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    • 9. 发明申请
    • WETTABILITY AND MATRIX IMBIBITION ANALYSIS
    • 可湿性和基质分析分析
    • WO2012087902A2
    • 2012-06-28
    • PCT/US2011/065776
    • 2011-12-19
    • SCHLUMBERGER CANADA LIMITEDSERVICES PETROLIERS SCHLUMBERGERSCHLUMBERGER HOLDINGS LIMITEDSCHLUMBERGER TECHNOLOGY B.V.PRAD RESEARCH AND DEVELOPMENT LIMITEDWILLBERG, DeanPAGELS, MarkusHINKEL, Jerald J.
    • WILLBERG, DeanPAGELS, MarkusHINKEL, Jerald J.
    • G01N13/00G01N1/30G01N33/24
    • G01N13/00G01N1/286
    • A method of determining wettability of a rock sample, such as from a core sample is described. The sample is preferably crushed or comminuted to a particulate size where micro fractures have been eliminated, but where the particles are still large enough to represent the native rock matrix and texture. The comminuted core sample is exposed to a test fluid for a given period of time. The rock sample can be split into many separate aliquots, and a series of tests is performed using a series of different fluids and/or the same fluid for different exposure times. The excess test fluid residing on the surfaces of sample particles is removed. The test fluid imbibed into the interior of the particulate sample is then measured. The test fluid can be, for example, water, a non-aqueous fluid, and/or a solution of miscible solvents. The technique used to measure the imbibed fluid depends on the solvent (imbibing fluid) being studied. In one example, this technique includes both gravimetric determination and quantitative chemical analysis. The detection of water can be via Karl Fischer titration.
    • 描述了确定诸如来自岩心样本的岩石样本的可润湿性的方法。 样品优选被粉碎或粉碎成其中已经消除微裂缝的微粒尺寸,但是其中微粒仍然足够大以代表天然岩石基质和质地。 将粉碎的核心样品暴露于测试流体一段给定的时间。 岩石样品可以分成许多独立的等分部分,并且对于不同的暴露时间使用一系列不同的流体和/或相同的流体进行一系列测试。 存在于样品颗粒表面的多余的测试流体被去除。 然后测量吸入颗粒样品内部的测试流体。 测试流体可以是例如水,非水流体和/或可混溶溶剂的溶液。 用于测量吸入液体的技术取决于正在研究的溶剂(吸液)。 在一个例子中,该技术包括重量测定和定量化学分析。 水的检测可以通过卡尔费休滴定法进行。