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1. 发明授权

US4373080A Polyisocyanates, preparation and use thereof 失效
标题翻译：聚异氰酸酯，其制备和用途
公开(公告)号：US4373080A
公开(公告)日：1983-02-08
申请号：US105356
申请日：1979-12-19
申请人： Wolfgang Reichmann , Klaus Konig , Manfred Schonfelder
发明人： Wolfgang Reichmann , Klaus Konig , Manfred Schonfelder
IPC分类号： C08G18/00 , C07C67/00 , C07C239/00 , C07C275/62 , C08G18/78 , C08G18/80 , C07C127/24
CPC分类号： C08G18/7831 , C07C275/62 , C08G18/7818 , C08G18/8038 , Y02P20/582
摘要： The present invention relates to a process for the production of specific polyisocyanates by reacting diamines containing hydrogen atoms which are active in the context of the isocyanate addition reaction with excess quantities of organic diisocyanates. The invention also relates to a modification of the above process characterized in that the diamines are reacted first with excess quantities of a first diisocyanate after which the thus obtained reaction product which contains a urea group and a biuret group is reacted in a second stage with a second diisocyanate. The invention also relates to the use of polyisocyanates as the isocyanate component in the production of polyurethane plastics by the isocyanate-polyaddition process.
摘要翻译：本发明涉及通过使异氰酸酯加成反应中有活性的含有氢原子的二胺与过量的有机二异氰酸酯反应制备特定的多异氰酸酯的方法。本发明还涉及上述方法的改进，其特征在于二胺首先与过量的第一种二异氰酸酯反应，然后将由此得到的包含脲基和缩二脲基的反应产物在第二阶段与第二异氰酸酯。本发明还涉及通过异氰酸酯加聚方法在聚氨酯塑料生产中使用多异氰酸酯作为异氰酸酯组分。

2. 发明授权

US4340712A Process for the preparation of polyisocyanates containing biuret and/or higher polyuret groups and use thereof as synthesis component in the preparation of polyurethane plastics 失效
标题翻译：制备含有缩二脲和/或更高级聚脲基团的多异氰酸酯的方法及其在制备聚氨酯塑料中作为合成成分的用途
公开(公告)号：US4340712A
公开(公告)日：1982-07-20
申请号：US105368
申请日：1979-12-19
申请人： Wolfgang Reichmann , Klaus Konig , Manfred Schonfelder
发明人： Wolfgang Reichmann , Klaus Konig , Manfred Schonfelder
IPC分类号： C08G18/00 , C07C273/18 , C07C275/62 , C08G18/78 , C08G18/80 , C07C127/22
CPC分类号： C08G18/8038 , C07C273/1827 , C08G18/7818 , C08G18/7831 , Y02P20/582
摘要： A process for the preparation of polyisocyanates containing biuret and/or higher polyuret groups by reacting secondary diamines with diisocyanates characterized in that the reaction is carried out in the presence of catalytic quantities of strong acids which form mixed carbamic acid anhydrides with isocyanates. Alternatively, the secondary diamines may be reacted with organic diisocyanates in the absence of catalysts to form a urea diisocyanate which is then reacted in the presence of catalytic quantities of strong acids which form mixed carbamic acid anhydrides either with the same diisocyanate used in the first step or a second diisocyanate. The invention also relates to the polyisocyanates containing biuret and/or higher polyuret groups obtainable by this process.
摘要翻译：通过使仲二胺与二异氰酸酯反应制备含有缩二脲和/或更高级聚脲基团的多异氰酸酯的方法，其特征在于反应在催化量的形成混合氨基甲酸酐的强酸与异氰酸酯的存在下进行。或者，仲二胺可以在不存在催化剂的情况下与有机二异氰酸酯反应以形成脲二异氰酸酯，然后在催化量的强酸存在下反应，所述强酸形成混合的氨基甲酸酐，或者与第一步中使用的相同的二异氰酸酯或第二二异氰酸酯。本发明还涉及通过该方法可获得的含有缩二脲和/或更高级聚脲基团的多异氰酸酯。

3. 发明授权

US4338431A Process for the preparation of neopentyl glycol polyesters and co-polyesters 失效
标题翻译：新戊二醇聚酯和共聚酯的制备方法
公开(公告)号：US4338431A
公开(公告)日：1982-07-06
申请号：US122149
申请日：1980-02-15
申请人： Klaus Konig , Wolfgang Reichmann , Manfred Schonfelder
发明人： Klaus Konig , Wolfgang Reichmann , Manfred Schonfelder
IPC分类号： C08G18/00 , C08G18/42 , C08G63/16 , C08G63/18 , C08G63/181 , C08G63/78 , C09D167/00 , C09J167/00 , C08G63/22
CPC分类号： C08G63/78 , C08G63/16
摘要： The present invention relates to an improved process for the preparation of neopentyl glycol polyesters by reacting neopentyl glycol with carboxylic acids or derivatives thereof in the presence of minor amounts of glycols which boil at lower temperatures than neopentyl glycol. These low-boiling glycols obviate previous difficulties relating to the sublimation of neopentyl glycol. Thus, the present process offers safety advantages since neopentyl glycol does not crystallize in the reaction apparatus and also provides better control over the molecular ratio of acid groups to alcohol groups.
摘要翻译：本发明涉及通过新戊二醇与羧酸或其衍生物在少量二醇的存在下反应来制备新戊二醇聚酯的改进方法，所述二元醇在比新戊二醇低的温度下沸腾。这些低沸点乙二醇消除了以前关于新戊二醇升华的困难。因此，本方法提供安全性优点，因为新戊二醇在反应装置中不结晶，并且还提供对酸基与醇基的分子比的更好控制。

4. 发明授权

US6054528A Aqueous coating adhesive and sealant compositions containing oxadiazolinones and polyamines 失效
标题翻译：水性涂料粘合剂和含有恶二唑啉酮和多胺的密封剂组合物
公开(公告)号：US6054528A
公开(公告)日：2000-04-25
申请号：US118244
申请日：1998-07-17
申请人： Josef Pedain , Klaus Konig , Peter Heitkamper , Manfred Schonfelder
发明人： Josef Pedain , Klaus Konig , Peter Heitkamper , Manfred Schonfelder
IPC分类号： C08K5/17 , C07D271/10 , C07D271/113 , C08G73/02 , C08K5/353 , C08L101/00 , C09D5/00 , C09D7/12 , C09D179/02 , C09J11/06 , C09J179/02 , C08L75/00 , B32B27/08 , B32B27/26 , B32B27/40 , C08G73/00
CPC分类号： C07D271/113 , C08G73/0233 , C09D179/02 , C09J179/02 , Y10T428/31551
摘要： The present invention relates to aqueous compositions containinga) bis(1,3,4-oxadiazolin-5-ones) corresponding to formula (I) ##STR1## wherein R represents a single bond or a divalent aliphatic, araliphatic or aromatic radical having 1 to 18 carbon atoms andb) organic polyamines or polyamine blends having an average of more than 2 NH-- and/or NH.sub.2 -- groups.The present invention also relates to coatings, adhesives or sealants prepared from these aqueous compositions, in particular automotive clear coats.
摘要翻译：本发明涉及含有a）对应于式（I）的双（1,3,4-恶二唑啉-5-酮）的含水组合物，其中R表示单键或具有1至18个碳原子的二价脂族，芳脂族或芳族基团原子和b）平均具有多于2个NH-和/或NH 2 - 基团的有机多胺或多胺共混物。本发明还涉及由这些含水组合物，特别是汽车清漆制备的涂料，粘合剂或密封剂。

5. 发明授权

US4692384A Polyester polyols and their use as polyol component in two component polyurethane lacquers 失效
标题翻译：聚酯多元醇及其在双组分聚氨酯漆中作为多元醇组分的用途
公开(公告)号：US4692384A
公开(公告)日：1987-09-08
申请号：US923986
申请日：1986-10-28
申请人： Josef Pedain , Klaus Konig , Manfred Schonfelder
发明人： Josef Pedain , Klaus Konig , Manfred Schonfelder
IPC分类号： C08G18/42 , C08G63/20 , B32B27/00
CPC分类号： C08G18/4219 , C08G18/4205 , C08G63/20 , Y10T428/31551 , Y10T428/31554 , Y10T428/31569
摘要： The present invention relates to polyester polyols having a hydroxyl number of about 80 to 250, containing reaction products of(a) 54 to 58 mol % of a polyol component and(b) 46 to 42 mol % of a dicarboxylic acid component,characterized in that(a) the polyol component contains (i) about 70 to 90 mol % of a hexane-1,6-diol and (ii) about 10 to 30 mol % of at least one higher valent alcohol selected from trimethylolpropane, glycerol, pentaerythritol and mixtures of these polyols, and(b) the dicarboxylic acid component contains (iii) about 50 to 80 mol % of isophthalic acid, (iv) about 20 to 30 mol % of at least one dicarboxylic acid of the formula HOOC--(CH.sub.2).sub.n --COOH (n=an integer from 2-8) and (v) 0 to about 20 mol % of at least one dicarboxylic acid or at least one dicarboxylic acid anhydride selected from terephthalic acid, phthalic acid, phthalic acid anhydride, tetrahydrophthalic acid, tetrahydrophthalic acid anhydride, hexahydrophthalic acid and hexahydrophthalic acid anhydride.The invention also relates to the use of these polyester polyols as the binder component for two-component polyurethane lacquers containing lacquer polyisocyanates for the production of lacquer coatings on molded plastics parts.
摘要翻译：本发明涉及羟值为约80〜250的聚酯多元醇，其含有（a）54〜58摩尔％的多元醇成分和（b）46〜42摩尔％的二羧酸成分的反应产物，其特征在于（a）多元醇组分含有（i）约70至90mol％的己烷-1,6-二醇和（ii）约10至30mol％的至少一种选自三羟甲基丙烷，甘油，季戊四醇的高级醇和这些多元醇的混合物，和（b）二羧酸组分含有（iii）约50至80摩尔％的间苯二甲酸，（iv）约20至30摩尔％的至少一种式HOOC-（CH 2 ）n-COOH（n = 2-8的整数）和（v）0至约20mol％的至少一种二羧酸或至少一种二羧酸酐，其选自对苯二甲酸，邻苯二甲酸，邻苯二甲酸酐，四氢邻苯二甲酸酸，四氢邻苯二甲酸酐，六氢邻苯二甲酸和六氢邻苯二甲酸酐。本发明还涉及这些聚酯多元醇作为用于在模制塑料部件上生产漆涂料的漆多异氰酸酯的双组分聚氨酯漆的粘合剂组分的用途。

6. 发明授权

US4656243A Polyester polyols and their use as polyol component in two-component polyurethane lacquers 失效
标题翻译：聚酯多元醇及其在双组分聚氨酯漆中作为多元醇成分的用途
公开(公告)号：US4656243A
公开(公告)日：1987-04-07
申请号：US737603
申请日：1985-05-24
申请人： Josef Pedain , Klaus Konig , Manfred Schonfelder
发明人： Josef Pedain , Klaus Konig , Manfred Schonfelder
IPC分类号： C08G18/42 , C08G63/20 , C08G63/16
CPC分类号： C08G18/4219 , C08G18/4205 , C08G63/20 , Y10T428/31551 , Y10T428/31554 , Y10T428/31569
摘要： The present invention relates to polyester polyols having a hydroxyl number of about 80 to 250, containing reaction products of(a) 54 to 58 mol % of a polyol component and(b) 46 to 42 mol % of a dicarboxylic acid component, characterized in that(a) the polyol component contains (i) about 70 to 90 mol % of hexane-1,6-diol and (ii) about 10 to 30 mol % of at least one higher valent alcohol selected from trimethylolpropane, glycerol, pentaerythritol and mixtures of these polyols, and(b) the dicarboxylic acid component contains (iii) about 50 to 80 mol % of isophthalic acid, (iv) about 20 to 30 mol % of at least one dicarboxylic acid of the formula HOOC--(CH.sub.2).sub.n --COOH (n=an integer from 2-8) and (v) 0 to about 20 mol % of at least one dicarboxylic acid or at least one dicarboxylic acid anhydride selected from terephthalic acid, phthalic acid, phthalic acid anhydride, tetrahydrophthalic acid, tetrahydrophthalic acid anhydride, hexahydrophthalic acid and hexahydrophthalic acid anhydride.The invention also relates to the use of these polyester polyols as the binder component for two-component polyurethane lacquers containing lacquer polyisocyanates for the production of lacquer coatings on molded plastics parts.
摘要翻译：本发明涉及羟值为约80〜250的聚酯多元醇，其含有（a）54〜58摩尔％的多元醇成分和（b）46〜42摩尔％的二羧酸成分的反应产物，其特征在于（a）多元醇组分含有（i）约70至90mol％的己烷-1,6-二醇和（ii）约10至30mol％的选自三羟甲基丙烷，甘油，季戊四醇和至少一种选自三羟甲基丙烷，甘油，季戊四醇和这些多元醇的混合物和（b）二羧酸组分含有（iii）约50至80摩尔％的间苯二甲酸，（iv）约20至30摩尔％的至少一种式HOOC-（CH 2） n-COOH（n = 2-8的整数）和（v）0至约20mol％的至少一种二羧酸或至少一种选自对苯二甲酸，邻苯二甲酸，邻苯二甲酸酐，四氢邻苯二甲酸的二羧酸酐，四氢邻苯二甲酸酐，六氢邻苯二甲酸和六氢邻苯二甲酸酐。本发明还涉及这些聚酯多元醇作为用于在模制塑料部件上生产漆涂料的漆多异氰酸酯的双组分聚氨酯漆的粘合剂组分的用途。

7. 发明授权

US5076958A Process for the production of isocyanurate polyisocyanates, the compounds obtained by this process and their use 失效
标题翻译：生产异氰酸酯聚异氰酸酯的方法，本方法获得的化合物及其用途
公开(公告)号：US5076958A
公开(公告)日：1991-12-31
申请号：US329902
申请日：1989-03-28
申请人： Josef Pedain , Manfred Schonfelder , Hans-Joachim Hofer , Walter Krauss
发明人： Josef Pedain , Manfred Schonfelder , Hans-Joachim Hofer , Walter Krauss
IPC分类号： C09D175/00 , C08G18/02 , C08G18/28 , C08G18/32 , C08G18/42 , C08G18/79 , C08G18/80
CPC分类号： C08G18/4238 , C08G18/3221 , C08G18/3253 , C08G18/3296 , C08G18/4205 , C08G18/4277 , C08G18/792 , C08G18/8016 , C08G18/8061
摘要： The present invention is directed to a process for the production of isocyanurate polyisocyanates by the partial trimerization of the isocyanate groups of aliphatic diisocyanates in the presence of catalysts which accelerate the trimerization of isocyanate groups, termination of the trimerization reaction at the particular degree of trimerization required and removal of unreacted starting diisocyanate and, optionally, other volatile constituents, characterized in that at least one diol containing ester groups and having an average molecular weight of 350 to 950 is added to the reaction mixture at any time before removal of the excess starting diisocyanate in a quantity of 1 to 50% by weight, based on the weight of the diisocyanate used as starting material, the type of reactants and the quantitative ratios between them being selected so that, on completion of the reaction, at least 10% by weight free starting diisocyanate is still present in the reaction mixture, not including any inert solvent used, and the molar ratio of isocyanurate groups to urethane groups in the end products is about 20:1 to 0.2:1.The present invention is also directed to the isocyanurate polyisocyanates obtained by this process and the use of these isocyanurate polyisocyanates, optionally blocked by blocking agents for isocyanate groups, for the production of polyurethane plastics, particularly two-component polyurethane lacquers.
摘要翻译：本发明涉及通过在促进异氰酸酯基团三聚化的催化剂存在下部分三聚异氰酸酯基团的异氰酸酯基团的生产来制备异氰脲酸酯多异氰酸酯的方法，在特定的三聚反应程度下终止三聚反应所需的并除去未反应的起始二异氰酸酯和任选的其它挥发性成分，其特征在于在除去过量的起始二异氰酸酯之前的任何时间将至少一种含有酯基并且平均分子量为350至950的二醇加入到反应混合物中以1至50重量％的量，以用作起始原料的二异氰酸酯的重量计，反应物的类型和它们之间的定量比被选择，使得在反应完成时，至少10重量％游离的起始二异氰酸酯仍然存在于反应混合物中，不包括任何内部 t溶剂，最终产物中异氰脲酸酯基与氨基甲酸酯基的摩尔比为约20:1至0.2:1。本发明还涉及通过该方法获得的异氰脲酸酯多异氰酸酯以及任选被异氰酸酯基团的封闭剂封闭的这些异氰脲酸酯多异氰酸酯用于生产聚氨酯塑料，特别是双组分聚氨酯漆的用途。

8. 发明授权

US4456647A Plastics mouldings finished with a three-layer coating and a process for producing the finish 失效
标题翻译：塑料模制品采用三层涂层和一种生产精加工工艺
公开(公告)号：US4456647A
公开(公告)日：1984-06-26
申请号：US448839
申请日：1982-12-10
申请人： Manfred Schonfelder , Helmut Steinberger , Helmut Schmid
发明人： Manfred Schonfelder , Helmut Steinberger , Helmut Schmid
IPC分类号： B32B27/00 , B32B27/18 , B32B27/30 , B32B27/42 , C08G18/61 , C08J7/04 , B32B7/02
CPC分类号： C08G18/61 , C08J7/045 , C08J2433/00 , C08J2469/00 , Y10T428/24975 , Y10T428/31507 , Y10T428/31551 , Y10T428/31554 , Y10T428/31576 , Y10T428/31594 , Y10T428/31598 , Y10T428/31601 , Y10T428/31663 , Y10T428/31862 , Y10T428/31928 , Y10T428/31935 , Y10T428/31942
摘要： The invention relates to plastics mouldings, more particularly transparent plastics mouldings, which are finished with a coating of three successively stoved, chemically different layers, and to a process for producing the finish. The special finish considerably improves the scratch resistance, abrasion resistance, weathering resistance and yellowing resistance of the plastics surfaces without affecting the transparency of the plastics moulding. The first layer (primer layer) is produced from a hardenable acrylic resin and an aminoplast resin, the second layer from a thermoplastic acrylic resin, a plasticizer and a masked polyisocyanate and the third layer (cover layer) from at least one partially hydrolyzed organosilane, an .alpha.,.omega.-dihydroxy polydimethyl siloxane, a silica sol and at least one masked polyisocyanate as binder in the presence of a water-soluble organic or inorganic acid. The three-layer coating contains UV-absorbers, light stabilizers and, optionally, standard auxiliaries.
摘要翻译：本发明涉及塑料模制品，更特别是透明的塑料模制品，其用三个相继烘烤的，化学不同的层的涂层和用于生产涂饰的方法来完成。特殊的表面处理可显着提高塑料表面的耐擦伤性，耐磨性，耐候性和耐黄变性，而不会影响塑料模制品的透明度。第一层（底漆层）由可硬化的丙烯酸树脂和氨基塑料树脂制成，来自热塑性丙烯酸树脂的第二层，增塑剂和掩蔽的多异氰酸酯，以及来自至少一种部分水解的有机硅烷的第三层（覆盖层） α，ω-二羟基聚二甲基硅氧烷，硅溶胶和至少一种掩蔽的多异氰酸酯作为粘合剂，在水溶性有机或无机酸存在下进行。三层涂层含有紫外线吸收剂，光稳定剂和任选的标准助剂。

9. 发明授权

US4444973A Coatings for thermoplastics 失效
标题翻译：热塑性塑料涂料
公开(公告)号：US4444973A
公开(公告)日：1984-04-24
申请号：US411751
申请日：1982-08-26
申请人： Manfred Schonfelder , Helmut Steinberger
发明人： Manfred Schonfelder , Helmut Steinberger
IPC分类号： C08G18/61 , C08G18/80 , C08J7/04 , C09D183/04 , C08G77/04
CPC分类号： C09D183/04 , C08G18/61 , C08G18/8061 , C08J7/047 , C08J2483/00 , Y10T428/31507 , Y10T428/31663
摘要： The present invention relates to protective coating formulations, in particular to transparent abrasion-resistant and scratch-resistant coatings on transparent thermoplastic polymers, which coatings essentially consist of a hydrolyzed siloxane compound, a dispersion of colloidal silicon dioxide, etherified methylolmelamine, a blocked polyisocyanate, acetic acid and a polysiloxane terminated by hydroxyl groups.
摘要翻译：本发明涉及保护性涂料制剂，特别涉及透明热塑性聚合物上的透明耐磨损和耐刮擦涂层，其涂层基本上由水解的硅氧烷化合物，胶体二氧化硅的分散体，醚化的羟甲基三聚氰胺，封端的多异氰酸酯，乙酸和由羟基封端的聚硅氧烷。

10. 发明授权

US6007619A Use of nonionic, water-dispersible polyisocyanates as concrete additives 失效
标题翻译：使用非离子，水分散性多异氰酸酯作为混凝土添加剂
公开(公告)号：US6007619A
公开(公告)日：1999-12-28
申请号：US988575
申请日：1997-12-11
申请人： Hans-Josef Laas , Martin Brahm , Jan Mazanek , Hermann Kober , Manfred Schonfelder , Dietbert Knofel , Karl-Georg Bottger , Anke Reinschmidt
发明人： Hans-Josef Laas , Martin Brahm , Jan Mazanek , Hermann Kober , Manfred Schonfelder , Dietbert Knofel , Karl-Georg Bottger , Anke Reinschmidt
IPC分类号： C04B24/28 , C04B28/02 , C04B103/60 , C08G18/28 , C08G18/48 , C08G18/70 , C08G18/79 , C08L75/08 , C04B24/12
CPC分类号： C08G18/283 , C04B24/282 , C08G18/282 , C08G18/706 , C08G2105/02
摘要： The present invention relates to a process for preparing mortar/concrete compositions by incorporating into the mortar/concrete compositions either before or during the mixing operation a water-dispersible polyisocyanate whicha) has an average isocyanate functionality of 1.8 to 4.0,b) contains 4.0 to 25.0 wt. % of aliphatically and/or cycloaliphatically bound isocyanate groups (calculated as NCO; molecular weight=42) andc) contains 5 to 80 wt. % of ethylene oxide units present within polyether chains (calculated as C.sub.2 H.sub.4 O; molecular weight=44), in whichd) the polyether chains contain an average of 5 to 50 ethylene oxide units.
摘要翻译：本发明涉及一种通过在混合操作之前或期间将水分散性多异氰酸酯掺入到砂浆/混凝土组合物中来制备砂浆/混凝土组合物的方法，a）具有1.8至4.0的平均异氰酸酯官能度，b）包含4.0 至25.0重量％脂肪和/或脂环结合的异氰酸酯基团的％（以NCO计算;分子量= 42），和c）含有5-80重量％存在于聚醚链内的环氧乙烷单元的％（以C 2 H 4 O计算;分子量= 44），其中d）聚醚链含有平均5至50个环氧乙烷单元。

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