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1. 发明授权

US4128568A Process for the continuous preparation of polydiorganosiloxanes 失效
标题翻译：连续制备聚二有机硅氧烷的方法
公开(公告)号：US4128568A
公开(公告)日：1978-12-05
申请号：US875025
申请日：1978-02-02
申请人： Werner Buchner , Bruno Degen , Ludwig Fries , Judat Helmut , Rudolf Mundil , Karl-Heinz Rudolph
发明人： Werner Buchner , Bruno Degen , Ludwig Fries , Judat Helmut , Rudolf Mundil , Karl-Heinz Rudolph
IPC分类号： C08G77/00 , C08G77/06 , C08G77/42 , C07F7/08
CPC分类号： C08G77/06
摘要： A process for the production of polymeric organosiloxanes comprising reacting diorganosiloxanes with substances regulating the chain length in the presence of alkaline and/or acid reaction catalysts and wherein the polymerization takes place in a reactor consisting of several zones and is provided with stirring or conveying elements, the arrangement of the stirring or conveying elements being such that the flow of material produced by the stirring or conveying element in each zone is the opposite of that in the adjacent zone or zones.
摘要翻译：一种用于生产聚合物有机硅氧烷的方法，其包括在碱性和/或酸性反应催化剂存在下使二有机硅氧烷与调节链长的物质反应，并且其中聚合在由几个区组成的反应器中进行，并且具有搅拌或输送元件，搅拌或输送元件的布置使得由每个区域中的搅拌或输送元件产生的材料的流动与相邻区域或区域中的相反。

2. 发明授权

US3939195A Preparation of silanol containing organopolysiloxanes 失效
标题翻译：含硅烷醇的有机聚硅氧烷的制备
公开(公告)号：US3939195A
公开(公告)日：1976-02-17
申请号：US539150
申请日：1975-01-07
申请人： Hans Joachim Lucking , Klaus Seyfried , Werner Buchner , Karl-Heinz Rudolph
发明人： Hans Joachim Lucking , Klaus Seyfried , Werner Buchner , Karl-Heinz Rudolph
IPC分类号： C08G77/00 , C08G77/06 , C08G77/08 , C08G77/16 , C08G77/20 , C08G77/22 , C08G77/32 , C07F7/08
CPC分类号： C08G77/20 , C08G77/16
摘要： A process for the preparation of an organopolysiloxanol comprising contacting at least one organochlorosilane of the formula(CH.sub.3).sub.a (C.sub.2 H.sub.5).sub.b (CH.sub.2 = CH --).sub.c SiCl.sub.4-a-b-cWhereina, b and c is 0, 1, 2 or 3And wherein2 .ltoreq. a+b+c .ltoreq. 3At a temperature of about -10.degree. to 90.degree.C with water containing NH.sub.4 Cl in an amount from 1 to 100 percent of its saturation concentration, the pH value of the aqueous solution being adjusted to between about 7.5 and 11.6 by introduction of NH.sub.3, separating the hydrolyzate from the aqueous solution immediately after hydrolysis, and flushing the hydrolyzate with an inert gas, to remove NH.sub.3 therefrom.
摘要翻译：一种制备有机聚硅氧烷的方法，包括使至少一种式（CH 3）a（C 2 H 5）b（CH 2 = CH - ）c SiCl 4-abc，其中A和B分别为0,2,2或3的有机氯硅烷和在约-10℃至90℃的温度下，在含有其饱和浓度的1至100％的量的含有NH 4 Cl的水的温度下，水溶液的pH值为通过引入NH 3调节至约7.5至11.6，水解后立即将水解产物与水溶液分离，并用惰性气体冲洗水解产物，以从其中除去NH 3。

3. 发明授权

US4060537A Preparation of organosiloxanes 失效
标题翻译：有机硅氧烷的制备
公开(公告)号：US4060537A
公开(公告)日：1977-11-29
申请号：US747262
申请日：1976-12-03
申请人： Gunther Maass , Hans Joachim Lucking , Werner Buchner , Bruno Degen
发明人： Gunther Maass , Hans Joachim Lucking , Werner Buchner , Bruno Degen
IPC分类号： C08G77/00 , C07F7/08 , C07F7/18 , C07F7/21 , C08G77/06
CPC分类号： C07F7/21 , C07F7/0874
摘要： In the preparation of cyclic and linear organosiloxanes by reacting an organohalogenosilane with a compound of the formulaROR'in whichR is an alkyl radical with 1-4 C atoms, andR' is hydrogen or an alkyl radical with 1-4 C atoms,The improvement which comprises effecting the reaction in an aqueous solution of a Lewis acid. Preferably the organohalogenosilane is a di- or tri-organo-chloro or -bromo-silane wherein the organo radical is selected from the group consisting of alkyl or alkenyl of up to 4 C atoms or aryl, especially dimethyldichlorosilane, and the Lewis acid is a 40-90% solution of ZnCl.sub.2, FeCl.sub.3, CdCl.sub.2 or H.sub.2 SO.sub.4. Advantageously ROR' is methanol, ethanol, propanol, dimethyl ether or diethyl ether.
摘要翻译：在通过有机卤代硅烷与式ROR'的化合物（其中R是具有1-4个C原子的烷基，R'是氢或具有1-4个C原子的烷基）反应制备环状和线性有机硅氧烷的过程中，其包含在路易斯酸的水溶液中影响反应的改进。优选地，有机卤代硅烷是二 - 或三 - 有机氯或溴 - 硅烷，其中有机基团选自由高达4个C原子的烷基或烯基或芳基，特别是二甲基二氯硅烷组成的组，路易斯酸是 40-90％的ZnCl2，FeCl3，CdCl2或H2SO4溶液。有利的是ROR是甲醇，乙醇，丙醇，二甲醚或乙醚。

4. 发明授权

US4202929A Production of non-stick coatings 失效
标题翻译：生产不粘涂料
公开(公告)号：US4202929A
公开(公告)日：1980-05-13
申请号：US949316
申请日：1978-10-06
申请人： Armand de Montigny , Hans Toepsch , Werner Buchner
发明人： Armand de Montigny , Hans Toepsch , Werner Buchner
IPC分类号： C08J7/04 , B05D5/08 , B05D7/04 , B05D7/24 , B32B27/00 , C08G18/61 , C08G77/388 , C08L83/04 , D21H19/32 , C08G47/02 , B32B9/04
CPC分类号： D21H19/32 , C08G18/61 , C08G77/388 , C08L83/04 , C08G77/16 , C08G77/24 , Y10S528/901 , Y10T428/31663
摘要： In the production of non-adherent coated paper substrate by applying to the substrate a solvent-containing mixture comprising (A) an .alpha.,.omega.-polyorganosiloxanediol, (B) an organosiloxane containing Si-H groups, (C) an alkyl- or alkenyl-triacetoxysiloxane, (D) an organic isocyanate with more than two isocyanate radicals and (E) a hardening catalyst, and then heating the substrate to harden the coating, the improvement which comprises including in the mixture applied to the substrate a reaction product (F) of a chloromethylpolymethylsiloxane of the formulaClCH.sub.2 (CH.sub.3).sub.2 Si[OSi(CH.sub.3)CH.sub.2 Cl].sub.n OSi(CH.sub.3).sub.2 Clwherein n is from 2 - about 200, with at most an equivalent molar amount of a primary alkyl, alkenyl or cycloalkyl amine with about 4-18 carbon atoms, e.g. butylamine, hexylamine, cyclohexylamine, 2-ethylhexylamine and allylamine. The coating hardens in a very short time in a drying oven but at normal temperatures the mass has a relatively long pot life.
摘要翻译：在通过向基材施加含有（A）α，ω-聚有机硅氧烷二醇，（B）含Si-H基的有机硅氧烷，（C）烷基 - 或烯基（D）具有多于两个异氰酸酯基团的有机异氰酸酯和（E）硬化催化剂，然后加热基材以使涂层硬化，其改进包括在施加到基材上的混合物中加入反应产物（F ）式ClCH 2（CH 3）2 Si [OSi（CH 3）CH 2 Cl] nOSi（CH 3）2 Cl的氯甲基聚甲基硅氧烷，其中n为2-约200，最多等摩尔量的伯烷基，烯基或环烷基胺与约4-18个碳原子，例如丁胺，己胺，环己胺，2-乙基己基胺和烯丙胺。涂层在干燥炉中在很短的时间内硬化，但在常温下，使用寿命较长。

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