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1. 发明授权

US08877861B2 One-pot synthetic method for synthesizing silver-containing waterborne polyurethane 有权
标题翻译：含银水性聚氨酯的一锅合成方法
公开(公告)号：US08877861B2
公开(公告)日：2014-11-04
申请号：US12264634
申请日：2008-11-04
申请人： Wei-Ho Ting , Shenghong A. Dai , Tzu-Wen Kuo , Ru-Jong Jeng
发明人： Wei-Ho Ting , Shenghong A. Dai , Tzu-Wen Kuo , Ru-Jong Jeng
IPC分类号： C08G18/00 , C08L75/00 , C08G18/28 , C08G18/08 , C08K3/20 , B32B27/00 , B32B27/40 , A01N25/00 , A01N59/16 , A61K33/38 , C08L75/04 , C08K3/08 , C08K3/00
CPC分类号： C08L75/04 , C08K3/015 , C08K3/08 , Y10T428/31551 , Y10T428/31605 , Y10T428/31609
摘要： The present invention relates to a one-pot synthetic method for synthesizing silver-containing waterborne polyurethane (WBPU). The method includes the steps of adding a silver ion-containing solution, such as silver nitrate solution, into WBPU emulsion to form a silver-containing PU emulsion by stirring, and dehydrating the silver-containing PU emulsion so as to obtain a WBPU containing nano-scaled silver particles having a uniform particle size and good dispersibility. The present invention provides a method that can be easily and speedily operated, and the silver-containing WBPU prepared according to the method of the present invention exhibits excellent antibacterial, bactericidal and deodorant effects but using a small amount of silver.
摘要翻译：本发明涉及一种合成含银水性聚氨酯（WBPU）的一锅合成方法。该方法包括以下步骤：通过搅拌将含有银离子的溶液（例如硝酸银溶液）加入到WBPU乳液中以形成含银PU乳液，并将含银PU乳液脱水以获得含有WBPU的纳米颗粒具有均匀粒度和良好分散性的均匀银粒子。本发明提供了一种易于操作的方法，并且根据本发明的方法制备的含银WBPU显示出优异的抗细菌，杀菌和除臭效果，但使用少量的银。

2. 发明申请

US20100113686A1 ONE-POT SYNTHETIC MEHTOD FOR SYNTHESIZING SILVER-CONTAINING WATERBORNE POLYURETHANE 审中-公开
标题翻译：用于合成含银水性聚氨酯的单磷酸合成酶
公开(公告)号：US20100113686A1
公开(公告)日：2010-05-06
申请号：US12264634
申请日：2008-11-04
申请人： Wei-Ho Ting , Shenghong A. Dai , Tzu-Wen Kuo , Ru-Jong Jeng
发明人： Wei-Ho Ting , Shenghong A. Dai , Tzu-Wen Kuo , Ru-Jong Jeng
IPC分类号： C08L75/04
CPC分类号： C08L75/04 , C08K3/015 , C08K3/08 , Y10T428/31551 , Y10T428/31605 , Y10T428/31609
摘要： The present invention relates to a one-pot synthetic method for synthesizing silver-containing waterborne polyurethane (WBPU). The method includes the steps of adding a silver ion-containing solution, such as silver nitrate solution, into WBPU emulsion to form a silver-containing PU emulsion by stirring, and dehydrating the silver-containing PU emulsion so as to obtain a WBPU containing nano-scaled silver particles having a uniform particle size and good dispersibility. The present invention provides a method that can be easily and speedily operated, and the silver-containing WBPU prepared according to the method of the present invention exhibits excellent antibacterial, bactericidal and deodorant effects but using a small amount of silver.
摘要翻译：本发明涉及一种合成含银水性聚氨酯（WBPU）的一锅合成方法。该方法包括以下步骤：通过搅拌将含有银离子的溶液（例如硝酸银溶液）加入到WBPU乳液中以形成含银PU乳液，并将含银PU乳液脱水以获得含有WBPU的纳米颗粒具有均匀粒度和良好分散性的均匀银粒子。本发明提供了一种易于操作的方法，并且根据本发明的方法制备的含银WBPU显示出优异的抗细菌，杀菌和除臭效果，但使用少量的银。

3. 发明申请

US20110118423A1 DEVELOPMENT OF A CROSS-LINKED EPOXY RESIN WITH FLAME-RETARDANT PROPERTIES 有权
标题翻译：开发具有阻燃性能的交联环氧树脂
公开(公告)号：US20110118423A1
公开(公告)日：2011-05-19
申请号：US13011911
申请日：2011-01-23
申请人： WEN-CHIUNG SU , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
发明人： WEN-CHIUNG SU , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
IPC分类号： C08G59/14
CPC分类号： C08G59/1477 , C08G59/184 , C08G59/5033 , C08L63/00
摘要： The invention discloses a cross-linked epoxy resin with flame-retardant properties and method for producing the same. The polymeric material of the invention includes an epoxy resin, a curing agent and a modification agent. Particularly, the modification agent is a derivative of 9,10-Dihydro-9-oxa-10-phosphaphenanthrene 10-oxide (DOPO). Moreover, the curing agent is 4,4′-diaminodiphenyl methane (DDM), or tris(4-aminophenyl)amine (NNH).
摘要翻译：本发明公开了具有阻燃性的交联型环氧树脂及其制造方法。本发明的聚合物材料包括环氧树脂，固化剂和改性剂。特别地，改性剂是9,10-二氢-9-氧杂-10-磷杂菲10氧化物（DOPO）的衍生物。此外，固化剂是4,4'-二氨基二苯基甲烷（DDM）或三（4-氨基苯基）胺（NNH）。

4. 发明授权

US07981980B2 Development of a cross-linked epoxy resin with flame-retardant properties 有权
标题翻译：开发具有阻燃性能的交联环氧树脂
公开(公告)号：US07981980B2
公开(公告)日：2011-07-19
申请号：US13011911
申请日：2011-01-23
申请人： Wen-Chiung Su , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
发明人： Wen-Chiung Su , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
IPC分类号： C08K5/5313 , C08L63/02
CPC分类号： C08G59/1477 , C08G59/184 , C08G59/5033 , C08L63/00
摘要： The invention discloses a cross-linked epoxy resin with flame-retardant properties and method for producing the same. The polymeric material of the invention includes an epoxy resin, a curing agent and a modification agent. Particularly, the modification agent is a derivative of 9,10-Dihydro-9-oxa-10-phosphaphenanthrene 10-oxide (DOPO). Moreover, the curing agent is 4,4′-diaminodiphenyl methane (DDM), or tris(4-aminophenyl)amine (NNH).
摘要翻译：本发明公开了具有阻燃性的交联型环氧树脂及其制造方法。本发明的聚合物材料包括环氧树脂，固化剂和改性剂。特别地，改性剂是9,10-二氢-9-氧杂-10-磷杂菲10氧化物（DOPO）的衍生物。此外，固化剂是4,4'-二氨基二苯基甲烷（DDM）或三（4-氨基苯基）胺（NNH）。

5. 发明申请

US20100130698A1 DEVELOPMENT OF A NOVEL CROSS-LINKED EPOXY RESIN WITH FLAME-RETARDANT PROPERTIES 有权
标题翻译：开发具有阻燃性能的新型交联环氧树脂
公开(公告)号：US20100130698A1
公开(公告)日：2010-05-27
申请号：US12276654
申请日：2008-11-24
申请人： WEN-CHIUNG SU , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
发明人： WEN-CHIUNG SU , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
IPC分类号： C08G59/14
CPC分类号： C08G59/1477 , C08G59/184 , C08G59/5033 , C08L63/00
摘要： The invention discloses a novel cross-linked epoxy resin with flame-retardant properties and method for producing the same. The polymeric material of the invention includes an epoxy resin, a curing agent and a modification agent. Particularly, the modification agent is a derivative of 9,10-Dihydro-9-oxa-10-phosphaphenanthrene 10-Oxide (DOPO). Moreover, the curing agent is 4,4′-diaminodiphenyl methane (DDM), or tris(4-aminephenyl)amine (NNH).
摘要翻译：本发明公开了一种具有阻燃性能的新型交联环氧树脂及其制造方法。本发明的聚合物材料包括环氧树脂，固化剂和改性剂。特别地，改性剂是9,10-二氢-9-氧杂-10-磷杂菲10-氧化物（DOPO）的衍生物。此外，固化剂是4,4'-二氨基二苯基甲烷（DDM）或三（4-氨基苯基）胺（NNH）。

6. 发明授权

US07897702B2 Epoxy resin, curing agent and 9,10-Dihydro-9-oxa-10-phosphaphenanthrene derivative 有权
标题翻译：环氧树脂，固化剂和9,10-二氢-9-氧杂-10-磷杂菲衍生物
公开(公告)号：US07897702B2
公开(公告)日：2011-03-01
申请号：US12276654
申请日：2008-11-24
申请人： Wen-Chiung Su , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
发明人： Wen-Chiung Su , Chun-Ku Liu , Ru-Jong Jeng , Shenghong A. Dai , Ching-Hsuan Lin
IPC分类号： C08K5/5313 , C08L63/02
CPC分类号： C08G59/1477 , C08G59/184 , C08G59/5033 , C08L63/00
摘要： The invention discloses a novel cross-linked epoxy resin with flame-retardant properties and method for producing the same. The polymeric material of the invention includes an epoxy resin, a curing agent and a modification agent. Particularly, the modification agent is a derivative of 9,10-Dihydro-9-oxa-10-phosphaphenanthrene 10-Oxide (DOPO). Moreover, the curing agent is 4,4′-diaminodiphenyl methane (DDM), or tris(4-aminephenyl)amine (NNH).
摘要翻译：本发明公开了一种具有阻燃性能的新型交联环氧树脂及其制造方法。本发明的聚合物材料包括环氧树脂，固化剂和改性剂。特别地，改性剂是9,10-二氢-9-氧杂-10-磷杂菲10-氧化物（DOPO）的衍生物。此外，固化剂是4,4'-二氨基二苯基甲烷（DDM）或三（4-氨基苯基）胺（NNH）。

7. 发明申请

US20090048418A1 Organic polyurethane shape memory material and a preparation method thereof 有权
标题翻译：有机聚氨酯形状记忆材料及其制备方法
公开(公告)号：US20090048418A1
公开(公告)日：2009-02-19
申请号：US11889867
申请日：2007-08-17
申请人： Wen-Chiung Su , Cheng-Che Tsai , Ching-Shiang Yu , Shenghong A. Dai , Ru-jong Jeng
发明人： Wen-Chiung Su , Cheng-Che Tsai , Ching-Shiang Yu , Shenghong A. Dai , Ru-jong Jeng
IPC分类号： C08G18/72 , C08G18/18
CPC分类号： C08G18/4277 , C08G18/2825 , C08G18/3275 , C08G18/714 , C08G18/7671 , C08G83/003 , C08G2280/00
摘要： An organic polyurethane shape memory material and a preparation method thereof are disclosed. The organic polyurethane shape memory material includes a C10 chain or C18 chain and it consists of hard segment and soft segment. The preparation method thereof includes the steps of:The single-chain type dendrimer reacts with diethylenetriamine to produce multiple chains type dendrimer. And then at least one type dendrimer reacts with N-(3-aminopropyl)diethanolamine to produce at least one type dendritic diols. Next polymer HO(C6H10O2)xC2H4OC2H4(C6H10O2)yOH, x+y=25˜26 reacts with methylenedi-p-phenyl diisocyanate and then at least one type dendritic diols is added to react so as to get organic polyurethane shape memory material. The material of the present invention overcomes shortcoming of metal alloy and ceramic such as poor processability, difficulty in modification and high cost. Moreover, it also increase mechanical properties of polymer.
摘要翻译：公开了一种有机聚氨酯形状记忆材料及其制备方法。有机聚氨酯形状记忆材料包括C10链或C18链，它由硬链段和软链段组成。其制备方法包括以下步骤：单链型树枝状聚合物与二亚乙基三胺反应产生多链型树枝状聚合物。然后至少一种类型的树枝状大分子与N-（3-氨基丙基）二乙醇胺反应以产生至少一种类型的树枝状二醇。下一个聚合物HO（C6H10O2）xC2H4OC2H4（C6H10O2）yOH，x + y = 25〜26与亚甲基二苯基二异氰酸酯反应，然后加入至少一种类型的枝状二醇进行反应，得到有机聚氨酯形状记忆材料。本发明的材料克服了金属合金和陶瓷的缺点，如加工性差，改性困难，成本高等问题。此外，它还增加了聚合物的机械性能。

8. 发明申请

US20080255395A1 Process for producing bis-alkoxylated diols of bisphenol a from spent polycarbonate discs(PC) or PC waste 有权
标题翻译：从废聚碳酸酯盘（PC）或PC废物生产双酚a的双烷氧基化二醇的方法
公开(公告)号：US20080255395A1
公开(公告)日：2008-10-16
申请号：US11978561
申请日：2007-10-30
申请人： Shenghong A. Dai , Chao-Hsing Lin , Hsing-yo Lin , Wei-Zhi Liao
发明人： Shenghong A. Dai , Chao-Hsing Lin , Hsing-yo Lin , Wei-Zhi Liao
IPC分类号： C07C43/02 , C07C41/01
CPC分类号： C07C43/23 , C07C41/01 , C08J11/16 , C08J11/24 , C08J2369/00 , Y02W30/705 , Y02W30/706
摘要： This invention provides one-pot reaction for digesting polycarbonate waste with alkylene glycol in the presence of a basic catalyst at 180° C. under normal atmospheric pressure. The digested product mixture was found to consist of bisphenol A (BPA) and monoalkoxylated and bisalkoxylated diols of BPA. Alkoxylation of BPA and monoalkoxylated diols of BPA is performed by adding urea or urea derivative (or carbonic acid ester or amine ester) to the digested product mixture at a high temperature under normal atmospheric pressure to obtain the final product, i.e., bisalkoxylated diols of BPA in high yield. The bisalkoxylated diols of BPA may be used as raw materials to synthesize polymer such as polyurethane (PU) or polyester.
摘要翻译：本发明提供在碱性催化剂存在下，在正常大气压下在180℃下将聚碳酸酯废料与亚烷基二醇消化的一锅反应。发现消化产物混合物由双酚A（BPA）和BPA的单烷氧基化和双烷氧基化二醇组成。通过在正常大气压下在高温下向消化产物混合物中加入尿素或尿素衍生物（或碳酸酯或胺酯）来进行BPA和BPA的单烷氧基化二醇的烷氧基化，得到最终产物，即BPA的双烷氧基化二醇以高产量。 BPA的双烷氧基化二醇可以用作合成聚氨酯（PU）或聚酯的聚合物的原料。

9. 发明申请

US20070282078A1 Synthesis of aryl N-acylurea from aryl isocyanates or aryl carbodiimides for use as intermediate in novel sequential self-repetitive reaction (SSRR) to form amides, amide-imides and their polymers 审中-公开
标题翻译：芳基N-酰基脲由芳基异氰酸酯或芳基碳二亚胺合成，用作新型顺序自重反应（SSRR）中的中间体，形成酰胺，酰胺 - 酰亚胺及其聚合物
公开(公告)号：US20070282078A1
公开(公告)日：2007-12-06
申请号：US11444306
申请日：2006-06-01
申请人： Shenghong A. Dai , Jiang-Jen Lin , Kuan-Liang Wei , Chih-Heng Wu , Wei-Hsiang Huang
发明人： Shenghong A. Dai , Jiang-Jen Lin , Kuan-Liang Wei , Chih-Heng Wu , Wei-Hsiang Huang
IPC分类号： C08F283/04
CPC分类号： C08G69/02 , C07D209/48 , C08G73/00
摘要： Disclosed is a process for synthesizing an aryl N-acylurea in both high selectivity and high yield, comprising reacting an aryl carbodiimide with a carboxylic acid under mild conditions. Thermolysis of N-acylureas at above about 120° C. gives amides and isocyanates, and the latter will undergo the repetitive reaction sequences in the presence of a carbodiimide catalyst. Based on this unique model, a sequential self-repetitive reaction (SSRR) is also developed in a versatile manner for converting aryl carbodiimides into amides, polyamides, polyamide-imides and polyamide-imide elastomers.
摘要翻译：公开了一种以高选择性和高产率合成芳基N-酰基脲的方法，包括在温和条件下使芳基碳二亚胺与羧酸反应。在约120℃以上热解N-酰基脲得到酰胺和异氰酸酯，后者将在碳二亚胺催化剂存在下经历重复的反应顺序。基于这种独特的模型，还以多功能方式开发顺序自重反应（SSRR），以将芳基碳二亚胺转化为酰胺，聚酰胺，聚酰胺 - 酰亚胺和聚酰胺 - 酰亚胺弹性体。

10. 发明授权

US5143945A Carboxylic acid modified carbon dioxide co-blown polyurethane-polyisocyanurate foams 失效
标题翻译：羧酸改性二氧化碳共挤聚氨酯 - 聚异氰脲酸酯泡沫
公开(公告)号：US5143945A
公开(公告)日：1992-09-01
申请号：US612723
申请日：1990-11-13
申请人： Thomas W. Bodnar , Leslie A. Cole , Shenghong A. Dai
发明人： Thomas W. Bodnar , Leslie A. Cole , Shenghong A. Dai
IPC分类号： C08G18/09 , C08J9/08 , C08J9/12 , C08J9/14
CPC分类号： C08J9/149 , C08G18/092 , C08J9/08 , C08J9/127 , C08J9/147 , C08G2101/0025 , C08G2101/0041 , C08J2203/12 , C08J2203/142 , C08J2205/052 , C08J2205/10 , C08J2375/04 , C08J2379/04
摘要： Disclosed are rigid polyurethane-polyisocyanurate foams prepared from polyisocyanates, polyols, trimer catalysts and a blowing agent mixture comprising (i) a halocarbon, and (ii) an organic carboxylic acid, and, optionally water.The foams have excellent aged K-factor values at fluorocarbon levels reduced by up to 75 percent over prior art materials.
摘要翻译：公开了由多异氰酸酯，多元醇，三聚体催化剂和发泡剂混合物制备的硬质聚氨酯 - 聚异氰脲酸酯泡沫，其包含（i）卤化碳，和（ii）有机羧酸，以及任选的水。与现有技术材料相比，泡沫具有优异的老化K-因子值，氟碳含量降低了75％。

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