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1. 发明授权

US07576136B2 Emulsified feedstock for hydrocarbon process units that incorporate spray atomization 有权
标题翻译：含有喷雾雾化的烃工艺装置的乳化原料
公开(公告)号：US07576136B2
公开(公告)日：2009-08-18
申请号：US11146954
申请日：2005-06-07
申请人： Wiley L. Parker , Alan E. Goliaszewski , Collin W. Cross
发明人： Wiley L. Parker , Alan E. Goliaszewski , Collin W. Cross
IPC分类号： B01F3/08 , C10G47/24 , C07C4/06
CPC分类号： C10G11/14 , B01F3/0811 , B01F3/0861 , B01F5/0602 , C10G11/18 , Y10S516/924
摘要： The present invention is directed to a method for producing an emulsified aqueous hydrocarbon solution comprising, providing a liquid hydrocarbon stream at a particular temperature and a separate water stream, mixing the water stream with a surfactant at a predetermined ratio, raising the pressure of the hydrocarbon stream to a pressure greater than the vapor pressure of steam at the temperature, spraying the water into the hydrocarbon stream at a pressure greater than that of the hydrocarbon stream in a pre-mix chamber; and passing the pressurized hydrocarbon-water mixture through a static mixing chamber.
摘要翻译：本发明涉及一种生产乳化的含水烃溶液的方法，其包括：在特定温度下提供液态烃流和单独的水流，以预定比例混合水流与表面活性剂，提高烃的压力在高于在该温度下的蒸汽压力的压力下流动，将水以比预混合室中的烃流的压力高的速率喷射到烃流中; 并将加压的烃 - 水混合物通过静态混合室。

2. 发明授权

US07553878B2 Spray atomization 有权
标题翻译：喷雾雾化
公开(公告)号：US07553878B2
公开(公告)日：2009-06-30
申请号：US10425153
申请日：2003-04-29
申请人： Wiley L. Parker , Collin W. Cross , Alan E. Goliaszewski
发明人： Wiley L. Parker , Collin W. Cross , Alan E. Goliaszewski
IPC分类号： B01F3/08 , C10G11/18 , C10G9/36
CPC分类号： C10L1/328
摘要： The present invention provides a feedstock composition for increasing the efficiency of atomization in hydrocarbon processing that includes a water-in-hydrocarbon oil emulsion including a non-ionic surfactant capable of stabilizing the emulsion and having a hydrophilic-lipophilic balance of greater than about 12. The emulsion includes water droplets of about 5 to about 10 microns in diameter, the droplets being dispersed substantially uniformly in the hydrocarbon oil phase. These surfactants are capable of stabilizing the water-in-hydrocarbon oil emulsion under relevant temperature and pressure conditions for hydrocarbon processing. The inventive feedstock composition provides a metastable water-in-oil emulsion where expanding water vapor explodes under spray conditions where the system pressure is released, demolishing a larger oil droplet and producing smaller oil droplets.
摘要翻译：本发明提供了一种用于提高烃加工中雾化效率的原料组合物，其包括含烃烃油乳液，其包括能够稳定乳液并具有大于约12的亲水亲油平衡的非离子表面活性剂。该乳液包括直径约5至约10微米的水滴，液滴基本均匀地分散在烃油相中。这些表面活性剂能够在碳氢化合物加工的相关温度和压力条件下稳定含烃烃油乳液。本发明的原料组合物提供了一种亚稳定的油包水乳液，其中膨胀水蒸汽在喷雾条件下爆炸，其中释放系统压力，拆除较大的油滴并产生较小的油滴。

3. 发明授权

US06872230B2 Lubricity additives for low sulfur hydrocarbon fuels 失效
标题翻译：低硫烃燃料的润滑添加剂
公开(公告)号：US06872230B2
公开(公告)日：2005-03-29
申请号：US10197307
申请日：2002-07-16
申请人： Collin W. Cross , Zen-Yu Chang , S. Blake Pruett , Alan E. Goliaszewski
发明人： Collin W. Cross , Zen-Yu Chang , S. Blake Pruett , Alan E. Goliaszewski
IPC分类号： C10L1/14 , C10L1/22 , C10L1/222 , C10L1/232 , C10L1/18
CPC分类号： C10L10/08 , C10L1/14 , C10L1/2227 , C10L1/232
摘要： The present invention relates to additives for enhancing the lubricity of hydrocarbon fuel oils, the inventive additive composition including one or more of the reaction products of (i) an alkylated polyamine and (ii) urea or isocyanate, or the salt adducts of these reaction products. More particularly, the present invention provides for a process for improving the lubricity of hydrocarbon fuel oils, which are low in inherent lubricity due to treatment to reduce sulfur and aromatic components for improved emissions.
摘要翻译：本发明涉及用于增强烃燃料油的润滑性的添加剂，本发明的添加剂组合物包括一种或多种（i）烷基化多胺和（ii）脲或异氰酸酯的反应产物或这些反应产物的盐加合物。更具体地说，本发明提供了一种用于改善烃燃料油的润滑性的方法，由于用于减少硫和芳族组分以改善排放物的处理，固体润滑性低。

4. 发明授权

US5981288A Methods for determining the concentration of surfactants in hydrocarbons 失效
标题翻译：确定烃类中表面活性剂浓度的方法
公开(公告)号：US5981288A
公开(公告)日：1999-11-09
申请号：US949318
申请日：1997-10-14
申请人： Wiley L. Parker , Alan E. Goliaszewski , Nancy R. Calvert
发明人： Wiley L. Parker , Alan E. Goliaszewski , Nancy R. Calvert
IPC分类号： G01N33/28 , G01N33/00
CPC分类号： G01N33/2805 , Y10T436/163333 , Y10T436/173845 , Y10T436/182 , Y10T436/200833 , Y10T436/201666 , Y10T436/203332 , Y10T436/25375
摘要： The present invention provides for a method and system for determining the concentration of a surfactant in a transparent hydrocarbon by performing the steps of adding a solid to the hydrocarbon; adding a second masking reagent to the hydrocarbon; mixing to form a dispersion; separating the dispersion from the mixture; and measuring the optical absorption of the dispersion.
摘要翻译：本发明提供了一种通过以下步骤确定透明烃中的表面活性剂的浓度的方法和系统：向烃中加入固体; 向所述烃中加入第二掩蔽试剂; 混合形成分散体; 从混合物中分离分散体; 并测量分散体的光吸收。

5. 发明授权

US5476988A Settling aids for solids in hydrocarbons 失效
标题翻译：沉淀碳氢化合物固体助剂
公开(公告)号：US5476988A
公开(公告)日：1995-12-19
申请号：US248927
申请日：1994-05-25
申请人： Paul R. Hart , Wiley L. Parker , Alan E. Goliaszewski , April Jean , Scott E. Lehrer
发明人： Paul R. Hart , Wiley L. Parker , Alan E. Goliaszewski , April Jean , Scott E. Lehrer
IPC分类号： B01D21/01 , B01J38/72 , C07C7/00 , C10G11/18 , C10G29/20 , C10G29/00
CPC分类号： C10G11/182 , B01D21/01 , B01J38/72 , C07C7/00 , C10G29/20 , Y02P20/584
摘要： A method for accelerating the settling of finely divided solids in hydrocarbon fluids comprising adding to the hydrocarbon a sufficient settling amount of quaternary fatty ammonium compound. Preferably, the hydrocarbon is a fluid catalytic cracker slurry containing spent catalyst fines.
摘要翻译：一种用于加速烃流体中细分固体沉降的方法，包括向烃中加入足够的沉淀量的季脂肪铵化合物。优选地，烃是含有废催化剂细粉的流化催化裂化浆。

6. 发明授权

US06328943B1 Inhibition of pyrophoric iron sulfide activity 失效
标题翻译：抑制自发硫化铁活性
公开(公告)号：US06328943B1
公开(公告)日：2001-12-11
申请号：US09112882
申请日：1998-07-09
申请人： Paul V. Roling , Wiley L. Parker , Alan E. Goliaszewski , Timothy S. Williams , Bernard C. Groce , Quincy K. A. Sintim
发明人： Paul V. Roling , Wiley L. Parker , Alan E. Goliaszewski , Timothy S. Williams , Bernard C. Groce , Quincy K. A. Sintim
IPC分类号： C01B1716
CPC分类号： C01G49/12
摘要： Methods for inhibiting pyrophoric iron sulfide activity are disclosed. Methods are disclosed for inhibiting the sulfidation of iron oxides to iron sulfides and/or the oxidation of iron sulfide to inhibit pyrophoric activity. The methods comprise contacting iron oxides and/or iron sulfide with a liquid, solution, aerosol, or gaseous inhibitor comprising alkylamines, arylamines, imines; oxygen-containing compounds such as alcohols, aldehydes, esters, acids and ketones; mixed nitrogen-containing and oxygen-containing compounds such as alkanolamines, non-polymeric amides, hydroxylamines, Mannich products, polyisobutylenesuccinimides, oximes; sulfur-containing compounds and phosphorus-containing compounds.
摘要翻译：公开了抑制自发性硫化铁活性的方法。公开了用于抑制铁氧化物硫化成铁硫化物和/或硫化铁的氧化以抑制发火活性的方法。所述方法包括使铁氧化物和/或硫化铁与包含烷基胺，芳基胺，亚胺的液体，溶液，气溶胶或气体抑制剂接触; 含氧化合物如醇，醛，酯，酸和酮; 混合的含氮和含氧化合物如烷醇胺，非聚合酰胺，羟胺，曼尼希产品，聚异丁烯琥珀酰亚胺，肟; 含硫化合物和含磷化合物。

7. 发明申请

US20110301061A1 HIGH THROUGHPUT EXPERIMENTATION METHODS FOR PHASE SEPARATION 审中-公开
标题翻译：用于相分离的高速实验方法
公开(公告)号：US20110301061A1
公开(公告)日：2011-12-08
申请号：US12795217
申请日：2010-06-07
申请人： Cato Russell McDaniel , David B. Engel , Alan E. Goliaszewski
发明人： Cato Russell McDaniel , David B. Engel , Alan E. Goliaszewski
IPC分类号： C40B30/10 , C40B60/12
CPC分类号： G01N33/2823 , B01F3/0807 , B01F11/0014 , C10G33/08 , C10G2300/80
摘要： A process for testing the effectiveness of demulsifying additives on oil/water emulsions includes adding samples containing differing combinations of oil, water and demulsifier to a plurality of elongate reactor vials, wherein each the elongate reactor vial has a longitudinal axis extending from its bottom to its rim. The plurality of reactor vials are placed into a reaction block mounted on a platform of a shaker, wherein the reactor vials are received in stations of the reaction block in a vertical orientation such that the longitudinal axis of each reactor vial is perpendicular to the platform. The reaction block is pivoted the so that the longitudinal axis of each reactor vial is parallel with the platform in a horizontal orientation. The method further includes agitating the reactor vials with the shaker to simultaneously form an oil/water emulsion in each reactor vial while the reactor vials are in the horizontal orientation and then pivoting the reaction block to return the reactor vials to a vertical orientation. The demulsification of the oil/water emulsion in the plurality of reactor vials is observed with the reactor vials in the vertical orientation. In one embodiment, the method further includes using an imaging device to record the demulsification of the oil/water emulsion.
摘要翻译：用于测试乳化添加剂对油/水乳液的有效性的方法包括将含有油，水和破乳剂的不同组合的样品添加到多个细长反应器小瓶中，其中每个细长反应器小瓶具有从其底部延伸到其的轮缘。将多个反应器小瓶放置在安装在振荡器的平台上的反应块中，其中反应器小瓶以垂直方向接收在反应块的站中，使得每个反应器小瓶的纵向轴线垂直于平台。反应块枢转，使得每个反应器小瓶的纵向轴线在水平方向上与平台平行。该方法还包括用振荡器搅拌反应器小瓶，以在每个反应器小瓶中同时形成油/水乳剂，同时反应器小瓶处于水平取向，然后枢转反应块以将反应器小瓶返回到垂直取向。在反应器小瓶中以垂直取向观察多个反应器小瓶中的油/水乳液的破乳。在一个实施方案中，该方法还包括使用成像装置记录油/水乳液的破乳。

8. 发明授权

US07740750B2 Application of visbreaker analysis tools to optimize performance 有权
标题翻译：应用减粘剂分析工具优化性能
公开(公告)号：US07740750B2
公开(公告)日：2010-06-22
申请号：US11456128
申请日：2006-07-07
申请人： Andre Vanhove , Tiffany N. Morris , Alan E. Goliaszewski , Brian W. Lasiuk , Donato Vinciguerra
发明人： Andre Vanhove , Tiffany N. Morris , Alan E. Goliaszewski , Brian W. Lasiuk , Donato Vinciguerra
IPC分类号： C10G9/16
CPC分类号： G01N21/534 , C10G9/007 , G01N15/0612 , G01N21/05 , G01N21/51 , G01N21/5911 , G01N33/28 , G01N2021/0346
摘要： A system and method for quantifying opaque inhomogeneities within a fluid sample. The system uses an optical lens system to focus a light beam onto a stage where the sample is introduced. The light beam is directed onto the sample in a pattern such that the intensity of transmitted light is measured as a function of path length. A photo detector measures the transmitted light through the sample. Fluctuations in transmitted light intensity are then correlated with detection of opaque inclusions in the sample. The system also includes an automated program which utilizes these optical concentration measurements to determine the fouling potential of visbroken tars, and regulates the introduction of chemical inhibitors into a visbreaker unit to improve the yield of light streams and/or economic value of product.
摘要翻译：用于量化流体样品中不透明不均匀性的系统和方法。该系统使用光学透镜系统将光束聚焦到引入样品的台上。光束以图案的形式被引导到样品上，使得测量透射光的强度作为路径长度的函数。光检测器测量通过样品的透射光。然后透射光强度的波动与样品中不透明夹杂物的检测相关。该系统还包括一个自动程序，利用这些光学浓度测量来确定减粘裂纹的污垢势，并且调节将化学抑制剂引入到抗裂解单元中以提高轻质物流的产率和/或产品的经济价值。

9. 发明授权

US5910469A Crude oil composition comprising an alkylphosphonate antifouling additive 失效
标题翻译：包含烷基膦酸盐防污添加剂的原油组合物
公开(公告)号：US5910469A
公开(公告)日：1999-06-08
申请号：US742726
申请日：1996-11-01
申请人： William S. Carey , Jeffrey H. Peltier , Alan E. Goliaszewski
发明人： William S. Carey , Jeffrey H. Peltier , Alan E. Goliaszewski
IPC分类号： C10G9/16 , C10G75/04 , C10M137/12
CPC分类号： C10G9/16 , C10G75/04 , Y10S585/95
摘要： Alkylphosphonate ester compounds or acids thereof are disclosed as effective fouling inhibitors in liquid hydrocarbonaceous medium undergoing processing at elevated temperatures.
摘要翻译：烷基膦酸酯化合物或其酸被公开为在高温下进行加工的液体烃类介质中的有效结垢抑制剂。

10. 发明授权

US5512183A Alkyl-allylphosphonate copolymer used for boiler water treatment 失效
标题翻译：用于锅炉水处理的烷基 - 烯丙基膦酸酯共聚物
公开(公告)号：US5512183A
公开(公告)日：1996-04-30
申请号：US350879
申请日：1994-12-07
申请人： Scott M. Boyette , Alan E. Goliaszewski
发明人： Scott M. Boyette , Alan E. Goliaszewski
IPC分类号： C02F5/14
CPC分类号： C02F5/14
摘要： A water soluble isopropenylphosphonic acid copolymer composition and method of use thereof are disclosed. The copolymer comprises repeat units (a) of the formula: ##STR1## wherein X=OH or OM, wherein M is a cation, and repeat units (b) of the formula: ##STR2## wherein R.sub.1 and R.sub.2 are independently hydrogen, C.sub.1-10 linear or branched alkyl, phenyl or alkyl substituted phenyl. The copolymers are effective in inhibiting the precipitation of scale forming salts and also act to inhibit corrosion in boiler water systems.
摘要翻译：公开了一种水溶性异丙烯基膦酸共聚物组合物及其使用方法。共聚物包含下式的重复单元（a）：其中X = OH或OM，其中M为阳离子，并具有下式的重复单元（b）：其中R 1和R 2独立地为氢，C 1 -10直链或支链烷基，苯基或烷基取代的苯基。共聚物有效抑制垢形成盐的沉淀，并且还起到抑制锅炉水体系中的腐蚀作用。

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