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1. 发明授权

US06485657B1 Gamma-ray stabilizer and thermoplastic polymer compound including the said stabilizer 失效
标题翻译： γ射线稳定剂和包括所述稳定剂的热塑性聚合物化合物
公开(公告)号：US06485657B1
公开(公告)日：2002-11-26
申请号：US09485509
申请日：2000-02-11
申请人： Wataru Funakoshi , Tetsuo Kanda , Fumitaka Kondo , Katsushi Sasaki
发明人： Wataru Funakoshi , Tetsuo Kanda , Fumitaka Kondo , Katsushi Sasaki
IPC分类号： G21C512
CPC分类号： C08K5/04 , A61M1/16 , B01D61/30 , B01D65/00 , B01D65/022 , B01D2321/346 , C08K5/005 , C08K5/527 , C08L69/00
摘要： A new gamma-ray stabilizer comprising a combination of 100 parts by weight of a benzyl compound (A) having a specific chemical structure and 0.01 to 10 parts by weight of a pentaerythritol phosphorous ester (B) having a spirocyclic structure. Said stabilizer is preferably blended in such a manner that said (A) is contained in an amount of 0.01 to 10 parts by weight based on 100 parts by weight of a thermoplastic polymer (polycarbonate or the like), and said (B) is contained in an amount of 0.01 to 1 part by weight based on 100 parts by weight of said (A). When the thermoplastic polymer is subjected to gamma-ray irradiation, said stabilizer can efficiently protect the thermoplastic polymer from the deterioration of physical properties and yellowing; and on molding processing, the stabilizer-added polymer is suffered from little color tone deterioration and has excellent color tone, and at the same time, the polymer is scarcely suffered from molecular weight decrease on molding, and exhibits excellent thermal stability, moldability or the like. The thermoplastic polymer (especially polycarbonate) composition containing said stabilizer thus obtained is suitable for medical apparatus and medical material uses, especially a jacket case for an artificial dialyzer.
摘要翻译：包含100重量份具有特定化学结构的苄基化合物（A）和0.01至10重量份具有螺环结构的季戊四醇磷酸酯（B）的组合的新型γ射线稳定剂。所述稳定剂优选以所述（A）的含量相对于100重量份的热塑性聚合物（聚碳酸酯等）为0.01〜10重量份的方式进行配合，所述（B）含有相对于所述（A）100重量份，为0.01〜1重量份。当热塑性聚合物进行γ射线照射时，所述稳定剂可以有效地保护热塑性聚合物免于物理性能的劣化和变黄; 在成型加工中，稳定剂添加聚合物几乎没有色调劣化，并且具有优异的色调，同时聚合物在成型时几乎没有分子量降低，并且显示出优异的热稳定性，成型性或喜欢。含有所得稳定剂的热塑性聚合物（特别是聚碳酸酯）组合物适用于医疗器械和医疗材料用途，尤其适用于人造透析器的外套。

2. 发明授权

US06608165B2 Aromatic polycarbonate and production process therefor 失效
标题翻译：芳香聚碳酸酯及其生产工艺
公开(公告)号：US06608165B2
公开(公告)日：2003-08-19
申请号：US10130048
申请日：2002-05-13
申请人： Wataru Funakoshi , Hiroaki Kaneko , Yuichi Kageyama , Takanori Miyoshi , Katsushi Sasaki
发明人： Wataru Funakoshi , Hiroaki Kaneko , Yuichi Kageyama , Takanori Miyoshi , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： A polycarbonate having excellent color and stability and a production process therefor. In the production of a polycarbonate by melt polycondensing a dihydroxy compound and a carbonic acid diester in the presence of an ester exchange catalyst, the each content of an aldehyde group in the dihydroxy compound and the carbonic acid diester is reduced to 3×10−6 equivalent/mol or less.
摘要翻译：具有优异的颜色和稳定性的聚碳酸酯及其制备方法。在通过在酯交换催化剂的存在下熔融缩聚二羟基化合物和碳酸二酯来制备聚碳酸酯中，二羟基化合物中醛基的各含量碳酸二酯的含量降低至3×10 -6当量/摩尔以下。

3. 发明授权

US06448365B1 Aromatic polycarbonate composition 有权
标题翻译：芳香族聚碳酸酯组合物
公开(公告)号：US06448365B1
公开(公告)日：2002-09-10
申请号：US09959830
申请日：2001-11-08
申请人： Wataru Funakoshi , Masumi Hirata , Hiroaki Kaneko , Yuichi Kageyama , Toru Sawaki , Katsushi Sasaki
发明人： Wataru Funakoshi , Masumi Hirata , Hiroaki Kaneko , Yuichi Kageyama , Toru Sawaki , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： G11B7/2534 , C08G64/06 , C08G64/14 , C08G64/307 , C08K5/52 , C08L69/00
摘要： An aromatic polycarbonate composition which contains 0.05 to 65 ppm of bonded phosphorus atoms to polycarbonate chains and free phosphorus compounds consisting of a tervalent phosphorus compound and a pentavalent phosphorus compound in a specific ratio. It is excellent in transparency, color stability and residence stability at the time of molding and is suitably used in disk substrates.
摘要翻译：一种芳族聚碳酸酯组合物，其含有0.05〜65ppm的键合磷原子与聚碳酸酯链，并且由特定比例的三价磷化合物和五价磷化合物组成的游离磷化合物。在成型时透明度，颜色稳定性和停留稳定性优异，适用于盘基材。

4. 发明授权

US06423813B1 Branched aromatic polycarbonate, and production method and blow-molded article thereof 失效
标题翻译：支链芳族聚碳酸酯及其制造方法和吹塑制品
公开(公告)号：US06423813B1
公开(公告)日：2002-07-23
申请号：US09959075
申请日：2001-10-18
申请人： Wataru Funakoshi , Yuichi Kageyama , Hiroaki Kaneko , Katsushi Sasaki
发明人： Wataru Funakoshi , Yuichi Kageyama , Hiroaki Kaneko , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/14
摘要： A method for producing a high-quality thermoplastic branched polycarbonate which is used in blow-molding, extrusion or vacuum molding from a linear aromatic polycarbonate efficiently. The thermoplastic branched polycarbonate is produced by melt-mixing and reacting a substantially linear aromatic polycarbonate with an acid anhydride having at least two cyclic acid anhydride groups in a molecule in the presence of a basic catalyst.
摘要翻译：一种用于生产由线性芳族聚碳酸酯进行吹塑，挤出或真空成型的高品质热塑性支链聚碳酸酯的方法。通过在碱性催化剂的存在下，使分子内具有至少两个环状酸酐基团的酸酐与基本上线性的芳族聚碳酸酯熔融混合并使其反应来制造热塑性支化聚碳酸酯。

5. 发明授权

US06562936B1 Apparatus and method for producing resin 有权
标题翻译：树脂生产设备及方法
公开(公告)号：US06562936B1
公开(公告)日：2003-05-13
申请号：US09786523
申请日：2001-06-11
申请人： Kazuki Hatono , Masumi Hirata , Hiroaki Kaneko , Toru Sawaki , Wataru Funakoshi , Katsushi Sasaki , Masasi Simonaru , Kouji Kiyoshige
发明人： Kazuki Hatono , Masumi Hirata , Hiroaki Kaneko , Toru Sawaki , Wataru Funakoshi , Katsushi Sasaki , Masasi Simonaru , Kouji Kiyoshige
IPC分类号： C08G6400
CPC分类号： B29C47/767 , B29C47/0009 , B29C47/38 , B29C47/402 , C08G64/205 , C08G64/307
摘要： A method of producing a polycarbonate or the like which is excellent in hydrolysis and heat stability such as a reduction in molecular weight at the time of molding and color retention and moldability such as releasability and transferability, rarely experiences residence deterioration such as coloring, crosslinking and gel formation and has an extremely small content of foreign matter by employing a special structure for an opening in the side surface of a horizontal cylindrical vacuum resin treating apparatus, supplying a molten polycarbonate into a unidirectional rotary intermeshing double-screw extruder under specific conditions, adding a specific agent under specific conditions and cleaning the inner surface of a production apparatus by a specific method.
摘要翻译：水解和热稳定性优异的聚碳酸酯等的制造方法，例如成型时的分子量的降低和保色性以及脱模性和转印性等成型性，很少发生着色，交联等的停留劣化，凝胶形成，并且通过采用水平圆筒形真空树脂处理装置的侧表面中的开口的特殊结构，并且在特定条件下将熔融聚碳酸酯供给到单向旋转啮合双螺杆挤出机中，并且具有非常少的异物含量，在特定条件下的特定试剂，并通过具体方法清洗生产装置的内表面。

6. 发明授权

US06323302B1 Carbonic acid diester, aromatic polycarbonate and facilities, and preparation thereof 有权
标题翻译：碳酸二酯，芳族聚碳酸酯和设备及其制备
公开(公告)号：US06323302B1
公开(公告)日：2001-11-27
申请号：US09445824
申请日：1999-12-14
申请人： Katsushi Sasaki , Wataru Funakoshi , Toru Sawaki , Masumi Hirata , Hiroaki Kaneko , Masanori Abe , Masasi Simonaru , Hidemi Takemoto , Jyuhou Matsuo , Yoshiki Matsuoka
发明人： Katsushi Sasaki , Wataru Funakoshi , Toru Sawaki , Masumi Hirata , Hiroaki Kaneko , Masanori Abe , Masasi Simonaru , Hidemi Takemoto , Jyuhou Matsuo , Yoshiki Matsuoka
IPC分类号： C08G6400
CPC分类号： C08G64/307
摘要： Aromatic polycarbonate having a reduced discoloration and improved heat stability, hue, etc. is provided by keeping a pressure in a raw material melting vessel and the linear velocity of a gas in a transporting piping in a specific range, keeping the concentration of a nitrogen-containing basic compound in a specific range, recycling a byproduct containing specific amounts of impurities, suppressing the amounts of a nitrogen-containing basic compound, metallic elements and a silicic acid derivative in the carbonic acid diester at specific values or less, prescribing the material quality of the reaction facilities, and/or forming an oxide layer at the inner wall surfaces of the reaction facilities.
摘要翻译：通过将原料熔融容器中的压力和输送管道中的气体的线速度保持在特定范围来提供具有减少变色和改善的热稳定性，色相等的芳族聚碳酸酯，保持氮气浓度，含有特定范围的碱性化合物，回收含有特定量的杂质的副产物，抑制碳酸二酯中的含氮碱性化合物，金属元素和硅酸衍生物的量在特定值以下，规定材料质量的反应设备，和/或在反应设备的内壁表面形成氧化物层。

7. 发明授权

US5858499A Polycarbonate copolymer containing oxaspiroundecane group and production process therefor 失效
标题翻译：含有氧杂环十一烷基团的聚碳酸酯共聚物及其制备方法
公开(公告)号：US5858499A
公开(公告)日：1999-01-12
申请号：US769418
申请日：1996-12-19
申请人： Masanori Abe , Keisuke Shinohara , Wataru Funakoshi , Katsushi Sasaki
发明人： Masanori Abe , Keisuke Shinohara , Wataru Funakoshi , Katsushi Sasaki
IPC分类号： C08G64/06 , C08G64/16 , C08G64/30 , G02B1/04 , G02B6/02 , G11B7/24
CPC分类号： C08G64/1608 , C08G64/30 , G02B6/02033
摘要： A polycarbonate copolymer which consists essentially of 5 to 95 mol % of recurring units containing a specific spiroglycol unit and 95 to 5 mol % of recurring units containing a specific biphenol unit, and has a reduced viscosity (.eta..sub.sp /c), measured at 20.degree. C. in a solution containing methylene chloride as a solvent and having a concentration of 0.5 g/dl, of at least 0.3 dl/g, a photoelasticity coefficient of 70.times.10.sup.-13 cm.sup.2 /dyne or less, and a glass transition temperature of at least 95.degree. C.; and a process for the production thereof. This polycarbonate copolymer is useful as a material for an information transmission medium or an information recording medium.
摘要翻译：一种聚碳酸酯共聚物，其基本上由5至95摩尔％的含有特定螺旋体单体的重复单元和95至5摩尔％的含有特定双酚单元的重复单元组成，并且具有在20℃下测量的粘度（η值）在含有二氯甲烷溶剂并且浓度为0.5g / dl，至少0.3dl / g，光弹性系数为70×10-13 cm 2 /达因或更低的溶液中，并且玻璃化转变温度为至少95℃。及其生产方法。该聚碳酸酯共聚物可用作信息传输介质或信息记录介质的材料。

8. 发明授权

US5668202A Process for production of stabilized polycarbonate 失效
标题翻译：生产稳定化聚碳酸酯的方法
公开(公告)号：US5668202A
公开(公告)日：1997-09-16
申请号：US665817
申请日：1996-06-19
申请人： Masumi Hirata , Wataru Funakoshi , Katsushi Sasaki
发明人： Masumi Hirata , Wataru Funakoshi , Katsushi Sasaki
IPC分类号： C08G64/20 , C08G64/30 , C08G64/40 , C08K5/36 , C08K5/41 , C08K5/42 , C08K5/50 , C08L69/00
CPC分类号： C08K5/42 , C08G64/307 , C08K5/41 , C08K5/50 , Y10S524/911 , Y10S524/912 , Y10S524/913
摘要： A process for the production of a stabilized polycarbonate which comprises melt-polycondensing an aromatic dihydroxy compound and a carbonic acid diester in the presence of a polycondensation catalyst and then, after the reaction mixture shows an intrinsic viscosity of at least 0.1, adding at least one stabilizer selected from the group consisting of specific compounds having a sulfonates group sulfonic acid anhydride group or a sulfate group in an amount of 0.01 to 500 ppm of a polycarbonate to be formed, to form a polycarbonate having a desired intrinsic viscosity.
摘要翻译：一种制备稳定化聚碳酸酯的方法，其包括在缩聚催化剂存在下使芳族二羟基化合物和碳酸二酯熔融缩聚，然后在反应混合物的特性粘度至少为0.1之后，加入至少一种选自具有磺酸基磺酸酐基的特定化合物或硫酸酯基的稳定剂，其量为所形成的聚碳酸酯的0.01至500ppm，以形成具有所需特性粘度的聚碳酸酯。

9. 发明授权

US06509435B1 Polycabonate, process for producing the same, and molded article thereof 有权
标题翻译：聚碳酸酯，其制造方法及其成型体
公开(公告)号：US06509435B1
公开(公告)日：2003-01-21
申请号：US09959829
申请日：2001-11-08
申请人： Yuichi Kageyama , Hiroaki Kaneko , Wataru Funakoshi , Katsushi Sasaki
发明人： Yuichi Kageyama , Hiroaki Kaneko , Wataru Funakoshi , Katsushi Sasaki
IPC分类号： C08G6400
CPC分类号： C08G64/307 , C08G64/06 , G11B7/2534
摘要： A polycarbonate which is stable against thermal decomposition at a temperature range for melt molding without adding a heat resistant stabilizer and suitable for the melt molding of a thin product, production method and molded products thereof. The polycarbonate is comprising mainly a recurring unit represented by the following formula (1), and has a percentage of the total of integrated intensities of all signals detected at four ranges, &dgr;=2.14 to 2.17 ppm, &dgr;=3.46 to 3.49 ppm, &dgr;=3.62 to 3.69 ppm and &dgr;=5.42 to 5.46 ppm to the integrated intensity of a signal derived from a methyl group detected at a range of &dgr;=1.50 to 2.00 ppm of 0.01 to 2.0% in its 1H-NMR spectrum in heavy chloroform and a viscosity average molecular weight of 10,000 to 100,000.
摘要翻译：一种在不添加耐热稳定剂并适于熔融成型薄产品的情况下，在熔融成型温度范围内对热分解稳定的聚碳酸酯，其制造方法及其成型体。聚碳酸酯主要包含由下式（1）表示的重复单元，并且具有在四个范围检测的所有信号的积分强度的总和的百分比，Δ= 2.14至2.17ppm，Δ= 3.46至3.49ppm，Δ = 3.62〜3.69ppm，δ= 5.42〜5.46ppm，在重氯仿中的1H-NMR光谱中，在δ= 1.50〜2.00ppm的范围内检测到的甲基衍生的信号的积分强度为0.01〜2.0％粘均分子量为10,000至100,000。

10. 发明授权

US06417291B1 Process for producing polyarylate 失效
标题翻译：多芳基化合物的制备方法
公开(公告)号：US06417291B1
公开(公告)日：2002-07-09
申请号：US09719984
申请日：2000-12-19
申请人： Hiroaki Kaneko , Wataru Funakoshi , Yuichi Kageyama , Katsushi Sasaki
发明人： Hiroaki Kaneko , Wataru Funakoshi , Yuichi Kageyama , Katsushi Sasaki
IPC分类号： C08F2000
CPC分类号： C08G63/84 , C08G63/19 , C08G63/83 , C08G63/916
摘要： In a process for producing a polyarylate through the polycondensation of an aromatic dihydroxy compound and an aromatic ester bond forming precursor, a salicylic acid ester compound having a specific structure is used as a terminal modifying agent. In a process for producing a polyarylate through the polycondensation of an aromatic dihydroxy compound and an ester bond forming aromatic dicarboxylic acid derivative, a polyarylate of high-molecular weight having excellent color tone and hue stability is obtained.
摘要翻译：在通过芳族二羟基化合物和芳香族酯键形成前体的缩聚制备多芳基化合物的方法中，使用具有特定结构的水杨酸酯化合物作为末端改性剂。在通过缩聚反应制备多芳基化合物的方法中，的芳族二羟基化合物和形成酯键的芳族二羧酸衍生物，得到具有优异色调和色调稳定性的高分子量聚芳酯。

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