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1. 发明授权

US4153584A High molecular weight high unsaturation C.sub.4 -C.sub.10 isoolefin conjugated diolefin copolymers and multipolymers containing methylcyclopentadiene 失效
标题翻译：高分子量高不饱和度C {HD 4 {B -C {HD 10 {B异烯烃共轭二烯烃共聚物和含有甲基环戊二烯
公开(公告)号：US4153584A
公开(公告)日：1979-05-08
申请号：US898473
申请日：1978-04-20
申请人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
发明人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
IPC分类号： C08F210/12 , C08C19/30 , C08J3/24 , C08K5/36
CPC分类号： C08F210/12
摘要： Substantially gel-free high unsaturation copolymers of isobutylene and methylcyclopentadiene and high unsaturation terpolymers of isobutylene cyclopentadiene and methylcyclopentadiene and terpolymers of isobutylene, isoprene and methylcyclopentadiene having a number average molecular weight of at least about 120,000 and a mole percent of unsaturation of at least 5% and the process for preparing said polymers which comprises carrying out the polymerization in a homogeneous phase, introducing to the system either an aluminum halide in a soluble form or a hydrocarbylaluminum dihalide and carrying the reaction out at a temperature of less than about -100.degree. C.
摘要翻译：基本上不含凝胶的异丁烯和甲基环戊二烯的高不饱和共聚物和异丁烯环戊二烯和甲基环戊二烯的高不饱和三元共聚物和异丁烯，异戊二烯和甲基环戊二烯的三元共聚物，其数均分子量至少约为120,000，不饱和度的摩尔百分数至少为5％以及制备所述聚合物的方法，其包括在均相中进行聚合，向系统中引入可溶形式的卤化铝或二卤化烃基铝，并在小于约-100℃的温度下进行反应。

2. 发明授权

US4139695A High molecular weight high unsaturation C4-C10 isoolefin conjugated diolefin copolymers and multipolymers containing methylcyclopentadiene 失效
标题翻译：高分子量高不饱和C4-C10异烯烃共轭二烯共聚物和含有甲基环戊二烯的多聚物
公开(公告)号：US4139695A
公开(公告)日：1979-02-13
申请号：US787366
申请日：1977-04-14
申请人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
发明人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
IPC分类号： C08F210/12 , C08L23/22
CPC分类号： C08L23/22 , C08F210/12
摘要： Substantially gel-free high unsaturation copolymers of isobutylene and methylcyclopentadiene and high unsaturation terpolymers of isobutylene cyclopentadiene and methylcyclopentadiene and terpolymers of isobutylene, isoprene and methylcyclopentadiene having a number average molecular weight of at least about 120,000 and a mole percent of unsaturation of at least 5% and the process for preparing said polymers which comprises carrying out the polymerization in a homogeneous phase, introducing to the system either an aluminum halide in a soluble form or a hydrocarbylaluminum dihalide and carrying the reaction out at a temperature of less than about -100.degree. C.
摘要翻译：基本上不含凝胶的异丁烯和甲基环戊二烯的高不饱和共聚物和异丁烯环戊二烯和甲基环戊二烯的高不饱和三元共聚物和异丁烯，异戊二烯和甲基环戊二烯的三元共聚物，其数均分子量至少约为120,000，不饱和度的摩尔百分数至少为5％以及制备所述聚合物的方法，其包括在均相中进行聚合，向系统中引入可溶形式的卤化铝或二卤化烃基铝，并在小于约-100℃的温度下进行反应。

3. 发明授权

US4031300A High molecular weight, high unsaturation isobutylene-cyclopentadiene copolymers 失效
标题翻译：高分子量，高不饱和度的异丁烯 - 环戊二烯共聚物
公开(公告)号：US4031300A
公开(公告)日：1977-06-21
申请号：US631444
申请日：1975-11-13
申请人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
发明人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
IPC分类号： C08F210/12 , C08L23/22 , C08F232/06
CPC分类号： C08L23/22 , C08F210/12
摘要： Substantially gel-free, high molecular weight, high unsaturation copolymers of isobutylene and cyclopentadiene having a number average molecular weight of at least 90,000 and a mole percent of unsaturation of at least 5% and the process for preparing said polymers which comprises carrying out the polymerization in a homogeneous phase, introducing to the system either an aluminum halide in a soluble form or a hydrocarbylaluminum dihalide and carrying the reaction out at a temperature of less than about -100.degree. C.
摘要翻译：具有数均分子量至少为90,000，摩尔百分比不饱和度至少为5％的异丁烯和环戊二烯的基本无凝胶的高不饱和共聚物以及制备所述聚合物的方法包括进行聚合在均相中，向系统中引入可溶形式的卤化铝或二卤化烃基铝，并在小于约-100℃的温度下进行反应。

4. 发明授权

US4215022A Isobutylene cyclodiolefin copolymers and terpolymers 失效
标题翻译：异丁烯环二烯烃共聚物和三元共聚物
公开(公告)号：US4215022A
公开(公告)日：1980-07-29
申请号：US952241
申请日：1978-10-16
申请人： Donald J. Buckley , Warren A. Thaler , Joseph P. Kennedy
发明人： Donald J. Buckley , Warren A. Thaler , Joseph P. Kennedy
IPC分类号： C08F210/10 , C08F210/12 , C08K5/00 , C08F8/34
CPC分类号： C08F210/12 , C08F210/10 , C08K3/06 , C08K5/00 , C08K5/18 , C08K5/44
摘要： Substantially gel free, high molecular weight, high unsaturation copolymers of isobutylene and cyclo-conjugated dienes having a number-average molecular weight of about 30,000 to about 90,000 and a mole % of unsaturation of about 5 to about 45 are prepared by a polymerization in a homogeneous phase, wherein the catalyst which is a hydrocarbyl aluminum dihalide or aluminum halide type catalyst dissolved in an aliphatic type solvent is added to a mixture of the isobutylene, cyclo-conjugated diene, and an aliphatic cosolvent and the polymerization reaction is carried out at a temperature of about -80.degree. to about -110.degree. C.
摘要翻译：基于无凝胶，高分子量，异丁烯和环共轭二烯的高不饱和共聚物，其数均分子量为约30,000至约90,000，不饱和摩尔百分数为约5至约45，通过在均匀相，其中将溶解在脂肪族溶剂中的烃基二卤化铝或卤化铝型催化剂的催化剂加入到异丁烯，环共轭二烯和脂族共溶剂的混合物中，聚合反应在温度约-80℃至约-110℃

5. 发明授权

US4153773A Isobutylene cyclodiolefin copolymers and terpolymers 失效
标题翻译：异丁烯环二烯烃共聚物和三元共聚物
公开(公告)号：US4153773A
公开(公告)日：1979-05-08
申请号：US803596
申请日：1977-06-06
申请人： Donald J. Buckley , Warren A. Thaler , Joseph P. Kennedy
发明人： Donald J. Buckley , Warren A. Thaler , Joseph P. Kennedy
IPC分类号： C08F210/12 , C08L23/22
CPC分类号： C08L23/22 , C08F210/12
摘要： Substantially gel free, high molecular weight, high unsaturation copolymers of isobutylene and cyclo-conjugated dienes having a number-average molecular weight of about 30,000 to about 90,000 and a mole % of unsaturation of about 5 to about 45 are prepared by a polymerization in a homogeneous phase, wherein the catalyst which is a hydrocarbyl aluminum dihalide or aluminum halide type catalyst dissolved in an aliphatic type solvent is added to a mixture of the isobutylene, cyclo-conjugated diene, and an aliphatic cosolvent and the polymerization reaction is carried out at a temperature of about -80.degree. to about -110.degree. C.
摘要翻译：基于无凝胶，高分子量，异丁烯和环共轭二烯的高不饱和共聚物，其数均分子量为约30,000至约90,000，不饱和摩尔百分数为约5至约45，通过在均匀相，其中将溶解在脂肪族溶剂中的烃基二卤化铝或卤化铝型催化剂的催化剂加入到异丁烯，环共轭二烯和脂族共溶剂的混合物中，聚合反应在温度约-80℃至约-110℃

6. 发明授权

US4151343A High unsaturation butyl rubbers 失效
标题翻译：高不饱和丁基橡胶
公开(公告)号：US4151343A
公开(公告)日：1979-04-24
申请号：US788504
申请日：1977-04-18
申请人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
发明人： Warren A. Thaler , Donald J. Buckley , Joseph P. Kennedy
IPC分类号： C08F2/00 , C08F2/04 , C08F4/00 , C08F4/06 , C08F210/00 , C08F210/12 , C08L23/22 , C08F232/06
CPC分类号： C08L23/22 , C08F210/00 , C08F210/12
摘要： Substantially gel-free, high unsaturation copolymers of isoolefin and diolefin and high unsaturation terpolymers of isoolefin, acyclic diene and cyclic diene having a number average molecular weight of at least about 90,000 and a mole percent of unsaturation of at least 5% and the process for preparing said polymers which comprises carrying out the polymerization in a homogeneous phase, introducing to the system either an aluminum halide in a soluble form or a hydrocarbylaluminum dihalide and carrying the reaction out at a temperature of less than about -100.degree. C.

7. 发明授权

US4229325A High unsaturation butyl rubbers with additives 失效
标题翻译：高不饱和丁基橡胶与添加剂
公开(公告)号：US4229325A
公开(公告)日：1980-10-21
申请号：US950417
申请日：1978-10-11
申请人： Warren A. Thaler , Donald J. Buckley , Kennedy Joseph P.
发明人： Warren A. Thaler , Donald J. Buckley , Kennedy Joseph P.
IPC分类号： C08F210/12 , C08L23/22 , C08C19/30 , C08J3/24 , C08K5/36
CPC分类号： C08L23/22 , C08F210/12
摘要： Substantially gel-free, high unsaturation copolymers of isobutylene and isoprene and high unsaturation terpolymers of isobutylene, isoprene and cyclopentadiene having a number average molecular weight of at least about 90,000 and a mole percent of unsaturation of at least 5% and the process for preparing said polymers which comprises carrying out the polymerization in a homogeneous phase, introducing to the system either an aluminum halide in a soluble form or a hydrocarbylaluminum dihalide and carrying the reaction out at a temperature of less than about -100.degree. C. Vulcanizable compositions are formed from the co- and ter- polymers by reacting them with a vulcanizing amount of sulfur donor and a delayed action accelerator, wherein the vulcanized compositions can be extended with fillers, non-polar process oils and rubbers.
摘要翻译：异丁烯和异戊二烯的基本无凝胶的高不饱和度共聚物和异丁烯，异戊二烯和环戊二烯的高不饱和三元共聚物，其数均分子量为至少约90,000，不饱和摩尔百分数为至少5％，制备所述聚合物包括在均相中进行聚合，向系统引入可溶形式的卤化铝或二卤化烃基铝，并在小于约-100℃的温度下进行反应。可硫化的组合物由通过使它们与硫化量的硫供体和延迟作用促进剂反应，其中硫化组合物可以用填料，非极性加工油和橡胶进行扩展。

8. 发明授权

US5872084A Dispersants derived from heavy polyamine and second amine 失效
标题翻译：衍生自重多胺和二胺的分散剂
公开(公告)号：US5872084A
公开(公告)日：1999-02-16
申请号：US7477
申请日：1998-01-15
申请人： Jacob I. Emert , Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
发明人： Jacob I. Emert , Joseph V. Cusumano , David C. Dankworth , William D. Diana , William B. Eckstrom , Keith R. Gorda , Antonio Gutierrez , Jon E. Stanat , Warren A. Thaler , Stephen Zushma
IPC分类号： C10M159/12 , C08F8/00 , C08F8/32 , C10L1/2383 , C10L1/30 , C10L10/00 , C10M129/93 , C10M129/95 , C10M133/56
CPC分类号： C10M133/56 , C08F8/14 , C08F8/32 , C10L1/2383 , C10L1/303 , C10L10/04 , C10M129/93 , C10M129/95 , C10M2207/125 , C10M2207/129 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2215/04 , C10M2215/26 , C10M2217/046 , C10M2217/06
摘要： A Koch functionalized product, which is the reaction product of at least one hydrocarbon with carbon monoxide and a nucleophilic trapping agent, is derivatized with a heavy polyamine and a second amine. The hydrocarbon is a hydrocarbon compound or a hydrocarbon polymer. A heavy polyamine is a mixture of polyamines containing small amounts of lower polyamine oligomers such as tetraethylene pentamine and pentaethylenehexamine and containing primarily oligomers with more than 6 nitrogens and more extensive branching. Rubber seals embrittlement is reduced or minimized.
摘要翻译：作为至少一种烃与一氧化碳和亲核捕集剂的反应产物的Koch官能化产物用重多胺和第二胺衍生化。烃是烃化合物或烃聚合物。重多胺是含有少量下述多胺低聚物如四亚乙基五胺和五亚乙基六胺的多胺的混合物，并且主要含有具有超过6个氮和更广泛支化的低聚物。橡胶密封件脆化减少或最小化。

9. 发明授权

US5691422A Saturated polyolefins having terminal aldehyde or hydroxy substituents and derivatives thereof 失效
标题翻译：具有末端醛或羟基取代基的饱和聚烯烃及其衍生物
公开(公告)号：US5691422A
公开(公告)日：1997-11-25
申请号：US662835
申请日：1996-06-12
申请人： Jacob Emert , Istvan T. Horvath , Richard H. Schlosberg , Warren A. Thaler , David A. Young , Stephen Zushma
发明人： Jacob Emert , Istvan T. Horvath , Richard H. Schlosberg , Warren A. Thaler , David A. Young , Stephen Zushma
IPC分类号： C08F8/00 , C08F8/32 , C08F210/16 , C08F210/18 , C10L1/198 , C10L1/22 , C10L1/238 , C10L1/2383 , C10L1/2387 , C10L10/00 , C10M133/54 , C10M133/58
CPC分类号： C10M133/58 , C08F210/18 , C08F8/00 , C08F8/32 , C10L1/198 , C10L1/238 , C10L1/2383 , C10L1/2387 , C10L10/18 , C10M133/54 , C08F210/16 , C10M2215/04 , C10M2215/042 , C10M2215/22 , C10M2215/221 , C10M2215/225 , C10M2215/226 , C10M2215/26 , C10M2215/30 , C10M2217/046 , C10M2217/06
摘要： A saturated polymer having a terminal aldehyde or hydroxy substituent which may be used directly or in a derivative form as a dispersant for both fuel and lubricating oil compositions, wherein the saturated polymer has a M.sub.n of about 300 to 10,000, and is derived from a polyolefin which is derived from a monomer of the formula H.sub.2 C.dbd.CHR.sup.4, wherein R.sup.4 is hydrogen or a straight or branched chain alkyl radical, and wherein the polyolefin has at least about 30% terminal vinylidene unsaturation. Particularly desirable amine derivatives can be formed by either a single step aminomethylation process or a two step hydroformylation and reductive amination process.
摘要翻译：具有末端醛或羟基取代基的饱和聚合物，其可以直接或以衍生形式用作燃料和润滑油组合物的分散剂，其中饱和聚合物的Mn为约300至10,000，并且衍生自聚烯烃其衍生自式H2C = CHR4的单体，其中R4是氢或直链或支链烷基，并且其中聚烯烃具有至少约30％的末端亚乙烯基不饱和键。特别理想的胺衍生物可以通过单步氨基甲基化方法或两步加氢甲酰化和还原胺化方法形成。

10. 发明授权

US5190797A Coating a substrate with an ionomer 失效
标题翻译：用离聚物涂覆基材
公开(公告)号：US5190797A
公开(公告)日：1993-03-02
申请号：US720042
申请日：1991-06-24
申请人： Warren A. Thaler , Cruise K. Jones , Evelyn N. Drake , Pacifico V. Manalastas , Edward N. Kresge
发明人： Warren A. Thaler , Cruise K. Jones , Evelyn N. Drake , Pacifico V. Manalastas , Edward N. Kresge
IPC分类号： B01J2/00 , B01J2/28 , C05G3/00
CPC分类号： B01J2/28 , B01J2/006 , C05G3/0029
摘要： The present invention relates to a process for the encapsulation of a solid substrate with a neutralized sulfonated polymer, which comprises the steps of: (a) forming a solution of a non-conjugated, diene polymer in a solvent selected from the group consisting of aliphatic, aromatic hydrocarbons and mixtures thereof; (b) contacting the solution of the unsaturated polymer with a sulfonating agent at a sufficient temperature and for a sufficient period of time to form a solution of a sulfonated polymer containing free acid; (c) forming a solution of a base selected from the group consisting of alkali metal hydroxides and mixtures thereof in a mixtrue of an aliphatic alcohol and a hydrocarbon, the hydrocarbon being selected from the group consisting of aliphatic and aromatic hydrocarbons and mixtures thereof; (d) adding the solution of base to the solution of sulfonated polymer in an amount sufficient to neutralize the polymer and the free acid, thereby forming a coating solution; (e) contacting the solid substrate with the coating solution while removing the solvent therefrom, thereby forming an encapsulated substrate. In a preferred embodiment, the solvent removed during step (e) is recovered and distilled to separate the solvent into at least two fractions, a fraction containing substantially hydrocarbon and an alcohol containing fraction. The separated solvents are then recycled to dissolve the polymer in step (a) and to dissolve the base in step (c).
摘要翻译：本发明涉及用中和的磺化聚合物包封固体基质的方法，其包括以下步骤：（a）在选自脂肪族的溶剂中的溶剂中形成非共轭二烯聚合物的溶液，芳族烃及其混合物; （b）在足够的温度下将不饱和聚合物的溶液与磺化剂接触足够的时间以形成含有游离酸的磺化聚合物的溶液; （c）在脂族醇和烃的混合物中形成选自碱金属氢氧化物及其混合物的碱的溶液，所述烃选自脂族和芳族烃及其混合物; （d）将碱溶液以足以中和聚合物和游离酸的量向磺化聚合物溶液中加入，从而形成涂布溶液; （e）将固体基质与涂布溶液接触，同时从其中除去溶剂，由此形成封装的基材。在优选的实施方案中，回收步骤（e）中除去的溶剂并蒸馏以将溶剂分离成至少两个馏分，基本上含有烃和含醇的馏分。然后将分离的溶剂再循环以在步骤（a）中溶解聚合物并在步骤（c）中溶解碱。

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