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1. 发明专利

JP2008024570A Structure-controlled carbon nanowall and method for controlling structure of carbon nanowall 有权
标题翻译：纳米结构控制碳纳米管和碳纳米管结构控制方法
公开(公告)号：JP2008024570A
公开(公告)日：2008-02-07
申请号：JP2006201927
申请日：2006-07-25
申请人： Toyota Motor Corp , Univ Nagoya , トヨタ自動車株式会社 , 国立大学法人名古屋大学
发明人： HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI , SUGIYAMA TORU , HAMA YUICHIRO
IPC分类号： C01B31/02 , B01J21/18 , B01J32/00 , H01M4/96
CPC分类号： B01J21/185 , B82Y30/00 , B82Y40/00 , C01B32/18 , H01M4/9083 , H01M4/926 , Y10T428/24355
摘要： PROBLEM TO BE SOLVED: To provide a method for controlling the structure of a carbon nanowall (CNW), in which the inter-wall space of the carbon nanowall (CNW) is varied to control the surface area and crystallinity of the carbon nanowall so that corrosion resistance of the carbon nanowall in a high electrical potential is improved and to provide the structure-controlled carbon nanowall (CNW) having a large surface area and the carbon nanowall (CNW) having high crystallinity. SOLUTION: The carbon nanowall (1) has ≥50 cm 2 /cm 2 -substrate×μm wall surface area. The carbon nanowall (2) has such the crystallinity that the half-value width of the D band of the Raman spectrum measured by using the irradiation laser having 514.5 nm wavelength is ≤85 cm -1 . The carbon nanowall (3) has ≥50 cm 2 /cm 2 -substrate×μm wall surface area and has such the crystallinity that the half-value width of the D band of the Raman spectrum measured by using the irradiation laser having 514.5 nm wavelength is ≤85 cm -1 . COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种控制碳纳米壁（CNW）的结构的方法，其中碳纳米壁（CNW）的壁间空间被改变以控制碳的表面积和结晶度纳米壁，使得在高电位下的碳纳米壁的耐腐蚀性得到改善，并提供具有大表面积的结构受控碳纳米壁（CNW）和具有高结晶度的碳纳米壁（CNW）。解决方案：碳纳米壁（1）具有≥50厘米 2 /厘米 2 - 基板×μm壁面积。碳纳米壁（2）具有通过使用具有514.5nm波长的照射激光器测量的拉曼光谱的D带的半值宽度为≤85cm -1的结晶度。碳纳米壁（3）具有≥50厘米 2 / cm 2 - 基板×μm壁面积，具有如下结晶度：D带的半值宽度通过使用具有514.5nm波长的照射激光器测量的拉曼光谱是≤85cm -1 。版权所有（C）2008，JPO＆INPIT

2. 发明专利

JP2012066966A Plasma cvd device and method of manufacturing carbon nanotube 审中-公开
标题翻译：等离子体CVD装置及制造碳纳米管的方法
公开(公告)号：JP2012066966A
公开(公告)日：2012-04-05
申请号：JP2010213250
申请日：2010-09-24
申请人： Nagoya Univ , Toyota Motor Corp , トヨタ自動車株式会社 , 国立大学法人名古屋大学
发明人： KATAYAMA YUKIHISA , HAMA YUICHIRO , HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： C01B31/02 , C23C16/26
摘要： PROBLEM TO BE SOLVED: To provide a plasma CVD device that eliminates the need to install a bias power source etc., and effectively provides only carbon in material gas to a substrate so as to grow carbon nanotubes by vertical orientation, and a method of manufacturing carbon nanotubes.SOLUTION: The plasma CVD device 10 includes a chamber 1, a plasma generation part 3 and a gas providing part 2 which communicate with the chamber 1, and a placing part 4 on which a substrate K where carbon nanotubes are grown in the chamber 1 is placed. At least carbon material gas is introduced from the gas providing part 2, and a bulk-like shield material 5 is arranged between the plasma generation part 3 and substrate K in the chamber 1.
摘要翻译：要解决的问题：提供一种等离子体CVD装置，其不需要安装偏置电源等，并且有效地仅将碳材料气体提供给基板，以便通过垂直取向生长碳纳米管，并且制造碳纳米管的方法。解决方案：等离子体CVD装置10包括与室1连通的室1，等离子体产生部分3和气体提供部分2以及放置部分4，碳纳米管在其中生长的基板K 放置室1。至少碳材料气体从气体提供部分2引入，并且在等离子体产生部分3和腔室1中的基底K之间布置有块状屏蔽材料5.版权所有：（C）2012，JPO＆INPIT

3. 发明专利

JP2011132068A Method of manufacturing carbon nanotube 审中-公开
标题翻译：制备碳纳米管的方法
公开(公告)号：JP2011132068A
公开(公告)日：2011-07-07
申请号：JP2009292952
申请日：2009-12-24
申请人： Nagoya Univ , Toyota Motor Corp , トヨタ自動車株式会社 , 国立大学法人名古屋大学
发明人： HAMA YUICHIRO , KATAYAMA YUKIHISA , HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： C01B31/02 , B01J23/75
摘要： PROBLEM TO BE SOLVED: To provide a method of mass-producing a quality carbon nanotube with little bending by using a substrate comprising cheaper materials such as aluminum, and magnesium. SOLUTION: The method of manufacturing a carbon nanotube including: a process which covers a coating film 12 comprising a metal or a metal compound on the surface of a substrate 11 including aluminum, magnesium, or zinc; a process which arranges a metal catalyst 15 on the surface of the coating film 12; and a process in which a carbon containing gas is supplied to the substrate 11 in which the metal catalyst 15 has been arranged, and which makes the metal catalyst 15 grow up a carbon nanotube 18, wherein the metal or metal compound has a melting point higher than that of the material composing the substrate 11, and consists of a material which is not alloyed with the metal catalyst 15 in the growth process of the carbon nanotube 18. COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：要解决的问题：提供一种通过使用包含廉价材料如铝和镁的基板来大量生产质量好的碳纳米管的方法。解决方案：制造碳纳米管的方法包括：在包括铝，镁或锌的基板11的表面上覆盖包含金属或金属化合物的涂膜12的工艺; 将金属催化剂15配置在涂膜12的表面上的工序; 并且向其中排列有金属催化剂15的基板11供给含碳气体的方法，使金属催化剂15长大成为碳纳米管18，其中金属或金属化合物的熔点较高比构成基板11的材料的材料组成，并且在碳纳米管18的生长过程中由不与金属催化剂15合金的材料组成。版权所有（C）2011，JPO＆INPIT

4. 发明专利

JP2011103255A Positive electrode for lithium secondary battery and method for preparing thereof 有权
标题翻译：用于锂二次电池的正电极及其制备方法
公开(公告)号：JP2011103255A
公开(公告)日：2011-05-26
申请号：JP2009258395
申请日：2009-11-11
申请人： Nagoya Univ , Toyota Motor Corp , トヨタ自動車株式会社 , 国立大学法人名古屋大学
发明人： YOSHIDA SATOSHI , HAMA YUICHIRO , HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： H01M4/13 , H01M4/139 , H01M4/66 , H01M4/72
CPC分类号： H01M4/131 , H01M4/0416 , H01M4/0423 , H01M4/0428 , H01M4/0473 , H01M4/1391 , H01M4/485 , H01M4/505 , H01M4/525 , H01M4/58 , H01M4/625 , H01M4/663 , H01M10/0525 , Y02E60/122
摘要： PROBLEM TO BE SOLVED: To provide a positive electrode for a lithium secondary battery capable of suppressing the crush of a positive electrode active material layer, with respect to compression from the outside.
SOLUTION: In a positive electrode 10 for a lithium secondary battery, a positive electrode active material layer 30 containing a positive electrode active material 36 is held on a positive electrode collector 20. The positive electrode active material layer 30 includes a carbon nanowalls 32, formed on the positive electrode collector 20 and the positive electrode active material 36 carried by the carbon nanowalls 32.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：解决的问题：为了提供能够抑制正极活性物质层的挤压的锂二次电池的正极，相对于从外部的压缩。解决方案：在锂二次电池用正极10中，将含有正极活性物质36的正极活性物质层30保持在正极集电体20上。正极活性物质层30包括碳纳米壁 32，形成在正极集电体20和由碳纳米壁32承载的正极活性物质36上。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2012218949A Method for manufacturing carbon nanotube 有权
标题翻译：制备碳纳米管的方法
公开(公告)号：JP2012218949A
公开(公告)日：2012-11-12
申请号：JP2011083003
申请日：2011-04-04
申请人： Toyota Motor Corp , Nagoya Univ , トヨタ自動車株式会社 , 国立大学法人名古屋大学
发明人： KATAYAMA YUKIHISA , HAMA YUICHIRO , HORI MASARU , KANO HIROYUKI , HIRAMATSU MINEO
IPC分类号： C01B31/02 , B01J23/755
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a carbon nanotube which can develop a carbon nanotube whose verticality is high and crystallinity is high, stably at a comparatively low temperature.SOLUTION: The method for manufacturing a carbon nanotube consists of a first step which provides any one kind among nickel, cobalt and iron or plural catalytic metals M and carbon C on the substrate W, and a second step which manufactures the carbon nanotube CNT which applies plasma CVD method, provides the plasma decomposed carbon to the substrate W, and develops this plasma decomposed carbon on the substrate W by using the catalytic metal M as a starting point.
摘要翻译：解决的问题：为了提供可以在相当低的温度下稳定地开发垂直度高且结晶度高的碳纳米管的碳纳米管的制造方法。解决方案：碳纳米管的制造方法由在基体W上的镍，钴，铁或多种催化金属M和碳C中提供任意一种的第一工序，第二工序，制造碳纳米管使用等离子体CVD法的CNT将等离子体分解碳提供给基板W，并通过使用催化金属M作为起点，在基板W上形成等离子体分解碳。版权所有（C）2013，JPO＆INPIT

6. 发明专利

JP2011103256A Negative electrode for lithium secondary battery, and method for preparing the negative electrode 有权
标题翻译：用于锂二次电池的负极及其制备负极的方法
公开(公告)号：JP2011103256A
公开(公告)日：2011-05-26
申请号：JP2009258396
申请日：2009-11-11
申请人： Nagoya Univ , Toyota Motor Corp , トヨタ自動車株式会社 , 国立大学法人名古屋大学
发明人： YOSHIDA SATOSHI , HAMA YUICHIRO , HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： H01M4/13 , H01M4/134 , H01M4/1395 , H01M4/66 , H01M4/70 , H01M4/72
CPC分类号： H01M4/1395 , H01M4/0416 , H01M4/0423 , H01M4/0428 , H01M4/0473 , H01M4/134 , H01M4/38 , H01M4/383 , H01M4/625 , H01M4/663 , H01M10/0525 , Y02E60/122
摘要： PROBLEM TO BE SOLVED: To provide a negative electrode for a lithium secondary battery, capable of suppressing the structural breakage of a negative electrode active material layer accompanying charging and discharging.
SOLUTION: In a negative electrode 10 for a lithium secondary battery, a negative electrode active material layer 30, containing a negative electrode active material 36, is held on a negative electrode collector 20. The negative electrode active material layer 30 includes a carbon nanowalls 32, formed on the negative electrode collector 20 and the negative electrode active material 36 carried by the carbon nanowalls 32.
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：解决的问题：提供一种能够抑制伴随充放电的负极活性物质层的结构断裂的锂二次电池用负极。解决方案：在用于锂二次电池的负极10中，将含有负极活性物质36的负极活性物质层30保持在负极集电体20上。负极活性物质层30包括碳纳米管32，形成在负极集电体20上，负极活性物质36由碳纳米壁32承载。版权所有（C）2011，JPO＆INPIT

7. 发明专利

JP2006315881A High density carbon nanotube assembly and method for producing the same 有权
标题翻译：高密度碳纳米管组件及其制造方法
公开(公告)号：JP2006315881A
公开(公告)日：2006-11-24
申请号：JP2005137932
申请日：2005-05-10
申请人： Nu Eco Engineering Kk , Nuエコ・エンジニアリング株式会社 , Univ Meijo , Univ Nagoya , 国立大学法人名古屋大学 , 学校法人名城大学
发明人： HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： C01B31/02 , B82B1/00 , B82B3/00 , C23C16/26 , C23C16/50
摘要： PROBLEM TO BE SOLVED: To provide uniform, high quality and high density carbon nanotubes.
SOLUTION: A buffer layer composed of TiN is formed on an Si-substrate. Co nano-particles having particle diameters of ≤5 nm are deposited on the buffer layer by generating pulse arcs in a range of about 100-300 times by using pulse arc plasma at a vacuum degree of 1×10
-5 Torr. Thereafter, carbon nanotubes are grown to form a high density assembly comprising carbon nanotubes having an average outer diameter of 4 nm and an average inner diameter of 3 nm, being vertical to the substrate and mutually highly parallel. This assembly is uniform and good in the electrical and mechanical characteristics.
COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供均匀，高质量和高密度的碳纳米管。解决方案：在Si衬底上形成由TiN组成的缓冲层。通过使用真空度为1×10 -5 -5℃的脉冲电弧等离子体，通过在约100-300倍的范围内产生脉冲弧，将缓冲层上的粒径为≤5nm的Co纳米颗粒沉积在缓冲层上， SP>乇。此后，生长碳纳米管，形成平均外径为4nm，平均内径为3nm的碳纳米管的高密度组件，其垂直于基板并相互高度平行。该组件均匀且电气和机械特性良好。版权所有（C）2007，JPO＆INPIT

8. 发明专利

JP2007070158A Carbon nanotube assembly and method for producing the same 有权
标题翻译：碳纳米管组件及其制造方法
公开(公告)号：JP2007070158A
公开(公告)日：2007-03-22
申请号：JP2005258581
申请日：2005-09-06
申请人： Nu Eco Engineering Kk , Nuエコ・エンジニアリング株式会社 , Univ Meijo , Univ Nagoya , 国立大学法人名古屋大学 , 学校法人名城大学
发明人： HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： C01B31/02 , B01J23/75 , B01J37/02 , B82B1/00 , B82B3/00
摘要： PROBLEM TO BE SOLVED: To provide single-walled carbon nanotubes having uniform and high quality and a high density. SOLUTION: Co-Ti nanoparticles having particle diameters of ≤2 nm are deposited on an Si-substrate by generating pulse arcs in a range of about 50-100 times by using pulse arc plasma at a vacuum degree of 1×10 -5 Torr. Thereafter, carbon nanotubes are grown to form assemblies of single-walled carbon nanotubes having an average outer diameter of 2 nm and a high density, and being vertical to the substrate and highly parallel with one another. These assemblies have uniform and good electrical and mechanical characteristics. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供具有均匀且高质量和高密度的单壁碳纳米管。解决方案：通过使用真空度为1×10 5的脉冲电弧等离子体，通过在约50-100倍的范围内产生脉冲电弧，将沉积在Si衬底上的粒径为≤2nm的Co-Ti纳米颗粒， SP> -5 乇。然后，生长碳纳米管，形成平均外径为2nm，高密度的单层碳纳米管的组装体，与基板垂直并且彼此高度平行。这些组件具有均匀和良好的电气和机械特性。版权所有（C）2007，JPO＆INPIT

9. 发明专利

JP2006315882A Carbon nanotube assembly and method for producing the same 有权
标题翻译：碳纳米管组件及其制造方法
公开(公告)号：JP2006315882A
公开(公告)日：2006-11-24
申请号：JP2005137933
申请日：2005-05-10
申请人： Nu Eco Engineering Kk , Nuエコ・エンジニアリング株式会社 , Univ Meijo , Univ Nagoya , 国立大学法人名古屋大学 , 学校法人名城大学
发明人： HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： C01B31/02 , B82B1/00 , B82B3/00
CPC分类号： B82Y40/00 , B82Y30/00 , C01B32/162 , C01B2202/36 , H01J1/304 , H01J9/025 , H01J37/32055
摘要： PROBLEM TO BE SOLVED: To provide carbon nanotube assemblies each having a new structure. SOLUTION: A buffer layer composed of TiN is formed on an Si-substrate. Co nano-particles having particle diameters of ≤5 nm are deposited on the buffer layer by generating pulse arcs in a range of about 3-150 times by using pulse arc plasma at a vacuum degree of 1×10 -5 Torr. Thereafter, carbon nanotubes are grown to form carbon nanotube assemblies assembled in a dotted form, each of which has a pyramid shape having a cone shape at its tip end and comprises carbon nanotubes having an average outer diameter of 4 nm and an average inner diameter of 3 nm are formed. These assemblies exhibit high electric field electron emitting efficiency. COPYRIGHT: (C)2007,JPO&INPIT
摘要翻译：要解决的问题：提供各自具有新结构的碳纳米管组件。解决方案：在Si衬底上形成由TiN组成的缓冲层。通过使用1×10 -5真空度的脉冲电弧等离子体，通过在约3-150次的范围内产生脉冲弧，将缓冲层上的粒径为≤5nm的Co纳米粒子沉积在缓冲层上， SP>乇。此后，生长碳纳米管以形成点阵形式的碳纳米管组件，每个碳纳米管组件的顶端具有锥形形状的金字塔形状，并且包括平均外径为4nm，平均内径为形成3nm。这些组件表现出高电场电子发射效率。版权所有（C）2007，JPO＆INPIT

10. 发明专利

JP2008239357A Method for manufacturing carbon nanowall 审中-公开
标题翻译：制造碳纳米管的方法
公开(公告)号：JP2008239357A
公开(公告)日：2008-10-09
申请号：JP2007078038
申请日：2007-03-25
申请人： Nu Eco Engineering Kk , Nuエコ・エンジニアリング株式会社 , Univ Meijo , Univ Nagoya , 国立大学法人名古屋大学 , 学校法人名城大学
发明人： HORI MASARU , HIRAMATSU MINEO , KANO HIROYUKI
IPC分类号： C01B31/02
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/18
摘要： PROBLEM TO BE SOLVED: To improve the crystallinity of a carbon nanowall.
SOLUTION: In a method for manufacturing a carbon nanowall wherein the carbon nanowall is formed on the surface of a substrate by using a plasma atmosphere of a raw material substance containing at least carbon and fluorine as constituent elements and hydrogen, the invented method is characterized by adding the formation of oxygen plasma to the plasma atmosphere.
COPYRIGHT: (C)2009,JPO&INPIT

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