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1. 发明申请

WO2005035513A1 A PROCESS FOR THE PRODUCTION OF ALKYLENE OXIDE USING A GAS-PHASE PROMOTER SYSTEM 审中-公开
标题翻译：使用气相促进剂系统生产氧化亚烷的方法
公开(公告)号：WO2005035513A1
公开(公告)日：2005-04-21
申请号：PCT/US2004/025906
申请日：2004-08-09
申请人： UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY CORPORATION , ZHANG, Liping , SOO, Hwaili , SERAFIN, Juliana, G.
发明人： ZHANG, Liping , SOO, Hwaili , SERAFIN, Juliana, G.
IPC分类号： C07D301/10
CPC分类号： C07D301/10 , Y02P20/582
摘要： An improved process for the manufacture of ethylene oxide through the epoxidation of ethylene using a catalyst comprising silver and at least one efficiency-enhancing salt of a member of a redox-half reaction pair. Added to the epoxidation reaction is a two-component gas-phase promoter system comprising a chlorine-containing component (for example ethyl chloride, methyl chloride, vinyl chloride and ethylene dichloride), and a nitrogen-containing component of nitric oxide and other compounds capable of generating under reaction conditions at least one gaseous efficiency-enhancing member of a redox-half reaction pair comprising NO, NO 2 , N 2 O 3 or N 2 O 4 . The amount of each component of said gaseous promoter is adjusted to maintain the ration of N* to Z* less than or equal to 1 wherein, N* is the nitric oxide equivalent in ppmv, ranging from 1 to 20 ppmv and Z* =ethyl chloride equivalent (ppmv) * 100 percent / ethane equivalent (mol percent) * 100 ranging from 5 to 40 ppmv.
摘要翻译：通过使用包含银和至少一种氧化还原半反应对成员的效率增强盐的催化剂通过乙烯环氧化制备环氧乙烷的改进方法。添加到环氧化反应中是包含含氯组分（例如氯乙烷，甲基氯，氯乙烯和二氯乙烷）的二组分气相促进剂体系，以及一氧化氮和其它化合物的含氮组分在反应条件下产生包含NO，NO 2，N 2 O 3或N 2 O 4的氧化还原半反应对的至少一种气体效率增强成分。调节所述气体促进剂的每种组分的量以保持N *至Z *的比例小于或等于1，其中N *是以ppmv计的一氧化氮当量，范围为1至20ppmv，Z * =乙基氯化物当量（ppmv）* 100％/乙烷当量（摩尔％）* 100为5〜40ppmv。

2. 发明申请

WO2005039757A1 CATALYSTS HAVING ENHANCED STABILITY, EFFICIENCY AND/OR ACTIVITY FOR ALKYLENE OXIDE PRODUCTION 审中-公开
标题翻译：具有增强的稳定性，有效和/或活性的烷基氧化铝生产的催化剂
公开(公告)号：WO2005039757A1
公开(公告)日：2005-05-06
申请号：PCT/US2004/033219
申请日：2004-10-07
申请人： UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY CORPORATION , DOW GLOBAL TECHNOLOGIES INC , SERAFIN, Juliana, G. , LIU, Albert Cheng-Yu , SEYEDMONIR, Seyed, R. , SOO, Hwaili , SZYMANSKI, Thomas
发明人： SERAFIN, Juliana, G. , LIU, Albert Cheng-Yu , SEYEDMONIR, Seyed, R. , SOO, Hwaili , SZYMANSKI, Thomas
IPC分类号： B01J21/06
CPC分类号： C07D301/10 , B01J21/066 , B01J23/50 , B01J23/66 , B01J23/686 , B01J23/688 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0018 , B01J37/0201 , B01J37/0203
摘要： A catalyst for the manufacture of alkylene oxide, for example ethylene oxide, by the vapor-phase epoxidation of alkene containing impregnated silver and at least one efficiency-enhancing promoter on an inert, refractory solid support, said support incorporating a sufficient amount of zirconium component (present and remaining substantially as zirconium silicate) as to enhance at least one of catalyst activity, efficiency and stability as compared to a similar catalyst which does not contain the zirconium component.
摘要翻译：用于通过气相环氧化含烯烃的浸渍的银和至少一种在惰性耐火固体载体上的效率增强促进剂来制备环氧烷烃例如环氧乙烷的催化剂，所述载体包含足量的锆组分（存在并基本上保持为硅酸锆），与不含锆组分的类似催化剂相比，可提高催化剂活性，效率和稳定性中的至少一种。

3. 发明申请

WO2005023418A1 IMPROVED ALUMINA CARRIERS AND SILVER-BASED CATALYSTS FOR THE PRODUCTION OF ALKYLENE OXIDES 审中-公开
标题翻译：改进的氧化铝载体和用于生产烷基氧化物的银基催化剂
公开(公告)号：WO2005023418A1
公开(公告)日：2005-03-17
申请号：PCT/US2004/017103
申请日：2004-06-02
申请人： UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY CORPORATION , THORSTEINSON, Erlind, M. , BHASIN, Madan, Mohan , LIU, Albert, Cheng-Yu , SERAFIN, Juliana, G. , SEYEDMONIR, Seyed, R. , SOO, Hwaili
发明人： THORSTEINSON, Erlind, M. , BHASIN, Madan, Mohan , LIU, Albert, Cheng-Yu , SERAFIN, Juliana, G. , SEYEDMONIR, Seyed, R. , SOO, Hwaili
IPC分类号： B01J23/68
CPC分类号： B01J23/50 , B01J21/04 , B01J21/12 , B01J23/66 , B01J23/688 , B01J37/0205 , B01J37/0207 , B01J37/06
摘要： An improved carrier useful for preparing a catalyst having excellent catalytic performance when used in the production of alkylene oxide, such as ethylene oxide. The carrier is obtained by a) impregnating a preformed alpha-alumina carrier with at least one modifier selected from among alkali metal silicates and alkaline earth metal silicates, b) drying said impregnated carrier; and c) calcining said dried carrier. The carrier may optionally be washed, prior to being impregnated by conventional catalytic material and/or promoter material.
摘要翻译：一种改进的载体，可用于制备当用于生产环氧烷烃如环氧乙烷时具有优异催化性能的催化剂。载体通过以下方法获得：a）用至少一种选自碱金属硅酸盐和碱土金属硅酸盐的改性剂浸渍预制的α-氧化铝载体，b）干燥所述浸渍的载体; 和c）煅烧所述干燥的载体。在用常规催化材料和/或促进剂材料浸渍之前，载体可以任选地被洗涤。

4. 发明申请

WO2010123842A1 SIMPLIFIED METHOD FOR PRODUCING ALKYLENE OXIDES WITH A HIGH EFFICIENCY CATALYST AS IT AGES 审中-公开
标题翻译：使用高效催化剂生产烷基氧化物的简化方法
公开(公告)号：WO2010123842A1
公开(公告)日：2010-10-28
申请号：PCT/US2010/031668
申请日：2010-04-20
申请人： DOW TECHNOLOGY INVESTMENTS LLC , ZHANG, Liping , SOO, Hwaili , HENSTOCK, William
发明人： ZHANG, Liping , SOO, Hwaili , HENSTOCK, William
IPC分类号： C07D301/10
CPC分类号： C07D301/10 , Y02P20/582
摘要： A simplified method of operating an alkylene oxide production process that utilizes a high efficiency silver catalyst is shown and described. The method accounts for declining catalyst activity that occurs as the catalyst ages by making alternating changes to the reaction temperature and an overall chloriding effectiveness parameter.
摘要翻译：显示和描述了使用高效银催化剂的环氧烷生产方法的简化操作方法。该方法考虑到随着催化剂老化而发生的催化剂活性下降，通过对反应温度进行交替改变和总体氯化效力参数。

5. 发明申请

WO2012141942A1 PROCESS FOR CONDITIONING A HIGH EFFICIENCY ETHYLENE OXIDE CATALYST 审中-公开
标题翻译：用于调节高效乙烯氧化物催化剂的方法
公开(公告)号：WO2012141942A1
公开(公告)日：2012-10-18
申请号：PCT/US2012/031990
申请日：2012-04-03
申请人： DOW TECHNOLOGY INVESTMENTS LLC , ZHANG, Liping , TUPE, Ravindra, Radhakisan , PHILLIPS, Ailene, Gardner , HINMAN, Paul, Victor , SOO, Hwaili
发明人： ZHANG, Liping , TUPE, Ravindra, Radhakisan , PHILLIPS, Ailene, Gardner , HINMAN, Paul, Victor , SOO, Hwaili
IPC分类号： B01J23/50 , B01J23/68 , C07D301/10
CPC分类号： C07D301/10 , B01J23/50 , B01J23/6567 , B01J37/08 , B01J38/00 , B01J38/04 , Y02P20/52 , Y02P20/582 , Y02P20/584
摘要： A process for conditioning a high efficiency silver catalyst used to manufacture ethylene oxide from ethylene, oxygen, and at least one organic chloride is described. A non-reactive conditioning gas comprising at least one of ethylene, oxygen, and a ballast gas is introduced to the catalyst at a conditioning temperature ranging from 150°C to 180°C for a selected period of at least 4 hours.
摘要翻译：描述了一种用于调节用于从乙烯，氧气和至少一种有机氯化物制造环氧乙烷的高效率银催化剂的方法。将包含乙烯，氧气和压载气体中的至少一种的非反应性调节气体在150℃至180℃的调节温度下引入至少4小时的选定时段。

6. 发明公开

EP1675678A1 CATALYSTS HAVING ENHANCED STABILITY, EFFICIENCY AND/OR ACTIVITY FOR ALKYLENE OXIDE PRODUCTION 无效
标题翻译：具有改进的稳定性，效率和/或活性亚的催化剂生产
公开(公告)号：EP1675678A1
公开(公告)日：2006-07-05
申请号：EP04794538.1
申请日：2004-10-07
申请人： UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY CORPORATION
发明人： SERAFIN, Juliana, G. , LIU, Albert Cheng-Yu , SEYEDMONIR, Seyed, R. , SOO, Hwaili , SZYMANSKI, Thomas
IPC分类号： B01J21/06 , B01J23/50 , B01J23/66 , C07D301/10
CPC分类号： C07D301/10 , B01J21/066 , B01J23/50 , B01J23/66 , B01J23/686 , B01J23/688 , B01J35/1009 , B01J35/1042 , B01J35/1076 , B01J37/0018 , B01J37/0201 , B01J37/0203
摘要： A catalyst for the manufacture of alkylene oxide, for example ethylene oxide, by the vapor-phase epoxidation of alkene containing impregnated silver and at least one efficiency-enhancing promoter on an inert, refractory solid support, said support incorporating a sufficient amount of zirconium component (present and remaining substantially as zirconium silicate) as to enhance at least one of catalyst activity, efficiency and stability as compared to a similar catalyst which does not contain the zirconium component.

7. 发明公开

EP1670776A1 A PROCESS FOR THE PRODUCTION OF ALKYLENE OXIDE USING A GAS-PHASE PROMOTER SYSTEM 无效
标题翻译：用于生产亚使用气相启动子系统
公开(公告)号：EP1670776A1
公开(公告)日：2006-06-21
申请号：EP04780699.7
申请日：2004-08-09
申请人： UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY CORPORATION
发明人： ZHANG, Liping , SOO, Hwaili , SERAFIN, Juliana, G.
IPC分类号： C07D301/10
CPC分类号： C07D301/10 , Y02P20/582
摘要： An improved process for the manufacture of ethylene oxide through the epoxidation of ethylene using a catalyst comprising silver and at least one efficiency-enhancing salt of a member of a redox-half reaction pair. Added to the epoxidation reaction is a two-component gas-phase promoter system comprising a chlorine-containing component (for example ethyl chloride, methyl chloride, vinyl chloride and ethylene dichloride), and a nitrogen-containing component of nitric oxide and other compounds capable of generating under reaction conditions at least one gaseous efficiency-enhancing member of a redox-half reaction pair comprising NO, NO2, N2O3 or N2O4. The amount of each component of said gaseous promoter is adjusted to maintain the ration of N* to Z* less than or equal to 1 wherein, N* is the nitric oxide equivalent in ppmv, ranging from 1 to 20 ppmv and Z* =ethyl chloride equivalent (ppmv) * 100 percent / ethane equivalent (mol percent) * 100 ranging from 5 to 40 ppmv.

8. 发明公开

EP1658136A1 IMPROVED ALUMINA CARRIERS AND SILVER-BASED CATALYSTS FOR THE PRODUCTION OF ALKYLENE OXIDES 审中-公开
标题翻译：改进的氧化铝载体，银基催化剂用于生产亚
公开(公告)号：EP1658136A1
公开(公告)日：2006-05-24
申请号：EP04753843.4
申请日：2004-06-02
申请人： UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY CORPORATION
发明人： THORSTEINSON, Erlind, M. , BHASIN, Madan, Mohan , LIU, Albert, Cheng-Yu , SERAFIN, Juliana, G. , SEYEDMONIR, Seyed, R. , SOO, Hwaili
IPC分类号： B01J23/68 , B01J37/06 , C07D301/10 , B01J21/04 , B01J21/12
CPC分类号： B01J23/50 , B01J21/04 , B01J21/12 , B01J23/66 , B01J23/688 , B01J37/0205 , B01J37/0207 , B01J37/06
摘要： An improved carrier useful for preparing a catalyst having excellent catalytic performance when used in the production of alkylene oxide, such as ethylene oxide. The carrier is obtained by a) impregnating a preformed alpha-alumina carrier with at least one modifier selected from among alkali metal silicates and alkaline earth metal silicates, b) drying said impregnated carrier; and c) calcining said dried carrier. The carrier may optionally be washed, prior to being impregnated by conventional catalytic material and/or promoter material.

9. 发明申请

WO2011082033A1 METHOD OF CONTROLLING THE PRODUCTION OF SILVER CHLORIDE ON A SILVER CATALYST IN THE PRODUCTION OF ALKYLENE OXIDES 审中-公开
标题翻译：在生产烷基氧化物中控制银催化剂上生产银氯化物的方法
公开(公告)号：WO2011082033A1
公开(公告)日：2011-07-07
申请号：PCT/US2010/061549
申请日：2010-12-21
申请人： DOW TECHNOLOGY INVESTMENTS LLC , HENSTOCK, William , SERAFIN, Juliana , LIU, Albert , SOO, Hwaili , LIU, Yujun , COLAKYAN, Manuk , PETKAR, Sagar
发明人： HENSTOCK, William , SERAFIN, Juliana , LIU, Albert , SOO, Hwaili , LIU, Yujun , COLAKYAN, Manuk , PETKAR, Sagar
IPC分类号： C07D301/10 , C07D301/32 , C07D301/36
CPC分类号： C07D301/10 , C07D301/32 , C07D301/36 , Y02P20/582
摘要： A plant and process for producing alkylene oxides to control the production of silver chloride on a high efficiency silver catalyst is disclosed and described. The process involves reacting an alkylene and an organic chloride gas phase promoter with oxygen over the high efficiency silver catalyst. The sulfur concentration in the alkylene oxide reactor feed is controlled to reduce the production of silver chloride which acts as a catalyst poison.
摘要翻译：公开和描述了一种用于生产环氧烷以控制高效率银催化剂上氯化银生产的设备和方法。该方法包括在高效率银催化剂上使亚烷基和有机氯化物气相促进剂与氧反应。控制环氧烷反应器进料中的硫浓度以减少作为催化剂毒物的氯化银的产生。

10. 发明申请

WO2012082389A1 METHOD OF STARTING-UP A PROCESS OF PRODUCING AN ALKYLENE OXIDE USING A HIGH-EFFICIENCY CATALYST 审中-公开
标题翻译：使用高效催化剂开始生产烷基氧化铝的方法
公开(公告)号：WO2012082389A1
公开(公告)日：2012-06-21
申请号：PCT/US2011/062856
申请日：2011-12-01
申请人： DOW TECHNOLOGY INVESTMENTS LLC , BASRUR, Arun G. , TUPE, Ravindra R. , SOO, Hwaili , HINMAN, Paul V.
发明人： BASRUR, Arun G. , TUPE, Ravindra R. , SOO, Hwaili , HINMAN, Paul V.
IPC分类号： C07D301/10 , C07B41/00
CPC分类号： C07D301/10 , Y02P20/582
摘要： A method for starting-up a high efficiency alkylene oxide catalyst is described. A feed gas comprising an alkylene, oxygen, and at least one organic chloride is introduced to the catalyst. The molar ratio of oxygen to alkylene, reaction temperature, and overall chloriding effectiveness are adjusted to specified ranges of values within a specified catalyst aging period.
摘要翻译：描述了一种启动高效环氧烷催化剂的方法。将包含亚烷基，氧和至少一种有机氯化物的进料气体引入催化剂。氧气与亚烷基的摩尔比，反应温度和总氯化效果在规定的催化剂老化时段内调整到规定的数值范围。

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