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1. 发明申请

WO1997028569A1 ELECTROCHEMICAL CELL OR BATTERY WITH A NEGATIVE ELECTRODE COMPRISING VANADIUM OXIDE, V6O13, OR LITHIATED VANADIUM OXIDE, LiyV6O13, AS AN ACTIVE MATERIAL 审中-公开
标题翻译：具有包含氧化钒，V 6 O 13或立方氧化钒，LiyV6O13作为活性材料的负电极的电化学电池或电池
公开(公告)号：WO1997028569A1
公开(公告)日：1997-08-07
申请号：PCT/US1997000159
申请日：1997-01-09
申请人： VALENCE TECHNOLOGY, INC. , SAIDI, Mohamed-Yazid , BARKER, Jeremy
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M04/48
CPC分类号： H01M4/485 , H01M4/505 , H01M10/0525 , H01M2004/027 , H01M2300/0025
摘要： The present invention provides an electrochemical cell or battery, which has a nonmetal negative electrode (anode). That is, no solid metal active material is used in the cell. Rather than the conventional solid lithium metal anode, the active material of the new anode comprises a compound of vanadium oxide. Accordingly, the lithium cell of the invention comprises a positive electrode and a negative electrode, where the negative electrode comprises a compound of vanadium oxide which in a fully discharged state is represented by the nominal general formula V6O13 or LiyV6O13, y equal to 0; and, in a fully or partially lithiated, fully or partially charged state, is represented by the nominal general formula LiyV6O13, where y is greater than 0 and less than or equal to 8. The unique negative electrode of the invention demonstrates exceptional performance without the disadvantages of metallic lithium negative electrodes.
摘要翻译：本发明提供一种具有非金属负极（阳极）的电化学电池或电池。也就是说，在电池中不使用固体金属活性材料。而不是传统的固体锂金属阳极，新阳极的活性材料包括氧化钒的化合物。因此，本发明的锂电池包括正极和负极，其中负极包括氧化钒的化合物，其在完全放电状态下由标称通式V6O13或LiyV6O13表示，y等于0; 并且在完全或部分锂化的完全或部分充电状态下，由标称通式Li y V 6 O 13表示，其中y大于0且小于或等于8.本发明的独特负极表现出卓越的性能，金属锂负极的缺点。

2. 发明申请

WO1998012761A1 LITHIUM-CONTAINING, LITHIUM-INTERCALATING PHOSPHATES AND THEIR USE AS THE POSITIVE OR NEGATIVE ELECTRODE MATERIAL IN A LITHIUM SECONDARY BATTERY 审中-公开
标题翻译：含锂的锂离子磷酸盐及其作为锂二次电池中的正极或负极电极材料的用途
公开(公告)号：WO1998012761A1
公开(公告)日：1998-03-26
申请号：PCT/US1997015544
申请日：1997-09-04
申请人： VALENCE TECHNOLOGY, INC. , BARKER, Jeremy , SAIDI, Mohamed-Yazid
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M04/58
CPC分类号： H01M10/052 , C01B25/45 , H01M4/04 , H01M4/0404 , H01M4/0409 , H01M4/0416 , H01M4/13 , H01M4/5825 , H01M4/583 , H01M4/622 , H01M4/625 , H01M10/0525 , H01M2004/021 , H01M2004/028
摘要： The invention provides an electrochemical cell which comprises a first electrode and a second electrode which is a counter electrode to said first electrode. The first electrode comprises a phosphorous compound of the nominal general formula Li3E'aE''b(PO4)3, desirably at least one E is a metal; and preferably, Li3M'M''(PO4)3. E' and E'' are the same or different from one another. Where E' and E'' are the same, they are preferably metals having more than one oxidation state. Where E' and E'' are different from one another, they are preferably selected from the group of metals where at least one of E' and E'' has more than one oxidation state. More specifically, there is disclosed a rechargeable lithium battery comprising an electrode, preferably the positive electrode, formed from a lithium intercalating metal phosphate of the type M'M''(PO4)3 where M', M'' are metals selected from Ti, Fe, V, Al, Mo, and Cr.
摘要翻译：本发明提供了一种电化学电池，其包括第一电极和作为与所述第一电极相对的电极的第二电极。第一电极包含标称通式为Li 3 E''E'b（PO 4）3的磷化合物，理想的是至少一个E是金属; 优选Li 3 M'M“（PO 4）3。 E'和E“彼此相同或不同。当E'和E“相同时，它们优选为具有多于一种氧化态的金属。其中E'和E“彼此不同，它们优选选自E'和E”中的至少一个具有多于一个氧化态的金属组。更具体地，公开了一种可再充电锂电池，其包括由M'M“（PO4）3型的嵌入金属磷酸盐形成的电极，优选正电极，其中M'，M”是选自Ti ，Fe，V，Al，Mo和Cr。

3. 发明申请

WO1998026469A1 STABILIZED ELECTROCHEMICAL CELL 审中-公开
标题翻译：稳定化学电池
公开(公告)号：WO1998026469A1
公开(公告)日：1998-06-18
申请号：PCT/US1997022525
申请日：1997-11-21
申请人： VALENCE TECHNOLOGY, INC. , SAIDI, Mohamed-Yazid , SCORDILIS-KELLEY, Chariclea , BARKER, Jeremy
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M10/40
CPC分类号： H01M4/505 , C01G45/1221 , C01G45/1242 , C01P2006/40 , H01M4/62 , H01M10/0525 , H01M10/0567
摘要： The present invention provides a novel composition and method for preventing decomposition of one or more electrochemical cell components comprising an electrode having an active material, and an electrolyte. The method of the invention effectively blocks decomposition of a lithium metal oxide cathode active material, and particularly lithium manganese oxide (LMO, nominally LiMn O). Such decomposition is prevented by including in the cell a basic compound which forms an electron donor species in the electrolyte solution; and by neutralizing at least a portion of the acid by reacting the donor species with the hydrogen-containing acids thereby preventing decomposition of the lithium manganese oxide by the acid. The preservation of the lithium manganese oxide prevents degradation of other cell components by other mechanism.
摘要翻译：本发明提供一种用于防止一种或多种电化学电池元件分解的新型组合物和方法，所述电化学电池组件包括具有活性材料的电极和电解质。本发明的方法有效地阻止锂金属氧化物正极活性物质，特别是锰酸锂（LMO，名义上为LiMn O）的分解。通过在电解液中包含在电解质溶液中形成电子供体物质的碱性化合物来防止这种分解; 并且通过使供体物质与含氢酸反应从而中和酸的至少一部分，从而防止酸分解锰酸锂。锂锰氧化物的保存通过其他机理防止其他电池组分的降解。

4. 发明申请

WO1998026467A1 ADDITIVE TO STABILIZE ELECTROCHEMICAL CELL 审中-公开
标题翻译：添加到稳定电化学细胞
公开(公告)号：WO1998026467A1
公开(公告)日：1998-06-18
申请号：PCT/US1997021292
申请日：1997-11-21
申请人： VALENCE TECHNOLOGY, INC. , SAIDI, Mohamed-Yazid , GAO, Feng , BARKER, Jeremy , SCORDILIS-KELLEY, Chariclea
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M10/40
CPC分类号： H01M10/0567 , H01M4/131 , H01M4/133 , H01M4/505 , H01M4/62 , H01M10/0525 , Y10T29/49108
摘要： The present invention provides a novel composition and method for preventing decomposition of one or more electrochemical cell components comprising an electrode having an active material, and an electrolyte. The method of the invention effectively blocks decomposition of a lithium metal oxide cathode active material, and particularly lithium manganese oxide (LMO, nominally LiMn2O4). Such decomposition is prevented by including in the cell a basic compound which forms an electron donor species in the electrolyte solution; and by neutralizing at least a portion of the acid by reacting the donor species with the hydrogen containing acids whereby preventing decomposition of the lithium manganese oxide by the acid. The preservation of the lithium manganese oxide prevents degradation of other cell components by other mechanism. The basic compound is desirably an organic base, preferably a butylamine.
摘要翻译：本发明提供一种用于防止一种或多种电化学电池元件分解的新型组合物和方法，所述电化学电池组件包括具有活性材料的电极和电解质。本发明的方法有效地阻止锂金属氧化物正极活性物质，特别是锰酸锂（LMO，名义上是LiMn 2 O 4）的分解。通过在电解液中包含在电解质溶液中形成电子供体物质的碱性化合物来防止这种分解; 并且通过使供体物质与含氢的酸反应来中和至少一部分酸，从而防止酸分解锰酸锂。锂锰氧化物的保存通过其他机理防止其他电池组分的降解。碱性化合物优选为有机碱，优选为丁胺。

5. 发明申请

WO1997048140A1 LITHIUM CELL HAVING MIXED LITHIUM-METAL-CHALCOGENIDE CATHODE 审中-公开
标题翻译：具有混合的锂金属 - 氯化铝阴极的锂电池
公开(公告)号：WO1997048140A1
公开(公告)日：1997-12-18
申请号：PCT/US1997009653
申请日：1997-06-03
申请人： VALENCE TECHNOLOGY, INC. , BARKER, Jeremy , SAIDI, Mohamed-Yazid
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M04/48
CPC分类号： H01M4/485 , C01P2004/80 , C01P2004/82 , C01P2006/40 , H01M4/131 , H01M4/133 , H01M4/1393 , H01M4/364 , H01M4/505 , H01M4/581 , H01M10/0525
摘要： The invention provides a new positive electrode active material having increased capacity and a method for operating an electrochemical lithium cell or battery which has the new positive electrode active material composition. The positive electrode comprises first and second lithium-containing active materials which are different from one another. The invention provides the ability to overcome first cycle inefficiency typically observed when using a single lithium-containing metal chalcogenide by adding a small amount of a second lithium-containing metal chalcogenide, preferably lithium copper oxide.
摘要翻译：本发明提供了一种具有增加容量的新型正极活性材料和一种具有新型正极活性材料组合物的电化学锂电池或电池的操作方法。正极包含彼此不同的第一和第二含锂活性物质。本发明提供克服通过添加少量第二含锂金属硫族化物，优选氧化铜锂在使用单一含锂金属硫族化物时通常观察到的第一循环无效率的能力。

6. 发明申请

WO1997050136A1 LITHIUM MANGANESE OXIDE CATHODES WITH HIGH CAPACITY AND STABILITY 审中-公开
标题翻译：具有高容量和稳定性的锰锰氧化物阴极
公开(公告)号：WO1997050136A1
公开(公告)日：1997-12-31
申请号：PCT/US1997009757
申请日：1997-06-10
申请人： VALENCE TECHNOLOGY, INC. , SAIDI, Mohamed-Yazid , KOKSBANG, Rene
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M04/50
CPC分类号： H01M4/505 , H01M4/131 , H01M4/1393 , H01M4/485 , H01M10/0525
摘要： A method for reducing capacity fading of an LiMn2O4 spinel electrode active material comprising substituting a minor amount of Z for Mn in the LiMn2O4 active material, where Z is a metal element having a +4 (IV) valence state and is characterized by an ability to form tetravalent chlorides. The Z substituted LiMn2O4 active material is further characterized by a lesser rate of capacity loss with cycling as compared to LiMn2O4 active material.
摘要翻译：一种用于减少LiMn 2 O 4尖晶石电极活性材料的容量衰减的方法，包括在LiMn2O4活性材料中代替少量的Z代表Mn，其中Z是具有+4（IV）价态的金属元素，其特征在于具有形成四价氯化物。 Z取代的LiMn2O4活性材料的特征还在于与LiMn2O4活性材料相比，循环时容量损失率较小。

7. 发明申请

WO1998026468A1 POLYMER ELECTROLYTES CONTAINING LITHIATED ZEOLITE 审中-公开
标题翻译：含有LITHIATED ZEOLITE的聚合物电解质
公开(公告)号：WO1998026468A1
公开(公告)日：1998-06-18
申请号：PCT/US1997021637
申请日：1997-12-08
申请人： VALENCE TECHNOLOGY, INC. , GAO, Feng , MITCHELL, Porter, H. , BARKER, Jeremy , SWOYER, Jeffrey
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M10/40
CPC分类号： H01M10/0563 , H01M4/62 , H01M6/168 , H01M10/052 , H01M10/0525 , H01M10/0565
摘要： A method of improving the structural integrity of polymer electrolytes of electrochemical cell by employing lithiated zeolites, and optionally, inorganic fillers selected from SiO2, Al2O3, TiO2 and ZrO is provided.
摘要翻译：提供了通过使用锂化沸石和任选的选自SiO 2，Al 2 O 3，TiO 2和ZrO的无机填料来改善电化学电池的聚合物电解质的结构完整性的方法。

8. 发明申请

WO1998020574A1 PROPYLENE CARBONATE BASED ELECTROLYTE FOR LITHIUM ION ELECTROCHEMICAL CELL 审中-公开
标题翻译：用于锂离子电化学电池的丙烯碳酸锂电解质
公开(公告)号：WO1998020574A1
公开(公告)日：1998-05-14
申请号：PCT/US1997019311
申请日：1997-11-03
申请人： VALENCE TECHNOLOGY, INC. , BARKER, Jeremy , GAO, Feng
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M10/40
CPC分类号： H01M10/0569 , H01M4/587 , H01M10/052 , H01M10/0565 , Y10T29/49108
摘要： Non-aqueous solid electrochemical cells with improved performance can be fabricated by employing intercalation based carbon anodes comprising graphite, coke, or mixtures thereof, and an electrolyte having an electrolyte solvent formed of propylene carbonate and 4,5 dichloroethylene carbonate. The cells are particularly suited for low temperature applications.
摘要翻译：具有改进性能的非水固体电化学电池可以通过使用包含石墨，焦炭或其混合物的基于嵌入的碳阳极和具有由碳酸丙烯酯和4,5二氯乙烯碳酸酯形成的电解质溶剂的电解质来制造。这些电池特别适用于低温应用。

9. 发明申请

WO1997038459A1 CARBONACEOUS ELECTRODE AND COMPATIBLE ELECTROLYTE AND BATTERY 审中-公开
标题翻译：碳酸电池和电容器和电池
公开(公告)号：WO1997038459A1
公开(公告)日：1997-10-16
申请号：PCT/US1997003636
申请日：1997-03-04
申请人： VALENCE TECHNOLOGY, INC. , BARKER, Jeremy , GAO, Feng
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M04/58
CPC分类号： H01M4/587 , H01M2/1613 , H01M2/1653 , H01M4/131 , H01M4/133 , H01M4/485 , H01M4/505 , H01M4/623 , H01M4/661 , H01M4/663 , H01M4/667 , H01M10/05 , H01M10/0525 , H01M10/0566 , H01M10/0569 , H01M2300/0025 , H01M2300/004 , H01M2300/0082 , H01M2300/0085
摘要： The inventions provides a battery which comprises a first electrode, a counter electrode which forms an electrochemical couple with said first electrode, and an electrolyte. The first electrode comprises graphite particles having an interlayer distance spacing of 002 planes (d002) as determined by x-ray diffraction of 0.330 to 0.340 nanometers (nm), a crystallite size in the direction of c-axis (Lc) being greater than about 90 nanometers (nm) and less than about 1000 nanometers, and at least 90 percent by weight of said graphite particles having a size less than about 24 microns ( mu m). The electrolyte comprises a solvent mixture and a solute; the solvent mixture comprises (i) ethylene carbonate (EC), and (ii) a solvent selected from the group consisting of propylene carbonate (PC), butylene carbonate (BC), and mixtures thereof with the ethylene carbonate being present in an amount by weight which is at least as great as the amount of any other solvent. Optionally, the solvent mixture further comprises one or more other organic solvents selected from the group consisting of methyl ethyl carbonate (MEC), diethyl carbonate (DEC), dipropyl carbonate (DPC), dimethyl carbonate (DMC), and mixtures thereof.
摘要翻译：本发明提供一种电池，其包括第一电极，与所述第一电极形成电化学耦合的对电极和电解质。第一电极包括通过x射线衍射测定为0.330至0.340纳米（nm）的层间距离间隔为002平面（d002）的石墨颗粒，c轴方向上的微晶尺寸（Lc）大于约 90纳米（nm）且小于约1000纳米，并且至少90重量％的所述石墨颗粒具有小于约24微米（μm）的尺寸。电解质包含溶剂混合物和溶质; 溶剂混合物包含（i）碳酸亚乙酯（EC）和（ii）选自碳酸亚丙酯（PC），碳酸亚丁酯（BC）及其与碳酸亚乙酯的混合物的溶剂的量以其重量至少等于任何其它溶剂的量。任选地，溶剂混合物还包含一种或多种选自碳酸甲乙酯（MEC），碳酸二乙酯（DEC），碳酸二丙酯（DPC），碳酸二甲酯（DMC））及其混合物的其它有机溶剂。

10. 发明申请

WO1997034330A1 CARBON ANODE FOR LITHIUM ION ELECTROCHEMICAL CELL 审中-公开
标题翻译：用于锂离子电化学细胞的碳阳极
公开(公告)号：WO1997034330A1
公开(公告)日：1997-09-18
申请号：PCT/US1997003267
申请日：1997-03-04
申请人： VALENCE TECHNOLOGY, INC. , SHI, Hang , BARKER, Jeremy , KOKSBANG, Rene
发明人： VALENCE TECHNOLOGY, INC.
IPC分类号： H01M04/58
CPC分类号： H01M10/0525 , C01B32/22 , H01M4/1393 , H01M4/587 , H01M2004/021 , Y10T29/49108
摘要： Increasing the percentage of the 3R phase present in graphite reduces the first capacity loss of anodes employing the so-modified graphite. Conversion of 2H phase graphite to 3R phase graphite can be achieved by grinding graphite. Non-aqueous solid electrochemical cells with improved performance can be fabricated by employing intercalation based carbon anodes comprising graphite with high percentage of 3R. When employed in an electrochemical cell, the first cycle capacity loss is of only about 10 %.
摘要翻译：增加存在于石墨中的3R相的百分比减少了使用如此改性的石墨的阳极的第一容量损失。 2H相石墨转化为3R相石墨可以通过研磨石墨来实现。具有改进性能的非水固体电化学电池可以通过采用含有高比例的3R的石墨的基于嵌层的碳阳极来制造。当用于电化学电池时，第一循环容量损失仅为约10％。

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