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1. 发明申请

US20100257873A1 METHOD FOR CONTROLLING THE WITHDRAWAL OF GAS 审中-公开
标题翻译：控制气体排放的方法
公开(公告)号：US20100257873A1
公开(公告)日：2010-10-14
申请号：US12746705
申请日：2008-11-17
申请人： Ulrich Mueller , Frank Poplow , Markus Schubert , Jan-Michael Graehn , Werner Gruenwald , Ian Faye
发明人： Ulrich Mueller , Frank Poplow , Markus Schubert , Jan-Michael Graehn , Werner Gruenwald , Ian Faye
IPC分类号： F17C11/00 , B65B3/00
CPC分类号： F17C11/005
摘要： The invention relates to a method for controlling the withdrawal of gas from a sorption reservoir. The temperature in the sorption reservoir having a decreasing amount of gas therein is increased until a maximum acceptable temperature is reached such that a predetermined minimum pressure in the sorption reservoir does not fall below that threshold. The invention also relates to a device for storing at least one gas, having a sorption reservoir that has at least one attachment via which the sorption reservoir can be filled with gas or via which gas can be withdrawn from the sorption reservoir. The invention also relates to a device having at least one heating element which can warm the sorption reservoir, also a control system that can increase the temperature in the sorption reservoir when withdrawing the gas in such a manner that a predetermined minimum temperature in the sorption reservoir is not fallen below in order to attain a maximum acceptable pressure.
摘要翻译：本发明涉及一种用于控制从吸附容器中排出气体的方法。吸附容器内的气体的温度降低，直至达到最大可接受的温度，使得吸附容器中的预定的最小压力不低于该阈值。本发明还涉及一种用于存储至少一种气体的装置，其具有吸附储存器，所述吸附储存器具有至少一个附件，吸附容器可通过该附件填充气体，或者可以通过该气体从吸附容器中排出气体。本发明还涉及一种具有至少一个加热元件的装置，该加热元件可以使吸附储存器温暖，也是一种控制系统，该控制系统可以在抽吸气体时增加吸附储存器中的温度，使得吸附储存器中的预定最小温度不能下降以达到最大可接受的压力。

2. 发明授权

US08658849B2 Process for the separation of unbranched hydrocarbons from their branched isomers 失效
标题翻译：从支链异构体中分离未分支烃的方法
公开(公告)号：US08658849B2
公开(公告)日：2014-02-25
申请号：US12668436
申请日：2008-06-30
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
IPC分类号： C07C7/13
CPC分类号： C07C7/12 , B01J20/22 , B01J20/226 , B01J2220/56 , C07C7/135 , C10G25/003 , C07C9/00
摘要： The present invention relates to a process for the separation of at least one unbranched C4-C2O hydrocarbon from a fluid mixture containing the unbranched hydrocarbon and at least one branched isomer of the unbranched hydrocarbon, which comprises the step of—contacting the fluid mixture with an adsorbent comprising a porous metal organic framework material, which material comprises at least one at least bidentate organic compound coordinately bound to at least one metal ion, to get the unbranched hydrocarbon adsorbed, wherein the at least one at least bidentate organic compound is a monocyclic, bicyclic or polycyclic ring system which is derived from at least one heterocycle selected from the group consisting of pyrrole, alpha-pyridone and gamma-pyridone and has at least two ring nitrogens and is unsubstituted or bears one or more substituents selected independently from the group consisting of halogen, Ci-6-alkyl, phenyl, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl, where the substituents Ci_6-alkyl and phenyl are unsubstituted or bear one or more substituents selected independently from the group consisting of halogen, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl. The present invention also relates to the use of said porous metal-organic framework material in a process for the separation of unbranched hydrocarbons from their branched isomers.
摘要翻译：本发明涉及从含有非支链烃和非支链烃的至少一种支链异构体的流体混合物中分离至少一种未分支的C 4 -C 20烃的方法，其包括使流体混合物与吸附剂，其包含多孔金属有机骨架材料，该材料包含与至少一种金属离子配位结合的至少一种至少二齿有机化合物，以获得非支化烃被吸附，其中至少一种至少二齿有机化合物是单环，衍生自选自吡咯，α-吡啶酮和γ-吡啶酮的至少一种杂环的双环或多环系统，并且具有至少两个环氮并且是未取代的或带有一个或多个独立地选自以下的取代基：的卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，苯基和OC 1-6 - 烷基，其中取代基C 1-6 - 烷基和苯基是未取代的或具有一个或多个独立地选自卤素，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，和OC 1-6烷基。本发明还涉及所述多孔金属 - 有机骨架材料在从其支化异构体中分离未分支烃的方法中的用途。

3. 发明申请

US20100197990A1 PROCESS FOR THE SEPARATION OF UNBRANCHED HYDROCARBONS FROM THEIR BRANCHED ISOMERS 失效
标题翻译：从分散式异构体中分离出未结合的烃类的方法
公开(公告)号：US20100197990A1
公开(公告)日：2010-08-05
申请号：US12668436
申请日：2008-06-30
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener , Ingo Richter , William Dolan , Frank Poplow
IPC分类号： C07C7/12
CPC分类号： C07C7/12 , B01J20/22 , B01J20/226 , B01J2220/56 , C07C7/135 , C10G25/003 , C07C9/00
摘要： The present invention relates to a process for the separation of at least one unbranched C4-C2O hydrocarbon from a fluid mixture containing the unbranched hydrocarbon and at least one branched isomer of the unbranched hydrocarbon, which comprises the step of—contacting the fluid mixture with an adsorbent comprising a porous metal organic framework material, which material comprises at least one at least bidentate organic compound coordinately bound to at least one metal ion, to get the unbranched hydrocarbon adsorbed, wherein the at least one at least bidentate organic compound is a monocyclic, bicyclic or polycyclic ring system which is derived from at least one heterocycle selected from the group consisting of pyrrole, alpha-pyridone and gamma-pyridone and has at least two ring nitrogens and is unsubstituted or bears one or more substituents selected independently from the group consisting of halogen, Ci-6-alkyl, phenyl, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl, where the substituents Ci_6-alkyl and phenyl are unsubstituted or bear one or more substituents selected independently from the group consisting of halogen, NH2, NH(d-6-alkyl), N(C1-6-alkyl)2, OH, Ophenyl and OCi-6-alkyl. The present invention also relates to the use of said porous metal-organic framework material in a process for the separation of unbranched hydrocarbons from their branched isomers.
摘要翻译：本发明涉及从含有非支链烃和非支链烃的至少一种支链异构体的流体混合物中分离至少一种未分支的C 4 -C 20烃的方法，其包括使流体混合物与吸附剂，其包含多孔金属有机骨架材料，该材料包含与至少一种金属离子配位结合的至少一种至少二齿有机化合物，以获得非支化烃被吸附，其中至少一种至少二齿有机化合物是单环，衍生自选自吡咯，α-吡啶酮和γ-吡啶酮的至少一种杂环的双环或多环系统，并且具有至少两个环氮并且是未取代的或带有一个或多个独立地选自以下的取代基：的卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，Ophenyl和OCi-6-alk 其中取代基C 1-6 - 烷基和苯基是未取代的或具有一个或多个独立地选自卤素，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，苯基和OC 1-6烷基。本发明还涉及所述多孔金属 - 有机骨架材料在从其支化异构体中分离未分支烃的方法中的用途。

4. 发明授权

US08530717B2 Process for the industrial isolation of propene 失效
标题翻译：丙烯工业隔离工艺
公开(公告)号：US08530717B2
公开(公告)日：2013-09-10
申请号：US13003839
申请日：2009-07-17
申请人： Markus Schubert , Ingo Richter , Ulrich Mueller , Frank Poplow , William Dolan , Christoph Kiener
发明人： Markus Schubert , Ingo Richter , Ulrich Mueller , Frank Poplow , William Dolan , Christoph Kiener
IPC分类号： C07C7/12
CPC分类号： C07C7/12 , C07C11/06
摘要： A process for the industrial isolation of propene from a gas stream comprising at least propene and propane, which involves contacting of the gas stream with an adsorbent having a porous metal organic framework having at least one at least bidentate organic compound coordinated to at least one metal ion, with the adsorbent becoming laden with propane and the gas stream therefore having an increased proportion of propene, wherein the W least bidentate organic compound is an imidazolate which is unsubstituted or has one or more substituents selected independently from of halogen, C1-6-alkyl, phenyl, NH2, NH(C1-6-alkyl), N(C1-6-alkyl)2, OH, O-phenyl and O—C1-6-alkyl.
摘要翻译：一种用于从包含至少丙烯和丙烷的气流中工业分离丙烯的方法，其包括使气流与具有多孔金属有机骨架的吸附剂接触，所述多孔金属有机骨架具有与至少一种金属配位的至少二齿有机化合物离子，吸附剂变得装满丙烷，因此气流具有增加的丙烯比例，其中W最小二齿有机化合物是未被取代的或具有一个或多个独立地选自卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，O-苯基和O-C 1-6 - 烷基。

5. 发明申请

US20110118526A1 PROCESS FOR INDUSTRIAL ISOLATION OF PROPENE 失效
标题翻译：工业分离丙烯的方法
公开(公告)号：US20110118526A1
公开(公告)日：2011-05-19
申请号：US13003839
申请日：2009-07-17
申请人： Markus Schubert , Ingo Richter , Ulrich Mueller , Frank Poplow , William Dolan , Christoph Kiener
发明人： Markus Schubert , Ingo Richter , Ulrich Mueller , Frank Poplow , William Dolan , Christoph Kiener
IPC分类号： C07C7/12
CPC分类号： C07C7/12 , C07C11/06
摘要： A process for the industrial isolation of propene from a gas stream comprising at least propene and propane, which involves contacting of the gas stream with an adsorbent having a porous metal organic framework having at least one at least bidentate organic compound coordinated to at least one metal ion, with the adsorbent becoming laden with propane and the gas stream therefore having an increased proportion of propene, wherein the W least bidentate organic compound is an imidazolate which is unsubstituted or has one or more substituents selected independently from of halogen, C1-6-alkyl, phenyl, NH2, NH(C1-6-alkyl), N(C1-6-alkyl)2, OH, O-phenyl and O—C1-6-alkyl.
摘要翻译：一种用于从包含至少丙烯和丙烷的气流中工业分离丙烯的方法，其包括使气流与具有多孔金属有机骨架的吸附剂接触，所述多孔金属有机骨架具有与至少一种金属配位的至少二齿有机化合物离子，吸附剂变得装满丙烷，因此气流具有增加的丙烯比例，其中W最小二齿有机化合物是未被取代的或具有一个或多个独立地选自卤素，C 1-6 - 烷基，苯基，NH 2，NH（C 1-6 - 烷基），N（C 1-6 - 烷基）2，OH，O-苯基和O-C 1-6 - 烷基。

6. 发明授权

US07968739B2 Method for electrochemical production of a crystalline porous metal organic skeleton material 有权
标题翻译：电化学生产结晶多孔金属有机骨架材料的方法
公开(公告)号：US07968739B2
公开(公告)日：2011-06-28
申请号：US10580407
申请日：2004-11-22
申请人： Ulrich Mueller , Hermann Puetter , Michael Hesse , Markus Schubert , Helge Wessel , Juergen Huff , Marcus Guzmann
发明人： Ulrich Mueller , Hermann Puetter , Michael Hesse , Markus Schubert , Helge Wessel , Juergen Huff , Marcus Guzmann
IPC分类号： C07F3/00 , C07F15/00
CPC分类号： C25B3/12 , B01D53/02 , B01D2253/204 , B01J20/226 , B01J20/28014 , B01J20/28042 , B01J31/1691 , B01J31/1805 , B01J31/1815 , B01J31/2239 , B01J31/226 , B01J2531/16 , B01J2531/26 , B01J2531/842 , C01B3/0015 , C01B21/0455 , C01B23/0057 , F17C11/005 , H01M8/04216 , Y02C10/08 , Y02E60/327 , Y02E60/328 , Y02P20/133 , Y02P70/56 , Y10S95/90 , Y10S502/526
摘要： A method of electrochemically preparing a crystalline, porous, metal-organic framework material comprising at least one at least bidentate organic compound coordinately bound to at least one metal ion, in a reaction medium comprising the at least one bidentate organic compound, wherein at least one metal ion is provided in the reaction medium by the oxidation of one anode comprising the corresponding metal.
摘要翻译：一种在包含至少一种二齿有机化合物的反应介质中电化学制备结晶多孔的金属 - 有机骨架材料的方法，其包含与至少一种金属离子配位结合的至少二齿有机化合物，其中至少一种金属离子通过包含相应金属的一个阳极的氧化在反应介质中提供。

7. 发明申请

US20110011805A1 POROUS METAL ORGANIC FRAMEWORKS AS DESICCANTS 审中-公开
标题翻译：多孔金属有机框架作为干燥剂
公开(公告)号：US20110011805A1
公开(公告)日：2011-01-20
申请号：US12863339
申请日：2009-01-23
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener
IPC分类号： B01D15/08
CPC分类号： B01J20/226 , B01D2253/204 , B01D2257/80 , B01J20/0233 , B01J2220/50
摘要： The present invention relates to the use of a porous metal organic framework comprising at least one at least bidentate organic compound coordinate to at least one metal ion as desiccant for reducing the water content of an organic liquid or for removing water from an organic liquid.
摘要翻译：本发明涉及多孔金属有机骨架的用途，所述多孔金属有机骨架包含至少一种至少二齿有机化合物与至少一种金属离子的配位作为干燥剂，用于降低有机液体的含水量或从有机液体中除去水分。

8. 发明授权

US07847115B2 Process for preparing porous organic framework materials 有权
标题翻译：制备多孔有机骨架材料的方法
公开(公告)号：US07847115B2
公开(公告)日：2010-12-07
申请号：US12161024
申请日：2007-02-08
申请人： Markus Schubert , Ulrich Mueller , Hendrick Mattenheimer
发明人： Markus Schubert , Ulrich Mueller , Hendrick Mattenheimer
IPC分类号： C07F3/00 , C07F15/00 , C07F5/02
CPC分类号： C07F3/003 , C07F19/005
摘要： The present invention relates to a process for preparing porous organic frameworks by reaction of a reaction mixture in a liquid phase comprising the appropriate starting compounds in the presence of a nonaqueous organic solvent in the presence of and/or with liberation of water, wherein the latter is withdrawn from the liquid phase of the reaction mixture during the reaction. Here, frameworks having relatively high specific surface areas can be obtained in a reproducible way.
摘要翻译：本发明涉及一种制备多孔有机骨架的方法，该方法通过在非水有机溶剂存在下和/或与水的释放下在包含合适的起始化合物的液相中反应混合物进行反应，其中后者在反应期间从反应混合物的液相中排出。这里，可以以可再现的方式获得比表面积相对较高的框架。

9. 发明申请

US20100154635A1 ALUMINIUM AMINOCAROBXYLATES AS POROUS METAL ORGANIC FRAMEWORKS 失效
标题翻译：作为多孔金属有机骨架的氨基铝酸铵
公开(公告)号：US20100154635A1
公开(公告)日：2010-06-24
申请号：US12601022
申请日：2008-05-20
申请人： Markus Schubert , Ulrich Mueller , Christoph Kiener
发明人： Markus Schubert , Ulrich Mueller , Christoph Kiener
IPC分类号： B01D53/02 , C07F5/06
CPC分类号： B01D53/02 , B01D2253/204 , B01D2253/306 , B01D2257/108 , B01D2257/504 , B01D2257/702 , B01D2259/4525 , B01J20/226 , B01J20/28042 , B01J20/28066 , B01J20/30 , B01J31/1691 , B01J31/1805 , B01J31/2226 , B01J2531/31 , C07F5/069 , F17C11/00 , F17C11/005 , Y02C10/08 , Y02P20/152
摘要： The present invention relates to a porous metal organic framework comprising an at least bidentate organic compound coordinated to at least one metal ion, where the at least one metal ion is AlIII and the at least bidentate organic compound is an at least monoamino-substituted aromatic dicarboxylic acid selected from the group consisting of terephthalic acid, 2,6-naphthalenedicarboxylic acid, 1,4-naphthalenedicarboxylic acid, 1,5-naphthalenedicarboxylic acid and derivatives thereof in which at least one CH group in the ring has been replaced by nitrogen, wherein the framework in powder form has a specific surface area determined by the Langmuir method (N2, 77 K) of at least 2500 m2/g.In addition, the invention relates to shaped bodies comprising these materials, their preparation and their use for the storage and separation of gases.
摘要翻译：本发明涉及一种多孔金属有机骨架，其包含与至少一种金属离子配位的至少二齿有机化合物，其中至少一种金属离子是AlIII，并且该至少二齿有机化合物是至少一个氨基取代的芳族二羧酸选自对苯二甲酸，2,6-萘二甲酸，1,4-萘二甲酸，1,5-萘二甲酸及其衍生物的酸，其中环中的至少一个CH基团已被氮取代，其中粉末形式的框架具有由Langmuir方法（N2，77K）确定的至少2500m2 / g的比表面积。此外，本发明涉及包含这些材料的成型体，它们的制备及其用于储存和分离气体的用途。

10. 发明授权

US07553352B2 Method for the controlled storage and release of gases using an electrochemically produced crystalline, porous, organometallic skeleton material 有权
标题翻译：使用电化学生产的结晶多孔的有机金属骨架材料控制储存和释放气体的方法
公开(公告)号：US07553352B2
公开(公告)日：2009-06-30
申请号：US10580192
申请日：2004-11-24
申请人： Ulrich Mueller , Hermann Puetter , Michael Hesse , Markus Schubert , Helge Wessel , Juergen Huff , Marcus Guzmann
发明人： Ulrich Mueller , Hermann Puetter , Michael Hesse , Markus Schubert , Helge Wessel , Juergen Huff , Marcus Guzmann
IPC分类号： C01B3/00 , H01M8/04
CPC分类号： C25B3/12 , B01D53/02 , B01D2253/204 , B01J20/226 , B01J20/28014 , B01J20/28042 , B01J31/1691 , B01J31/1805 , B01J31/1815 , B01J31/2239 , B01J31/226 , B01J2531/16 , B01J2531/26 , B01J2531/842 , C01B3/0015 , C01B21/0455 , C01B23/0057 , F17C11/005 , H01M8/04216 , Y02C10/08 , Y02E60/327 , Y02E60/328 , Y02P20/133 , Y02P70/56 , Y10S95/90 , Y10S502/526
摘要： The present invention relates to a method of absorbing and/or storing gases, in which the gas to be stored is brought into contact with an electrochemically prepared metal-organic framework under conditions suitable for absorption of the gas, with absorption of the gas into the metal-organic framework occurring, and, if appropriate, the conditions are subsequently changed so that release of the stored gas occurs.
摘要翻译：本发明涉及一种吸收和/或储存气体的方法，其中待储存的气体在适于吸收气体的条件下与电化学制备的金属 - 有机骨架接触，吸收气体进入发生金属 - 有机骨架，并且如果合适的话，随后改变条件以便释放储存的气体。

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