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1. 发明授权

US5382702A Process for the production of 5-alkoxy-2,4-dinitro-alkylbenzenes 失效
标题翻译： 5-烷氧基-2,4-二硝基 - 烷基苯的制备方法
公开(公告)号：US5382702A
公开(公告)日：1995-01-17
申请号：US142383
申请日：1993-11-19
申请人： Wolfgang R. Balzer , Thomas Clausen , Alexa Weinges
发明人： Wolfgang R. Balzer , Thomas Clausen , Alexa Weinges
IPC分类号： C07C201/08 , C07C201/12 , C07C205/12 , C07C205/37 , C07C43/205
CPC分类号： C07C201/08 , C07C201/12
摘要： Process for producing 5-alkoxy-2,4-dinitroalkylbenzenes of the general formula (I) ##STR1## R.sup.1 =C.sub.1 to C.sub.4 alkyl; R=C.sub.1 to C.sub.6 alkyl group, C.sub.2 to C.sub.4 hydroxyalkyl, C.sub.3 to C.sub.4 dihydroxyalkyl,in which a 3-fluoroalkylbenzene is nitrated and the obtained 2,4-dinitro-5-fluoroalkylbenzene is then reacted with a suitable alcohol at -5.degree. C. to +25.degree. C. with the addition of sodium hydroxide or potassium hydroxide.
摘要翻译： PCT No.PCT / EP93 / 00678 Sec。 371日期：1993年11月19日 102（e）1993年11月19日PCT 1993年3月20日PCT PCT。出版物WO93 / 2551200 日本1993年12月23日。通式（I）的5-烷氧基-2,4-二硝基烷基苯的制备方法（Ⅰ）R1 = C1〜C4烷基; R = C1至C6烷基，C2至C4羟基烷基，C3至C4二羟基烷基，其中3-氟烷基苯被硝化，所得2,4-二硝基-5-氟烷基苯然后与适当的醇在-5℃下反应至+ 25℃，加入氢氧化钠或氢氧化钾。

2. 发明授权

US5542953A 5-halogen-2,4-Bis (alkylamino)-1-alkylbenzenes and hair dye compositions containing same 失效
标题翻译： 5-卤代-2,4-双（烷基氨基）-1-烷基苯和含有它们的染发剂组合物
公开(公告)号：US5542953A
公开(公告)日：1996-08-06
申请号：US142492
申请日：1993-10-22
申请人： Wolfgang R. Balzer , Thomas Clausen , Anke Frank , Alexa Weinges
发明人： Wolfgang R. Balzer , Thomas Clausen , Anke Frank , Alexa Weinges
IPC分类号： A61K8/00 , A61K8/33 , A61K8/40 , A61K8/41 , A61K8/49 , A61Q5/10 , C07C211/52 , C07C215/16 , A61K7/13 , C07C211/51
CPC分类号： A61Q5/10 , A61K8/411 , A61K8/69 , C07C211/52 , C07C215/16
摘要： The composition for the oxidative dyeing of hair contains at least one coupler of the general formula ##STR1## where R is a straight-chain or branched C.sub.1 - to C.sub.4 -alkyl group, X is chlorine or fluorine, and R.sup.1 is a straight-chain or branched C.sub.1 - to C.sub.4 -alkyl group or a straight-chain or branched C.sub.2 - to C.sub.4 -hydroxyalkyl group. The 5-halogen-2,4-bis(alkylamino)-1-alkylbenzenes of the formula (I) are novel. The couplers of the general formula (I) may be obtained through simple chemical reactions, are easily soluble in water and have an outstanding shelf stability, in particular as a constituent of the hair dye composition described here. The dyeing results which can be achieved with the hair dye composition according to the invention are particularly distinguished by the color intensity of the red hues, in addition to the multitude of shades, and by a good purity of color with respect to blue hues.
摘要翻译： PCT No.PCT / EP93 / 00011 Sec。 371日期：1993年10月22日 102（e）日期1993年10月22日PCT 1993年1月7日PCT PCT。出版物WO93 / 16677 日本1993年9月2日头发的氧化染色组合物含有至少一种通式为（I）的成色剂，其中R是直链或支链的C 1 -C 4烷基，X是氯或氟，R 1为直链或支链C 1至C 4烷基或直链或支链C 2至C 4 - 羟基烷基。式（I）的5-卤代-2,4-二（烷基氨基）-1-烷基苯是新颖的。通式（I）的成色剂可以通过简单的化学反应获得，易溶于水并具有优异的贮存稳定性，特别是作为本文所述的染发剂组合物的成分。通过根据本发明的染发剂组合物可以实现的染色结果特别地除了多种色调之外的红色调的颜色强度以及相对于蓝色色调的良好的颜色纯度。

3. 发明授权

US5224965A Composition for the oxidative dyeing of hair and new 5-halogen-2,4-diamino alkylbenzenes 失效
标题翻译：头发和新5-卤代-2,4-二氨基亚苄基氧化剂的组合物
公开(公告)号：US5224965A
公开(公告)日：1993-07-06
申请号：US847080
申请日：1992-04-07
申请人： Thomas Clausen , Alexa Weinges , Wolfgang R. Balzer
发明人： Thomas Clausen , Alexa Weinges , Wolfgang R. Balzer
IPC分类号： C07C205/12 , C07C211/52 , D06P1/32 , D06P3/08
CPC分类号： A61Q5/10 , A61K8/411 , C07C205/12 , C07C211/52
摘要： The composition for the oxidative dyeing of hair contains at least one coupler substance of the formula ##STR1## where R is a straight-chain or branched C.sub.1 - to C.sub.4 -alkyl group and X is fluorine or bromine, and new 5-halogen-2,4-diaminoalkylbenzenes.The coupler substances of formula (I) are obtainable by simple chemical reactions, easily soluble in water and have a good shelf stability particularly as constituents of the hair dye composition described here.In addition to the multitude of color shades, the dye results which can be achieved with the hair dye composition according to the invention are distinguished particularly by the intensity of color of the red tones and good uniformity of color of the blue tones.
摘要翻译： PCT No.PCT / EP91 / 01565 Sec。 371日期：1992年4月7日 102（e）日期1992年4月7日PCT 1991年8月17日PCT PCT。出版物WO92 / 04005 头发氧化染色的组合物含有至少一种式（I）的成色剂物质，其中R是直链或支链的C 1〜C 4 - 烷基，X是氟或溴，以及新的5-卤代-2,4-二氨基烷基苯。式（I）的成色剂物质可以通过简单的化学反应获得，易溶于水并且具有良好的贮存稳定性，特别是作为本文所述的染发组合物的成分。除了多种色调之外，根据本发明的染发组合物可以实现的染色结果特别地由红色调的颜色强度和蓝色色调的良好均匀性区分开来。

4. 发明授权

US5718731A Oxidation hair dye composition based on 4,5-diaminopyrazole and m-phenylenediamine derivatives 失效
标题翻译：基于4,5-二氨基吡唑和间苯二胺衍生物的氧化染发剂组合物
公开(公告)号：US5718731A
公开(公告)日：1998-02-17
申请号：US696327
申请日：1996-08-13
申请人： Isolde Loewe , Alexa Weinges , Wolfgang R. Balzer , Stefan Gerstung
发明人： Isolde Loewe , Alexa Weinges , Wolfgang R. Balzer , Stefan Gerstung
IPC分类号： A61K8/00 , A61K8/41 , A61K8/49 , A61Q5/10 , C07D231/38 , D06P1/32 , D06P3/08 , A61K7/13
CPC分类号： A61Q5/10 , A61K8/494 , D06P1/32
摘要： The oxidation hair dye composition contains from 0.01 to 4.0 percent by weight of a developer substance including at least one diaminopyrazole of the formula (I) ##STR1## wherein R.sup.1 is selected from the group consisting of hydrogen, an alkyl group having from 1 to 6 carbon atoms, a hydroxyalkyl group having from 2 to 4 carbon atoms and a substituted or unsubstituted benzyl group, and R.sup.2 and R.sup.3, independently, are each selected from the group consisting of hydrogen, an alkyl group having from 1 to 6 carbon atoms and a hydroxyalkyl group having from 2 to 4 carbon atoms; and from 0.01 to 4.0 percent by weight of a coupler substance including at least one m-phenylenediamine selected from the group consisting of N-(3-dimethylamino)phenyl urea and 3-(N-methylsulfonyl)amino-N,N-dimethylaniline.
摘要翻译：氧化染发剂组合物含有0.01至4.0重量％的显影剂物质，其包含至少一种式（I）的二氨基吡唑其中R 1选自氢，烷基，其具有 1至6个碳原子，具有2至4个碳原子的羟烷基和取代或未取代的苄基，R 2和R 3各自独立地选自氢，具有1至6个碳原子的烷基原子和具有2至4个碳原子的羟烷基; 和0.01至4.0重量％的包含至少一种选自N-（3-二甲基氨基）苯基脲和3-（N-甲基磺酰基）氨基-N，N-二甲基苯胺的间苯二胺的成色剂物质。

5. 发明授权

US5645610A Substituted 2-alkylamino-4-amino-1-alkylbenzene compounds and oxidation hair dye compositions based on said compounds 失效
标题翻译：基于所述化合物的取代的2-烷基氨基-4-氨基-1-烷基苯化合物和氧化染发组合物
公开(公告)号：US5645610A
公开(公告)日：1997-07-08
申请号：US450476
申请日：1995-05-26
申请人： Wolfgang R. Balzer , Anke Frank , Alexa Weinges
发明人： Wolfgang R. Balzer , Anke Frank , Alexa Weinges
IPC分类号： A61K8/00 , A61K8/33 , A61K8/41 , A61K8/49 , A61Q5/10 , C07C211/50 , C07C211/52 , C07C215/16 , C07C217/84 , C07D213/73 , C07D231/38 , C07D239/46 , D06P1/32 , D06P3/08 , A61K7/13 , C07C209/00
CPC分类号： A61Q5/10 , A61K8/411 , C07C217/84
摘要： The new coupler compounds of the invention are 4-amino-2 -(2'-hydroxyethyl)-amino-5-methoxytoluene and/or 4-amino-2-(2'-hydroxyethyl)amino-5-chlorotoluene. The invention also includes an oxidation hair dye composition including an effective amount, advantageously from 0.01 to 5 percent by weight, of the above-mentioned new coupler compounds together with one or more known developer compounds and optionally certain direct dyes.
摘要翻译：本发明的新的成色剂化合物是4-氨基-2-（2'-羟乙基） - 氨基-5-甲氧基甲苯和/或4-氨基-2-（2'-羟乙基）氨基-5-氯甲苯。本发明还包括氧化染发剂组合物，其包含有效量，有利地为0.01至5重量％的上述新的成色剂化合物以及一种或多种已知的显影剂化合物和任选的某些直接染料。

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