400/02 , G01N24/085 , G01R33/44 , Y02P20/125 , C08F2/00
摘要： Method of determining the composition of polymer mixtures comprising defined polymer components of differing mean molar masses Mn, which comprises the steps (a) recording of at least one 1H-NMR relaxation curve of the polymer mixture and (b) calculating the proportions of the polymer components by matching the measured relaxation curve with the relaxation curves of the individual polymer components. In this way, the composition of polymer mixtures can be determined quickly and simply. Furthermore, process integration for regulating the polymerization is possible.
摘要翻译：确定包含不同平均摩尔质量Mn的限定的聚合物组分的聚合物混合物的组成的方法，其包括步骤（a）记录聚合物混合物的至少一个1H-NMR松弛曲线，和（b）计算聚合物的比例通过将测量的松弛曲线与各个聚合物组分的松弛曲线相匹配来获得组分。以这种方式，可以快速且简单地确定聚合物混合物的组成。此外，用于调节聚合的方法集成是可能的。

9. 发明授权

US07468279B2 Selection of polymerization catalysts and apparatus for carrying this out 失效
标题翻译：聚合催化剂的选择和携带这一点的装置
公开(公告)号：US07468279B2
公开(公告)日：2008-12-23
申请号：US10528268
申请日：2003-09-16
申请人： Wolfgang Rohde , Marc Oliver Kristen , Dieter Lilge
发明人： Wolfgang Rohde , Marc Oliver Kristen , Dieter Lilge
IPC分类号： G01N31/10 , C40B30/10 , B01J19/24
CPC分类号： C40B40/18 , B01J8/1836 , B01J19/0013 , B01J19/0046 , B01J31/143 , B01J31/2295 , B01J2208/00061 , B01J2208/00203 , B01J2219/00283 , B01J2219/00286 , B01J2219/00306 , B01J2219/00333 , B01J2219/00353 , B01J2219/00367 , B01J2219/00423 , B01J2219/00493 , B01J2219/00495 , B01J2219/00585 , B01J2219/00596 , B01J2219/00698 , B01J2219/00722 , B01J2219/00745 , B01J2219/00747 , C08F10/00 , C40B30/08 , C40B40/14 , C40B60/14 , C08F4/24 , C08F4/69
摘要： In a method of selecting polymerization catalysts, in particular Phillips catalysts for the polymerization of olefins, from a multiplicity of catalysts on the basis of their catalytic properties, a multiplicity of catalyst precursors or catalyst supports are converted in parallel into polymerization catalysts in a pretreatment step in an array of reactors, where the pretreatment comprises at least one thermal treatment step at from 250 to 1200° C. Furthermore, at least one starting material is converted with the aid of the respective polymerization catalysts under prescribed polymerization conditions into at least one polymer product in a polymerization step and, finally, analysis of the polymer product or products is carried out to determine its composition and/or chosen properties. This makes it possible to carry out a thermal pretreatment of polymerization catalysts quickly under defined conditions which can be varied.
摘要翻译：在选择聚合催化剂，特别是用于烯烃聚合的菲利普斯催化剂的方法中，从多种催化剂的催化性能基础上选择多个催化剂前体或催化剂载体在预处理步骤中并行转化为聚合催化剂在一系列反应器中，其中预处理包括在250-1200℃下的至少一个热处理步骤。此外，在规定的聚合条件下，将至少一种起始原料借助于相应的聚合催化剂转化成至少一种聚合物产物在聚合步骤中，最后进行聚合物产物的分析以确定其组成和/或所选择的性质。这使得可以在可以改变的限定条件下快速进行聚合催化剂的热预处理。

10. 发明申请

US20070240475A1 Method and Roll Stand for Multiply Influencing Profiles 有权
标题翻译：多重影响型材的方法和轧辊架
公开(公告)号：US20070240475A1
公开(公告)日：2007-10-18
申请号：US10584173
申请日：2004-11-22
申请人： Günter Kneppe , Wolfgang Rohde , Sabine Rohde
发明人： Günter Kneppe , Wolfgang Rohde , Sabine Rohde
IPC分类号： B21B41/04
CPC分类号： B21B13/142 , B21B13/147 , B21B27/021 , B21B37/40 , B21B2013/025 , B21B2013/028
摘要： When rolling sheets or strips in roll stands using working rolls, which are supported on back-up rolls or on intermediate rolls having back-up rolls, whereby the setting of the roll gap is effected by axially displacing roll pairs provided with curved contours, differences from the required profile occur in the instance of larger widths of a product range due to excessive extensions in the edge areas or in the quarter areas that are manifested in the form of so-called quarter waves in the flatness of the product. In order to rectify this problem by using a simple mechanism and to improve the setting mechanism and the strategy for creating absolutely planar strips with a predetermined thickness profile over the entire width of the rolling stock, the invention provides that for forming the roll gap set profiles (10, 11) for two selected displacing positions, the contours of the rolls of one roll pair are shaped in such a manner that they produce, in the roll gap, a profile (20, 21), which is symmetric with regard to the center of the roll and which has a profile maximum in the center of the roll that can be altered by displacing the rolls, whereas the contours of the rolls of at least one second roll pair produce, in the roll gap, a profile (22, 23), which is symmetric with regard to the center of the roll and which has two identical maxima outside of the center of the roll that can be altered by displacing the rolls.
摘要翻译：当在辊架上轧制板材或条带时，其使用工作辊，其被支撑在备用辊上或具有支撑辊的中间辊上，由此辊间隙的设定通过轴向移位设置有弯曲轮廓的辊对来实现，差异在产品范围较宽的情况下，由于在产品平面度上以所谓的四分之一波浪的形式表现的边缘区域或四分之一区域中的过度扩展，所以要求的分布发生。为了通过使用简单的机构来解决这个问题，并且改进了在机车车辆的整个宽度上制造具有预定厚度轮廓的绝对平面条带的设定机构和策略，本发明提供了用于形成辊隙组合轮廓（10,11），对于两个选定的位移位置，一个辊对的辊的轮廓成形为使得它们在辊隙中产生轮廓（20,21），轮廓（20,21）关于辊的中心具有在辊的中心最大的轮廓，该轮廓可以通过移动辊而改变，而至少一个第二辊对的辊的轮廓在辊间隙中产生轮廓（22， 23），其对于辊的中心是对称的，并且在辊的中心之外具有两个相同的最大值，该最大值可以通过移动辊而改变。

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