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1. 发明授权

US4623740A N,N'- and N,N',N'-substituted silylureas and process for their production 失效
标题翻译： N，N'-和N，N'，N'-取代的甲硅烷基脲及其制备方法
公开(公告)号：US4623740A
公开(公告)日：1986-11-18
申请号：US750272
申请日：1985-07-01
申请人： Ulrich Deschler , Wolfgang Buder , Peter Kleinschmit , Rudolf Michel
发明人： Ulrich Deschler , Wolfgang Buder , Peter Kleinschmit , Rudolf Michel
IPC分类号： C07F7/18 , C07F7/10
CPC分类号： C07F7/182
摘要： The invention is directed to N,N' and N,N',N'-substituted silylureas and a process for their production in which in a single step process there are reacted a halogenoalkylsilane or a halogenbenzylsilane with a primary or secondary amine and an alkali cyanate in equimolar amounts.
摘要翻译：本发明涉及N，N'和N，N'，N'-取代的甲硅烷基脲及其制备方法，其中在单步骤中使卤代烷基硅烷或卤代苄基硅烷与伯胺或仲胺和碱反应氰酸酯等摩尔量。

2. 发明授权

US4835297A Method of preparing sulfenic acid chlorides and sulfenic acid esters 失效
标题翻译：制备磺酰氯和亚磺酸酯的方法
公开(公告)号：US4835297A
公开(公告)日：1989-05-30
申请号：US940069
申请日：1986-12-10
申请人： Ulrich Deschler , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
发明人： Ulrich Deschler , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
IPC分类号： C07F7/18
CPC分类号： C07F7/1892
摘要： The invention is directed to a method of preparing sulfenic acid chlorides and sulfenic acid esters with hydrolyzable silyl groups in which an oligosulfane containing silyl groups is chlorinated, the sulfenic acid chloride produced is separated and converted by reaction with an alkali alcoholate to the corresponding sulfenic acid ester.
摘要翻译：本发明涉及一种制备具有水解性甲硅烷基的亚磺酰氯和亚磺酸酯的方法，其中含有甲硅烷基的低级亚烷基被氯化，所产生的亚磺酰氯与碱性醇化物反应分离并转化成相应的亚磺酸酯。

3. 发明授权

US4837322A Mixtures of sulfurous triazine compounds 失效
标题翻译：亚硫酸三嗪化合物的混合物
公开(公告)号：US4837322A
公开(公告)日：1989-06-06
申请号：US89895
申请日：1987-08-27
申请人： Ulrich Deschler , Georg Hellwig , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
发明人： Ulrich Deschler , Georg Hellwig , Rudolf Michel , Peter Kleinschmit , Siegfried Wolff
IPC分类号： C07D251/52 , C08K5/34 , C08K5/378 , C08L21/00
CPC分类号： C07D251/52 , C08K5/378
摘要： Mixtures of sulfurous triazine compounds and methods of preparing these compounds with the general formula ##STR1## in which R.sup.1, R.sup.2 =H,R.sup.2 =benzyl,R.sup.2, R.sup.3, R.sup.4 =C.sub.1 -C.sub.8 -alkyl, allyl, C.sub.3 -C.sub.8 cycloalkyl, the latter unsubstituted or substituted with 1-3 methyl groups, 2-hydroxyethyl, 3-hydroxypropyl, 2-hydroxypropyl orR.sup.3 and R.sup.4 (together): C.sub.4 -C.sub.6 -alkylene, --(CH.sub.2 --CHX).sub.2 Y withX=H, CH.sub.3, Y=O,S,S.sub.a : Polysulfide chain with 2-10 S atoms (i.e. 2.ltoreq.a.ltoreq.10), in which the individual polysulfides are present in such concentrations that the statistical average value of "a" is a whole or fractional numerical value in the range from 2 to 5., characterized in that a triazine compound of the general formula ##STR2## in which R.sup.1, R.sup.2, R.sup.3, R.sup.4 have the meanings indicated above is reacted with an ammonium polysulfide or alkali polysulfide and dissolved in a protic polar solvent, especially water, at a temperature of 80.degree. to 140.degree. C.
摘要翻译：亚硫基三嗪化合物的混合物和制备这些具有通式Ⅰ的化合物的方法，其中R1，R2 = H，R2 =苄基，R2，R3，R4 = C1-C8-烷基，烯丙基，C3-C8环烷基，未取代或被1-3个甲基取代的后者，2-羟基乙基，3-羟丙基，2-羟基丙基或R 3和R 4（一起）：C 4 -C 6亚烷基， - （CH 2 -CHX）2 Y，X = CH 3，Y = O，S，Sa：具有2-10个S原子的多硫链（即2

4. 发明授权

US4697009A N-silylpropyl-N'-acyl-ureas and process for their production 失效
标题翻译： N-甲硅烷基丙基-N'-酰基脲及其生产方法
公开(公告)号：US4697009A
公开(公告)日：1987-09-29
申请号：US875867
申请日：1986-06-18
申请人： Ulrich Deschler , Peter Kleinschmit , Rudolf Michel
发明人： Ulrich Deschler , Peter Kleinschmit , Rudolf Michel
IPC分类号： C08G18/00 , C07F7/18 , C08G18/80 , C07F7/10
CPC分类号： C07F7/182
摘要： The invention is directed to N-silylpropyl-N'-acyl ureas and their production from an alkali cyanate, a 3-halopropylsilane and in a given case, a cyclic acidamide. By heating the compounds of the invention the blocked isocyanate function can be set free.
摘要翻译：本发明涉及N-甲硅烷基丙基-N'-酰基脲，它们由碱式氰酸酯，3-卤代丙基硅烷的产生，在给定情况下是环状酰胺。通过加热本发明的化合物，可以使封闭的异氰酸酯官能团自由。

5. 发明授权

US4507490A Process for the production of sulfur containing organosilicon compounds 失效
标题翻译：含硫有机硅化合物生产工艺
公开(公告)号：US4507490A
公开(公告)日：1985-03-26
申请号：US593308
申请日：1984-03-26
申请人： Peter Panster , Rudolf Michel , Peter Kleinschmit , Ulrich Deschler
发明人： Peter Panster , Rudolf Michel , Peter Kleinschmit , Ulrich Deschler
IPC分类号： C07F7/08 , C07F7/18
CPC分类号： C07F7/182 , C07F7/1892
摘要： The invention is directed to a process for the production of sulfur containing organosilicon compounds by reaction of an oligosulfide obtained in the reaction solution from a hydrogen sulfide an alkali metal and sulfur with a haloalkylsilane.
摘要翻译：本发明涉及一种生产含硫有机硅化合物的方法，该方法是将反应溶液中得到的硫化氢与碱金属和硫与卤代烷基硅烷的反应制得。

6. 发明授权

US4584395A Method for preparation of 3-chloropropyl-trichlorosilane 失效
标题翻译： 3-氯丙基三氯硅烷的制备方法
公开(公告)号：US4584395A
公开(公告)日：1986-04-22
申请号：US699696
申请日：1985-02-08
申请人： Peter Panster , Rudolf Michel , Wolfgang Buder , Peter Kleinschmit
发明人： Peter Panster , Rudolf Michel , Wolfgang Buder , Peter Kleinschmit
IPC分类号： C07F7/12 , B01J31/00 , C07B61/00 , C07F7/14 , C07F7/08
CPC分类号： C07F7/14
摘要： A method for the preparation of 3-chloropropyltrichlorosilane is carried out by conversion of trichlorosilane with allylchloride in the presence of a platinum containing polymeric organosiloxane-ammonium compound containing units represented by the structural formula: ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 represent a group of the formula:R.sup.5 --SiO.sub.3/2 (2)wherein R.sup.5 denotes an alkylene group and the free valences of the oxygen atoms are saturated by silicon atoms of further groups of the formula (2), optionally with incorporation of crosslinking agents, R.sup.4 has the same meaning as R.sup.1, R.sup.2 and R.sup.3 or hydrogen, alkyl, cycloalkyl or benzyl, Y.sup.x- represents PtX.sub.4.sup.2- or PtX.sub.6.sup.2- (X is Cl or Br) and can also be an inorganic 1 to 3 functional anion of a protonic acid which yields stable salts with amine bases or the hydroxy group, and x is a number from 1 to 3.
摘要翻译：制备3-氯丙基三氯硅烷的方法是通过在含有由下列结构式表示的含有单元的含铂聚合物有机硅氧烷 - 铵化合物存在下，将三氯硅烷与烯丙基氯反应进行的：其中R1，R2和R3 代表式为R5-SiO3 / 2（2）的基团，其中R5表示亚烷基并且氧原子的游离价被另外的式（2）的基团的硅原子饱和，任选地加入交联剂，R4与R1，R2和R3或氢，烷基，环烷基或苄基具有相同的含义，Yx-表示PtX42-或PtX62-（X是Cl或Br），也可以是质子的无机1至3官能阴离子其与胺碱或羟基产生稳定的盐，x为1至3的数。

7. 发明授权

US06506922B2 Process for the production of yellow bis(3-[triethoxysilyl]-propyl) polysulfane 有权
标题翻译：制备黄色双（3- [三乙氧基甲硅烷基] - 丙基）多硫烷的方法
公开(公告)号：US06506922B2
公开(公告)日：2003-01-14
申请号：US09948712
申请日：2001-09-10
申请人： Roland Krafczyk , Ulrich Deschler , Rudolf Michel , Christoph Batz-Sohn
发明人： Roland Krafczyk , Ulrich Deschler , Rudolf Michel , Christoph Batz-Sohn
IPC分类号： C07F708
CPC分类号： C07F7/188 , C07F7/1892
摘要： Process for the production of yellow bis(3-[triethoxysilyl]propyl)polysulfane with an average sulfur chain length of less than 4 and an iodine colour value of ≦10 mg iodine/100 ml, wherein neutral chloropropyltriethoxysilane is mixed with chloropropyltrichlorosilane and then reacted with sodium sulfide (Na2S) and sulfur, disodium tetrasulfide (Na2S4) and Na2S or disodium trisulfide (Na2S3) and Na2S in ethanol.
摘要翻译：制备平均硫链长度小于4且碘色值<= 10mg碘/ 100ml的黄色双（3- [三乙氧基甲硅烷基]丙基）多硫烷的方法，其中中性氯丙基三乙氧基硅烷与氯丙基三氯硅烷混合，然后与硫化钠（Na2S）和硫磺，二硫化二钠（Na2S4）和Na2S或二硫化钠（Na2S3）和Na2S在乙醇中反应。

8. 发明授权

US4129585A Process for the production of sulfur containing organosilicon compounds 失效
标题翻译：含硫有机硅化合物生产工艺
公开(公告)号：US4129585A
公开(公告)日：1978-12-12
申请号：US884212
申请日：1978-03-07
申请人： Wolfgang Buder , Hans-Dieter Pletka , Rudolf Michel , Rudolf Schwarz , Gerhard Dusing
发明人： Wolfgang Buder , Hans-Dieter Pletka , Rudolf Michel , Rudolf Schwarz , Gerhard Dusing
IPC分类号： C07F7/18 , C08K5/548 , C08K5/549 , C07F7/08 , C07F7/10
CPC分类号： C08K5/548 , C07F7/1892 , C08K5/549
摘要： There is provided a process for the production of sulfur containing organosilicon compounds of the formula (I) Z -- Alk -- S.sub.x -- Alk -- Z, where Z is the grouping: ##STR1## in which R.sup.1 is an alkyl group having 1 to 5 carbon atoms, a cycloalkyl group with 5 to 8 carbon atoms, the benzyl group, phenyl or phenyl substituted with at least one methyl, ethyl or chloro group, R.sup.2 is alkoxy of 1 to 4 carbon atoms, methoxyethoxy, cycloalkoxy with 5 to 8 carbon atoms, phenoxy or benzyloxy, R.sup.3 and R.sup.4 are alkyl of 1 to 3 carbon atoms or hydrogen, Alk is divalent saturated hydrocarbon group having 1 to 5 carbon atoms or such a group interrupted by --O--, --S-- or --NH-- and x is a number from 2.0 to 6.0 comprising reacting an alkali metal alcoholate, preferably in alcoholic solution with a compound of the formula (II) Z -- Alk -- Hal, where Hal is chlorine, bromine or iodine with a hydrosulfide of the formula (III) MeSH, in which Me is ammonium, an alkali metal atom or an equivalent of an alkaline earth metal or zinc and with sulfur, preferably in the presence of at least one organic solvent, separating from the halide formed, and removing the organic solvent.
摘要翻译：提供了一种制备式（I）Z-Alk-Sx-Alk-Z的含硫有机硅化合物的方法，其中Z是分组：其中R 1是烷基具有1至5个碳原子的环烷基，具有5至8个碳原子的环烷基，苄基，苯基或被至少一个甲基，乙基或氯基取代的苯基，R 2是1至4个碳原子的烷氧基，甲氧基乙氧基， 5至8个碳原子，苯氧基或苄氧基，R3和R4是1至3个碳原子的烷基或氢，Alk是具有1至5个碳原子的二价饱和烃基或被-O - ， - S-或 - -NH-，x是2.0至6.0的数，包括使碱金属醇盐，优选在醇溶液中与式（II）化合物Z-Alk-Hal反应，其中Hal为氯，溴或碘，其中硫氢化物为 Me III，其中Me为铵，碱金属原子或碱性ea当量第二金属或锌和硫，优选在至少一种有机溶剂的存在下，与形成的卤化物分离，并除去有机溶剂。

9. 发明授权

US06423859B1 Process for the preparation of organosilylalkylpolysulfanes 有权
标题翻译：制备有机硅烷基烷基聚硫烷的方法
公开(公告)号：US06423859B1
公开(公告)日：2002-07-23
申请号：US09903858
申请日：2001-07-13
申请人： Alfred Alig , Christoph Batz-Sohn , Ulrich Deschler , Rudolf Michel , Jörg Münzenberg , Raymund Sonnenschein , Werner Will , Gerd Rainhard Zezulka , Karl-Heinz Rützel
发明人： Alfred Alig , Christoph Batz-Sohn , Ulrich Deschler , Rudolf Michel , Jörg Münzenberg , Raymund Sonnenschein , Werner Will , Gerd Rainhard Zezulka , Karl-Heinz Rützel
IPC分类号： C07R708
CPC分类号： C07F7/1892
摘要： The invention relates to a process for the preparation of organosilylalkylpolysulfanes, of the general formula I (R1R2R3SiR4)2Sx (I) by reaction of organosilylalkylpolysulfanes of the general formula II (R1R2R3SiR4)2Sy (II) with an ionic sulfide of the general formula M+2S2− (III) and an organosilylalkyl halide of the general formula R1R2R3SiR4X (IV), the long-chain organosilylalkylpolysulfane of the general formula (II) and the organosilylalkyl halide of the general formula (IV) being initially introduced into the reaction vessel and the ionic sulfide of the general formula (III) being added to this solution in several portions.
摘要翻译：本发明涉及制备通式Ⅰ（R1R2R3SiR4）2Sx（Ⅰ）的有机甲硅烷基烷基聚硫烷的方法，通过使通式II（R1R2R3SiR4）2Sy（Ⅱ）的有机甲硅烷基烷基聚硫与通式M + 2SII（III）和通式为R 1 R 2 R 3 SiR 4 X（IV）的有机甲硅烷基烷基卤化物，通式（II）的长链有机甲硅烷基烷基聚
硫烷和通式（IV）的有机甲硅烷基烷基卤化物最初引入反应容器中，将通式（III）的离子性硫化物分几部分加入到该溶液中。

10. 发明授权

US06380413B2 Process for the preparation of yellow bis (3-[triethoxysilyl]propyl) tetrasulfane 有权
标题翻译：制备黄色双（3- [三乙氧基甲硅烷基]丙基）四亚砜的方法
公开(公告)号：US06380413B2
公开(公告)日：2002-04-30
申请号：US09852050
申请日：2001-05-10
申请人： Roland Krafczyk , Ulrich Deschler , Rudolf Michel
发明人： Roland Krafczyk , Ulrich Deschler , Rudolf Michel
IPC分类号： C07F708
CPC分类号： C07F7/1892
摘要： Process for the preparation of yellow bis(3-[triethoxysilyl]propyl)tetrasulfane having an iodine colour value of ≦10 mg of iodine/100 ml, in which process a small amount of chloropropyltrichlorosilane is added to neutral chloropropyltriethoxysilane and reaction with sodium polysulfide or with Na2S and sulfur in ethanol is then carried out.
摘要翻译：制备碘色值<= 10mg碘/黄的黄色双（3- [三乙氧基甲硅烷基]丙基）四亚砜的方法，其中将少量氯丙基三氯硅烷加入到中性氯丙基三乙氧基硅烷中并与多硫化钠反应或用Na 2 S和硫在乙醇中进行。

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