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1. 发明授权

US06271285B1 Ink composition for ink jet recording 失效
标题翻译：用于喷墨记录的油墨组合物
公开(公告)号：US06271285B1
公开(公告)日：2001-08-07
申请号：US09049878
申请日：1998-03-27
申请人： Toshiyuki Miyabayashi , Yasushi Takamatsu , Futoshi Hoshino , Masatoshi Kaneko , Toshihiro Yoshimura
发明人： Toshiyuki Miyabayashi , Yasushi Takamatsu , Futoshi Hoshino , Masatoshi Kaneko , Toshihiro Yoshimura
IPC分类号： C08F22006
CPC分类号： C09D11/30 , C08F8/44
摘要： An ink composition is provided which can realize an image having excellent rubbing/scratch resistance and waterfastness, is free from a clogged nozzle problem, and enables stable printing. The ink composition comprises a colorant, a fine particle of a polymer, a water-soluble organic solvent, and water, the fine particle of the polymer having a film-forming property, a carboxyl group on its surface, and a reactivity with a divalent metal salt such that, when three volumes of an aqueous emulsion, of the fine particle of the polymer, having a fine particle concentration of 0.1% by weight is brought into contact with one volume of an aqueous divalent metal salt solution having a concentration of 1 mol/liter, the time for the transmission of light at a wavelength of 700 nm to be decreased to 50% of the initial transmission is not more than 1×104 sec.
摘要翻译：提供一种能够实现具有优异的摩擦/耐擦伤性和耐水性的图像的墨水组合物，没有堵塞的喷嘴问题，并且能够稳定地印刷。油墨组合物包含着色剂，聚合物的细颗粒，水溶性有机溶剂和水，具有成膜性的聚合物的细颗粒，其表面上的羧基和与二价金属盐，使得当三倍体积的具有0.1重量％的细颗粒浓度的聚合物细颗粒的水性乳液与一体积的浓度为1的二价金属盐水溶液接触时， mol /升，将波长为700nm的光的透射时间减少到初始透射的50％以下的时间不超过1×104秒。

2. 发明授权

US07008901B2 Emulsion for thermal recording material and thermal recording materials made by using the same 有权
标题翻译：用于使用相同的热敏记录材料和热敏记录材料的乳液
公开(公告)号：US07008901B2
公开(公告)日：2006-03-07
申请号：US10611955
申请日：2003-07-03
申请人： Shinjirou Sakurai , Masaya Kusumoto , Masatoshi Kaneko , Futoshi Hoshino
发明人： Shinjirou Sakurai , Masaya Kusumoto , Masatoshi Kaneko , Futoshi Hoshino
IPC分类号： B41M5/40
CPC分类号： B41M5/44 , B01F17/005 , B01J13/0021 , B01J13/0034 , Y10T428/254 , Y10T428/2998
摘要： The present invention provides an emulsion for thermal recording material to be used as the resin component of a protective layer constituting a thermal recording material, characterized by comprising a copolymer resin (A) prepared by copolymerizing (a) methacrylamide with (b) a vinyl monomer having a carboxyl group and resin particles (B) prepared by polymerizing (c) a vinyl monomer, with the resin (A) distributed substantially on the surfaces of the resin particles (B).
摘要翻译：本发明提供一种用作构成热敏记录材料的保护层的树脂组分的热敏记录材料用乳液，其特征在于包含通过使（a）甲基丙烯酰胺与（b）乙烯基单体共聚而制备的共聚物树脂（A）具有羧基和通过聚合（c）乙烯基单体制备的树脂颗粒（B），树脂（A）基本上分布在树脂颗粒（B）的表面上。

3. 发明授权

US5401800A Substantially flat surfaced vinyl polymer emulsion particles having a concavity and process for preparing them 失效
标题翻译：具有凹面的基本平坦的表面的乙烯基聚合物乳液颗粒和用于制备它们的方法
公开(公告)号：US5401800A
公开(公告)日：1995-03-28
申请号：US26242
申请日：1993-03-01
申请人： Futoshi Hoshino , Makoto Nakano , Takeshi Yanagihara
发明人： Futoshi Hoshino , Makoto Nakano , Takeshi Yanagihara
IPC分类号： B41M5/44 , C08F2/00 , C08F2/22 , C08F291/00 , D21H19/42 , D21H19/56 , D21H19/60 , C08K5/00 , C08K7/00
CPC分类号： B41M5/44 , C08F291/00 , D21H19/42 , D21H19/56 , D21H19/60 , Y10T428/24479 , Y10T428/254 , Y10T428/2982
摘要： Substantially flat surfaced emulsion particles polymerized vinyl monomer, having a concavity in at least one of the flat surfaces, a diameter D of from 0.1 to 5.0 .mu.m, and a particle diameter thickness d ratio (d/D) of 1.2 to 5.0 prepared by the step of (1) aqueous emulsion polymerizing a first vinyl monomer or mixture of monomers (a) to form vinyl polymer seed particles; and (2) aqueous emulsion polymerizing a second vinyl monomer or mixture of monomers (b) in the presence of the vinyl polymer seed particles and a non-aqueous organic solvent having a surface tention to water at 20.degree. C. of 48 dyne/cm or more, in a weight ratio of monomer (a) to monomer (b) of 0.5/99.5 to 50/50; and are useful in high performance recording material, paint compositions and paper coating compositions.
摘要翻译：基本上平坦的表面乳状颗粒聚合的乙烯基单体在至少一个平坦表面具有凹陷，直径D为0.1-5.0μm，粒径d（D / D）为1.2-5.0，由（1）水乳液聚合第一乙烯基单体或单体混合物（a）以形成乙烯基聚合物种子颗粒的步骤; 和（2）在乙烯基聚合物种子颗粒和表面具有表达水的20℃下的48达因/厘米的非水有机溶剂的存在下，使第二乙烯基单体或单体（b）的混合物聚合的水性乳液以上，单体（a）与单体（b）的重量比为0.5 / 99.5〜50/50; 并且可用于高性能记录材料，涂料组合物和纸涂料组合物中。

4. 发明授权

US6090892A Redispersible polymer and production process thereof 失效
标题翻译：可再分散聚合物及其制备方法
公开(公告)号：US6090892A
公开(公告)日：2000-07-18
申请号：US679445
申请日：1996-07-12
申请人： Tadashi Ishida , Yoshio Kikuta , Futoshi Hoshino , Katsunari Matsumoto
发明人： Tadashi Ishida , Yoshio Kikuta , Futoshi Hoshino , Katsunari Matsumoto
IPC分类号： C04B24/26 , C08F2/22 , C08F291/00 , C08L33/14
CPC分类号： C04B24/26 , C08F291/00
摘要： Disclosed herein are a (co)polymer comprising, as an essential component, a (co)polymer containing a recurring unit in a predetermined proportion, and its production process. The recurring unit contains a specific amido group and/or a particular hydroxyl group as a pendant group. This (co)polymer is generally obtained in the form of powder and features extremely easy redispersion, and is useful especially as a cement additive for improving physical properties of cement.
摘要翻译：本文公开了包含以预定比例含有重复单元的（共）聚合物作为必要组分的（共）聚合物及其制备方法。重复单元含有特定的酰氨基和/或特定的羟基作为侧基。这种（共）聚合物通常以粉末形式获得，并且具有非常容易的再分散性，并且特别用作改善水泥物理性能的水泥添加剂。

5. 发明授权

US5094998A Fine-particle aggregate emulsion 失效
标题翻译：微粒聚集乳液
公开(公告)号：US5094998A
公开(公告)日：1992-03-10
申请号：US599969
申请日：1990-10-19
申请人： Futoshi Hoshino , Makoto Nakano , Takeshi Yanagihara
发明人： Futoshi Hoshino , Makoto Nakano , Takeshi Yanagihara
IPC分类号： B41M5/44 , C08F2/22 , C08F259/00 , C08F263/02 , C08F265/00 , C08F291/00 , C09D5/02 , D21H19/42
CPC分类号： B41M5/44 , C08F259/00 , C08F263/02 , C08F265/00 , C08F291/00 , C09D5/024 , D21H19/42
摘要： Disclosed in a fine-particle aggregate emulsion comprising aggregate particles formed from a copolymer (a) composed of an unsaturated carboxylic acid and a vinyl monomer copolymerizable therewith, and a foreign polymer (b) formed by polymerization of a vinyl monomer differing in composition from that used in copolymer (a), foreign polymer (b) being present in the form of particles having a diameter of 0.05 to 0.5 .mu., the aggregate particles having a diameter of 0.2 to 3.0 .mu..This fine-particle aggregate emulsion is useful in paints, paper coating and information recording paper.

6. 发明授权

US4948772A Substantially flat surfaced vinyl polymer emulsion particles having a concavity and process for preparing them 失效
标题翻译：具有凹面的基本平坦的表面的乙烯基聚合物乳液颗粒和用于制备它们的方法
公开(公告)号：US4948772A
公开(公告)日：1990-08-14
申请号：US373427
申请日：1989-06-30
申请人： Futoshi Hoshino , Makoto Nakano , Takeshi Yanagihara
发明人： Futoshi Hoshino , Makoto Nakano , Takeshi Yanagihara
IPC分类号： B41M5/44 , C08F2/00 , C08F2/22 , C08F291/00 , D21H19/42 , D21H19/56 , D21H19/60
CPC分类号： B41M5/44 , C08F291/00 , D21H19/42 , D21H19/56 , D21H19/60 , Y10T428/24479 , Y10T428/254 , Y10T428/2982
摘要： Substantially flat surfaced emulsion particles polymerized vinyl monomer, having a concavity in at least one of the flat surfaces, a diameter D of from 0.1 to 5.0 .mu.m, and a particle diameter thickness d ratio (d/D) of 1.2 to 5.0, prepared by the step of (1) aqueous emulsion polymerizing a first vinyl monomer or mixture of monomers (a) to form vinyl polymer seed particles; and (2) aqueous emulsion polymerizing a second vinyl monomer or mixture of monomers (b) in the presence of the vinyl polymer seed particles and a non-aqueous organic solvent having a surface tention to water at 20.degree. C. of 48 dyne/cm or more, in a weight ratio of monomer (a) to monomer (b) of 0.5/99.5 to 50/50; and are useful in high performance recording material, paint compositions and paper coating compositions.
摘要翻译：基本上平坦的表面乳状颗粒聚合的乙烯基单体在至少一个平坦表面具有凹度，直径D为0.1-5.0μm，粒径厚度d比（d / D）为1.2-5.0，制备通过（1）水乳液聚合第一乙烯基单体或单体（a）的混合物以形成乙烯基聚合物种子颗粒的步骤; 和（2）在乙烯基聚合物种子颗粒和表面具有表达水的20℃下的48达因/厘米的非水有机溶剂的存在下，使第二乙烯基单体或单体（b）的混合物聚合的水性乳液以上，单体（a）与单体（b）的重量比为0.5 / 99.5〜50/50; 并且可用于高性能记录材料，涂料组合物和纸涂料组合物中。

7. 发明授权

US5216044A Synthetic core-shell particle resin emulsion, process for producing and coating compositions comprising same 失效
标题翻译：合成核 - 壳颗粒树脂乳液，用于生产和涂覆组合物的方法
公开(公告)号：US5216044A
公开(公告)日：1993-06-01
申请号：US604491
申请日：1990-10-26
申请人： Futoshi Hoshino , Makoto Nakano , Kousuke Someya , Junko Morita , Takeshi Yanagihara
发明人： Futoshi Hoshino , Makoto Nakano , Kousuke Someya , Junko Morita , Takeshi Yanagihara
IPC分类号： C08F2/22 , C08F8/12 , C08F265/00 , C08F265/04 , C08L33/04 , C09D5/00 , C09D5/02 , C09D133/04 , C09D151/00 , D21H19/14 , D21H19/38 , D21H19/56 , D21H21/54
CPC分类号： D21H21/54 , C08F265/04 , C09D151/003 , D21H19/56 , Y10S525/902
摘要： A synthetic resin emulsion whose polymer particles are solid core-shell particles in which form pores spontaneously upon drying is produced by the steps of preparing as core particles from 2 to 60 parts by weight of polymer (A) by emulsion polymerization of from 10 to 80 parts by weight of acrylate ester (a.sub.1) having an alkyl group of from 1 to 3 carbon atoms and from 90 to 20 parts by weight another of vinyl-type monomer (a.sub.2) copolymerizable therewith, forming a shell of a polymer (B) on the surface of the core particles of polymer (A) by emulsion polymerization in the presence thereof of from 98 to 40 parts by weight of vinyl-type monomer (b), different from polymer (a.sub.1) and successively hydrolyzing the core portion of the particles with an alkaline material. Organic pigments prepared from the synthetic resin emulsion can improve the hiding power, brightness, gloss and other properties of articles coated therewith.

8. 发明授权

US5106813A Thermosensitive recording material 失效
标题翻译：耐热记录材料
公开(公告)号：US5106813A
公开(公告)日：1992-04-21
申请号：US500303
申请日：1990-03-28
申请人： Futoshi Hoshino , Makoto Nakano , Kousuke Someya , Junko Morita , Takeshi Yanagihara
发明人： Futoshi Hoshino , Makoto Nakano , Kousuke Someya , Junko Morita , Takeshi Yanagihara
IPC分类号： B41M5/28 , B41M5/30 , B41M5/337 , B41M5/42 , B41M5/44 , C08L33/04 , C08L33/12
CPC分类号： B41M5/44 , B41M2205/04
摘要： A thermosensitive recording paper is disclosed useful for thermosensitive recording which comprises a substrate, a thermosensitive recording layer and an undercoat layer interposed therebetween which contains 10 to 40 parts of a binder and 60 to 90 parts by weight of crosslinked polymer microparticles having a particle diameter of 0.2 to 5.0 .mu.m and a ratio of weight average diameter to number average diameter of 2.0 or less.

9. 发明授权

US5041464A Process for preparing polymer emulsion particles having pores 失效
标题翻译：制备具有孔的聚合物乳液颗粒的方法
公开(公告)号：US5041464A
公开(公告)日：1991-08-20
申请号：US457078
申请日：1989-12-26
申请人： Futoshi Hoshino , Takeshi Yanagihara , Makoto Nakano
发明人： Futoshi Hoshino , Takeshi Yanagihara , Makoto Nakano
IPC分类号： C08F2/22 , C08F6/14 , C08F8/12 , C08F263/04 , C08F291/00 , C09D7/12 , C09D123/26 , D21H19/00 , D21H19/58 , D21H19/60
CPC分类号： D21H19/60 , C08F263/04 , C08F291/00 , C08F8/44 , D21H19/58 , C08F2810/50
摘要： A process for preparing polymer emulsion particles having pores therein, an outside diameter D of 0.1 to 5.0[ , an inside diameter d of 0.05 to 4.0.mu. , and a ratio (d/D) of 0.1 to 0.9 in dry condition, comprising the steps of forming core-shell emulsion particles from specific monomers by two-emulsion polymerizations, and swelling the core of the particles with water by hydrolyzing the vinyl acetate part of polymer (A), thereby inducing the hydroxyl groups therein, e.g., using an acidic material or a basic material at 50.degree. to 100.degree. C. The particles when use as a pigment in coating compositions provide excellent converage rate, brightness, gloss and water resistance.

10. 发明授权

US5500286A Multi-shell emulsion particle 失效
标题翻译：多壳乳液颗粒
公开(公告)号：US5500286A
公开(公告)日：1996-03-19
申请号：US341110
申请日：1994-11-18
申请人： Kousuke Someya , Akihiro Yamazaki , Futoshi Hoshino , Takeshi Yanagihara
发明人： Kousuke Someya , Akihiro Yamazaki , Futoshi Hoshino , Takeshi Yanagihara
IPC分类号： B41M5/44 , C08F2/22 , C08F285/00 , D21H19/20 , B32B27/30 , C08F257/02 , C08F265/02 , C08F265/04
CPC分类号： B41M5/44 , C08F285/00 , D21H19/20 , Y10T428/2989
摘要： A multi-shell emulsion particle of dry state structure having one or more of penetrating pore(s) connecting the surface layer of the particle with the interior of the particle and having a particle diameter of from 0.1 to 5.0.mu. preferably from 0.1 to 1.2.mu.. The particles can be prepared by carrying out emulsion polymerization of a vinyl monomer (a) containing from 5 to 80% by weight of an unsaturated carboxylic acid to obtain a polymer (A), forming a polymer (B) in the presence of a particle consisting of the resultant polymer (A) while adding a vinyl monomer (b) in an amount of 10 times by weight or less and at a rate of 3 times by weight per hour or more for the weight of the polymer (A), and treating the resultant multi-shell emulsion polymer with an alkaline material to neutralize and swell the polymer (A); or, after the neutralization treatment, further forming a polymer (C) by adding and emulsion-polymerizing a vinyl monomer (c) in an amount of 20 times by weight or less for the total weight of the polymer (A) and polymer (B). The emulsion particle is useful as a component of resin compositions for paints, paper-coating and heat-sensitive recording materials.
摘要翻译：一种干状结构的多壳乳液颗粒，其具有将颗粒的表面层与颗粒内部连接的一个或多个渗透孔，其粒径为0.1〜5.0μm，优选为0.1〜1.2μm 。可以通过进行含有5〜80重量％的不饱和羧酸的乙烯基单体（a）的乳液聚合来制备颗粒，从而获得聚合物（A），在颗粒存在下形成聚合物（B）在聚合物（A）的重量中加入乙烯基单体（b）的量为10重量份以下，以每小时3倍的速度加入得到的聚合物（A），以及用碱性物质处理得到的多壳乳液聚合物以中和和膨胀聚合物（A）; 或者在中和处理后，通过将聚合物（A）和聚合物（B）的总重量的20重量％以下的乙烯基单体（c）加入并乳液聚合，进一步形成聚合物（C））。乳液颗粒可用作涂料，纸涂层和热敏记录材料的树脂组合物的组分。

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