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1. 发明授权

US5591804A Fluorinated onium salts, curable compositions containing same, and method of curing using same 失效
标题翻译：含氟鎓盐，含有它们的可固化组合物和使用它们的固化方法
公开(公告)号：US5591804A
公开(公告)日：1997-01-07
申请号：US576097
申请日：1995-12-21
申请人： William D. Coggio , Dirk H. C. Arren , Douglas S. Parker , Allan T. Worm
发明人： William D. Coggio , Dirk H. C. Arren , Douglas S. Parker , Allan T. Worm
IPC分类号： C08K5/17 , C08F8/00 , C08K5/36 , C08K5/50 , C08L27/16 , C08F8/30
CPC分类号： C08F8/00 , C08F2800/20
摘要： A compound having the formula: ##STR1## where Q is an onium ion; A.sup.- is a counterion; R.sup.1, R.sup.2, R.sup.3, and R.sup.4, independently, comprise (a) a non-fluorinated alkyl, cycloalkyl, aryl, or aralkyl group; (b) an onium-containing group; or (c) a group having the formula --(CH.sub.2).sub.n --Y--R.sup.5 in which n is at least two; Y is a spacer arm comprising a --CH.sub.2 --, --O--, --OCH.sub.2 --, --S--, --SO.sub.2 --, or --Z--SO.sub.2-- group; Z is an --R.sup.6 --O--, --N(R.sup.7)--, or --N(H)-- group; R.sup.6 is a substituted or unsubstituted phenylene group; R.sup.7 is a non-fluorinated alkyl, cycloalkyl, aryl, or alkaryl group; and R.sup.5 is a fluorinated group, perfluorinated group, or combination thereof, with the proviso that (i) at least one of R.sup.1, R.sup.2, R.sup.3, and R.sup.4 comprises a group having the formula --(CH.sub.2).sub.n --Y--R.sup.5 ; (ii) the total number of fluorine atoms in said compound is at least 5; and (iii) when Q is a sulfonium ion, there is no R.sup.4 group. The invention further includes curable compositions comprising vinylidene fluoride-containing polymers and the above-described compounds, as well as a method for curing such compositions.
摘要翻译：具有下式的化合物：其中Q是鎓离子; A-是抗衡离子 R 1，R 2，R 3和R 4独立地包含（a）非氟化烷基，环烷基，芳基或芳烷基; （b）含鎓基团; 或（c）具有式 - （CH 2）n -Y-R 5的基团，其中n至少为2; Y是包含-CH 2 - ， - O - ， - OCH 2 - ， - S - ， - SO 2 - 或-Z-SO 2 - 基团的间隔臂; Z是-R 6 -O-，-N（R 7） - 或-N（H） - 基; R6是取代或未取代的亚苯基; R7是非氟化的烷基，环烷基，芳基或烷芳基; 并且R 5是氟化基团，全氟化基团或其组合，条件是（i）R 1，R 2，R 3和R 4中的至少一个包含具有式 - （CH 2）n -Y-R 5的基团; （ii）所述化合物中的氟原子总数至少为5; 和（iii）当Q是锍离子时，不存在R 4基团。本发明还包括包含偏二氟乙烯的聚合物和上述化合物的可固化组合物，以及用于固化该组合物的方法。

2. 发明授权

US06734254B1 Co-curable blends featuring bromine-and iodine-containing fluoroplastic polymers 有权
标题翻译：具有溴和碘的氟塑料聚合物的共可共混共混物
公开(公告)号：US06734254B1
公开(公告)日：2004-05-11
申请号：US10340969
申请日：2003-01-13
申请人： Allan T. Worm , William D. Coggio , Ralph Kaulbach , Friedrich Kloos
发明人： Allan T. Worm , William D. Coggio , Ralph Kaulbach , Friedrich Kloos
IPC分类号： C08L2710
CPC分类号： C08L27/12 , C08L27/16 , C08L27/18 , C08L2205/02 , C08L2666/04
摘要： Provided is a co-curable blend comprising (a) a fluoroplastic comprising (i) bromine atoms, iodine atoms, and combinations thereof, and (ii) units derived from a fluorinated monomer, and a peroxide curable fluoroelastomer gum. The invention also provides a composition comprising a fluoroplastic comprising (i) bromine atoms, iodine atoms, and combinations thereof and (ii) units derived from a fluorinated monomer, peroxide curable fluoroelastomer gum, a peroxide curative, and optionally a coagent. The fluoroplastic has an MFI no greater than 5 g/10 min., and/or an average particle size greater than 100 nm. The invention also provides a method of making a fluoropolymer blend and cured articles.
摘要翻译：本发明提供一种共可固化共混物，其包含（a）氟塑料，其包含（i）溴原子，碘原子及其组合，和（ii）源自氟化单体的单元和可过氧化物固化的含氟弹性体胶。本发明还提供包含氟塑料的组合物，其包含（i）溴原子，碘原子及其组合，和（ii）源自氟化单体，过氧化物可固化的含氟弹性体胶，过氧化物固化剂和任选的助剂的单元。氟塑料具有不大于5g / 10min的MFI，和/或大于100nm的平均粒度。本发明还提供了制备含氟聚合物共混物和固化制品的方法。

3. 发明授权

US07148300B2 Fluoroelastomers with improved permeation resistance and method for making the same 失效
标题翻译：具有改善渗透阻力的氟弹性体及其制备方法
公开(公告)号：US07148300B2
公开(公告)日：2006-12-12
申请号：US10659877
申请日：2003-09-11
申请人： Tatsuo Fukushi , Allan T. Worm , Erik D. Hare , Greggory S. Bennett , William D. Coggio
发明人： Tatsuo Fukushi , Allan T. Worm , Erik D. Hare , Greggory S. Bennett , William D. Coggio
IPC分类号： C08F116/12
CPC分类号： C08F214/18 , C08F214/16 , C08K5/0025 , C08L27/12
摘要： A compound is prepared, suitable for forming fluoroelastomers, having the unique features of a low glass transition temperature and desirable permeation resistance. The compound generally comprises two primary components. The first component is an amorphous copolymer including interpolymerized units derived from one or more perfluorinated ethers. The second component is a curable component including at least one filler having at least 10 parts per 100 parts of the first component. Upon vulcanization the resulting elastomeric compound has desirable physical characteristics as indicated by the durometer, the retraction at lower temperatures (TR-10) and permeation resistance.
摘要翻译：制备适合于形成含氟弹性体的化合物，其具有低玻璃化转变温度和所需渗透阻力的独特特征。化合物通常包含两个主要组分。第一组分是包含衍生自一种或多种全氟化醚的共聚单元的无定形共聚物。第二组分是可固化组分，其包含至少一种每100份第一组分至少10份的填料。硫化后，得到的弹性体化合物具有所需的物理特性，如硬度计所示，在较低温度下回缩（TR-10）和耐渗透性。

4. 发明授权

US6087406A Recycle of vulcanized fluorinated elastomers 失效
公开(公告)号：US6087406A
公开(公告)日：2000-07-11
申请号：US854787
申请日：1997-05-12
申请人： Allan T. Worm , Erik D. Hare , Paul N. Nelson
发明人： Allan T. Worm , Erik D. Hare , Paul N. Nelson
IPC分类号： C08L27/12 , C08J11/18 , C08K5/00 , C08K5/13 , C08K5/435 , C08L27/24 , C08F8/50
CPC分类号： C08J11/18 , C08K5/0025 , C08J2327/12 , Y02W30/706
摘要： Compositions and techniques useful to effectively recycle crosslinked (i.e., vulcanized or cured) fluoroelastomers are disclosed. The invention utilizes an additive system that includes a cure-enhancing additive, a crosslinking agent, and an accelerator.

5. 发明授权

US4287322A Epichlorohydrin elastomer compositions 失效
标题翻译：表氯醇弹性体组合物
公开(公告)号：US4287322A
公开(公告)日：1981-09-01
申请号：US87503
申请日：1979-10-23
申请人： Allan T. Worm
发明人： Allan T. Worm
IPC分类号： C08K5/00 , C08L71/03 , C08G65/32
CPC分类号： C08L71/03 , C08K5/0025
摘要： A gum stock composition comprising polyepichlorohydrin gum, polyphenol, organo-onium compound, and acid acceptor is shaped and cured to form shaped elastomeric articles.
摘要翻译：包含聚表氯醇胶，多酚，有机鎓化合物和酸受体的树胶组合物成型并固化以形成成型的弹性体制品。

6. 发明授权

US06255536B1 Fluorine containing vinyl ethers 有权
标题翻译：含氟乙烯醚
公开(公告)号：US06255536B1
公开(公告)日：2001-07-03
申请号：US09470497
申请日：1999-12-22
申请人： Allan T. Worm , George G. I. Moore , Miguel A. Guerra , Werner Schwertfeger , Klaus Hintzer , Zai-Ming Qiu , Erik D. Hare
发明人： Allan T. Worm , George G. I. Moore , Miguel A. Guerra , Werner Schwertfeger , Klaus Hintzer , Zai-Ming Qiu , Erik D. Hare
IPC分类号： C07F4311
CPC分类号： C07C41/24 , C07C41/18 , C07C41/48 , C07C67/307 , C07C2601/14 , C07C69/708 , C07C43/17 , C07C43/192 , C07C43/313
摘要： The present invention describes a novel process for the preparation of perfluorovinyl ethers. The process involves providing a hydrocarbon precursor that may be partially halogenated, fluorinating the precursor to provide a perfluorinated intermediate, and converting the perfluorinated intermediate to the desired perfluorinated ether. Novel perfluorovinyl ethers are also provided.
摘要翻译：本发明描述了制备全氟乙烯基醚的新方法。该方法包括提供可以部分卤化的烃前体，氟化前体以提供全氟化中间体，并将全氟化中间体转化为所需的全氟化醚。还提供了新的全氟乙烯基醚。

7. 发明授权

US4233421A Fluoroelastomer composition containing sulfonium curing agents 失效
标题翻译：含有锍固化剂的含氟弹性体组合物
公开(公告)号：US4233421A
公开(公告)日：1980-11-11
申请号：US15171
申请日：1979-02-26
申请人： Allan T. Worm
发明人： Allan T. Worm
IPC分类号： C08L27/14 , C08K5/36 , C08K5/37 , C08L1/00 , C08L27/00 , C08L27/16 , C08F8/40 , C08F8/34 , C08F14/22
CPC分类号： C08K5/36
摘要： A thermally stable, curable fluoroelastomer composition containing sulfonium curing agent is described. The composition is curable in reactive admixture with an inorganic acid acceptor and includes:(a) a fluoroelastomer comprising vinylidene fluoride;(b) at least one triorgano sulfonium compound; and(c) at least one aromatic polyhydroxy compound.
摘要翻译：描述了含有锍固化剂的热稳定的可固化的含氟弹性体组合物。该组合物可与无机酸受体反应混合而固化，并包括：（a）包含偏二氟乙烯的含氟弹性体; （b）至少一种三有机锍化合物; 和（c）至少一种芳族多羟基化合物。

8. 发明授权

US06294627B1 Low temperature fluorocarbon elastomers 有权
标题翻译：低温氟碳弹性体
公开(公告)号：US06294627B1
公开(公告)日：2001-09-25
申请号：US09313438
申请日：1999-05-18
申请人： Allan T. Worm , Nikolai Vladimirovich Veretennikov , Margarita Alekseevna Volkova , Sergey Vasilievich Sokolov
发明人： Allan T. Worm , Nikolai Vladimirovich Veretennikov , Margarita Alekseevna Volkova , Sergey Vasilievich Sokolov
IPC分类号： C08F11612
CPC分类号： C08F216/1416 , C08F214/222 , C08F216/1408
摘要： A fluorocarbon polymer which includes: repeating units derived from one or more perfluorinated ethers of the formula CF2═CFO—(CF2)m—(O(CF2)p)n—ORf1 wherein Rf1 is a perfluorinated (C1-C4)alkyl group, m=1-4, n=0-6, and p=1-2; and repeating units derived from vinylidene fluoride; wherein the polymer has a glass transition temperature of −50° C. or lower and an oxygen to carbon ratio of at least about 0.2.
摘要翻译：一种碳氟聚合物，其包括：衍生自一种或多种式CF 2 = CFO-（CF 2）m - （O（CF 2）p）n -OR f 1的全氟化醚的重复单元，其中Rf1是全氟化（C1-C4）烷基， m = 1-4，n = 0-6，p = 1-2; 和衍生自偏二氟乙烯的重复单元; 其中所述聚合物的玻璃化转变温度为-50℃以下，氧碳比为至少约0.2。

9. 发明授权

US06255535B1 Fluorine containing allylethers and higher homologs 有权
标题翻译：含氟烯丙基醚和高级同系物
公开(公告)号：US06255535B1
公开(公告)日：2001-07-03
申请号：US09470034
申请日：1999-12-22
申请人： Jay F. Schulz , George G. I. Moore , Werner Schwertfeger , Klaus Hintzer , Zai-Ming Qiu , Miguel A. Guerra , Erik D. Hare , Allan T. Worm
发明人： Jay F. Schulz , George G. I. Moore , Werner Schwertfeger , Klaus Hintzer , Zai-Ming Qiu , Miguel A. Guerra , Erik D. Hare , Allan T. Worm
IPC分类号： C07C4330
CPC分类号： C07C43/17 , C07C41/16 , C07C41/22 , C07C41/24 , C07C43/313 , C07C43/126
摘要： The present invention describes a novel process for the preparation of perfluoro allyl ethers. The process involves providing a hydrogen-containing precursor comprising at least one 1,2-dichloro alkyl ether moiety, fluorinating the precursor to provide a perfluorinated intermediate, and dechlorinating the perfluorinated intermediate to the corresponding perfluorinated ether. A reaction product of a perfluorinated olefin and an allyl ether may also be used as a precursor. Such a reaction product is chlorinated before the fluorination step. Perfluoro vinyl or allyl ethers may be used in place of the perfluorinated olefin. Novel perfluoro alkoxy compounds are also described.
摘要翻译：本发明描述了制备全氟烯丙基醚的新方法。该方法包括提供包含至少一个1,2-二氯烷基醚部分的含氢前体，氟化前体以提供全氟化中间体，并将全氟化中间体脱氯至相应的全氟化醚。全氟化烯烃和烯丙基醚的反应产物也可以用作前体。这样的反应产物在氟化步骤之前被氯化。可以使用全氟乙烯基或烯丙基醚代替全氟化烯烃。还描述了新的全氟烷氧基化合物。

10. 发明授权

US06864336B2 Fluoroelastomers having low temperature characteristics and solvent resistance 有权
标题翻译：具有低温特性和耐溶剂性的氟弹性体
公开(公告)号：US06864336B2
公开(公告)日：2005-03-08
申请号：US10660437
申请日：2003-09-11
申请人： Harald Kaspar , Klaus Hintzer , Guy van Gool , Franz März , Allan T. Worm , Tatsuo Fukushi
发明人： Harald Kaspar , Klaus Hintzer , Guy van Gool , Franz März , Allan T. Worm , Tatsuo Fukushi
IPC分类号： C09K3/10 , C08F2/16 , C08F2/38 , C08F8/00 , C08F8/22 , C08F14/00 , C08F214/22
CPC分类号： C08F8/30 , C08F2800/10 , C08F2810/20 , C08F2810/30 , C08F214/22
摘要： The present invention is based on quad-fluoropolymer suitable for the preparation of a fluoroelastomer. The fluoropolymer comprises repeating units derived from 10 to 40 mol % of tetrafluoroethylene, 40 to 65 mol % of vinylidene fluoride, 1 to 30 mol % of a perfluorinated vinyl ether of the formula CF2═CFOCF2CF2CF2OCF3, 1 to 20 mol % of perfluoromethyl vinylether.
摘要翻译：本发明基于适用于制备含氟弹性体的四氟聚合物。氟聚合物包含衍生自10〜40摩尔％的四氟乙烯，40〜65摩尔％的偏氟乙烯，1〜30摩尔％的式CF2 = CFOCF2CF2CF2OCF3的全氟化乙烯基醚，1〜20摩尔％的全氟甲基乙烯基醚的重复单元。

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