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1. 发明申请

US20180025957A1 POLYPHENYLENE SULFIDE RESIN COMPOSITION, MOLDED PRODUCT FORMED THEREFROM AND METHOD OF PRODUCING SEMICONDUCTOR PACKAGE 审中-公开
公开(公告)号：US20180025957A1
公开(公告)日：2018-01-25
申请号：US15548529
申请日：2016-02-24
申请人： Toray Industries, Inc.
发明人： Naoya Ouchiyama , Hideki Matsumoto , Kei Saitoh , Shunsuke Horiuchi
IPC分类号： H01L23/29 , H01L21/56
CPC分类号： H01L23/293 , B29C45/00 , B29C45/14655 , B29K2081/04 , B29L2031/3406 , C08K3/34 , C08K3/36 , C08K7/00 , C08K7/10 , C08K7/18 , C08K7/20 , C08K2003/2227 , C08K2003/265 , C08K2201/003 , C08L81/02 , C08L81/04 , H01L21/563 , H01L23/29 , H01L23/31
摘要： A polyphenylene sulfide resin composition includes 5-50% by weight of (A) a polyphenylene sulfide resin having a weight-average molecular weight of not less than 10000 and a polydispersity, which is expressed by dividing the weight-average molecular weight by a number-average molecular weight, of not higher than 2.5; and 95-50% by weight of (B) fused silica in a spherical form having a volume-average particle diameter of not less than 0.1 μm and less than 1.0 μm, wherein a total of (A) and (B) is kept at 100% by weight.

2. 发明申请

US20170226292A1 POLYPHENYLENE SULFIDE FIBER 审中-公开
公开(公告)号：US20170226292A1
公开(公告)日：2017-08-10
申请号：US15515519
申请日：2015-09-24
申请人： Toray Industries, Inc.
发明人： Hiroo Katsuta , Reo Mitsunaga , Daisuke Yamamoto , Shunsuke Horiuchi , Yoshitsugu Funatsu
IPC分类号： C08G75/16 , C08L23/32 , C08G75/02 , D01F6/76 , B01D39/08 , C08K5/375 , D01D5/12
CPC分类号： D01F6/765 , D02J1/22 , D02J13/00 , D02J13/005
摘要： A poly(phenylene sulfide) fiber changes little in fiber structure and has excellent long-term heat resistance. Namely, the poly(phenylene sulfide) fiber has a degree of crystallization of 45.0% or higher, a content of movable amorphous components of 15.0% or less, and a weight-average molecular weight of 300,000 or less.

3. 发明申请

US20160137807A1 POLYARYLENE SULFIDE RESIN COMPOSITION AND METHOD FOR PRODUCING SAME 有权
标题翻译：聚亚烷基硫酸酯树脂组合物及其生产方法
公开(公告)号：US20160137807A1
公开(公告)日：2016-05-19
申请号：US14901322
申请日：2014-06-18
申请人： TORAY INDUSTRIES, INC.
发明人： Shu Kaiho , Shunsuke Horiuchi , Kenji Ishitake , Koji Yamauchi
IPC分类号： C08K3/08
CPC分类号： C08K3/08 , C08K2003/0862 , C08K2201/003 , C08L81/02
摘要： A polyarylene sulfide resin composition containing nickel microparticles having an average particle diameter of 0.5 to 20 nm is produced by heating a cyclic polyarylene sulfide in the presence of at least one component selected from components (i), (ii) and (iii).
摘要翻译：含有平均粒径为0.5〜20nm的镍微粒的聚芳硫醚树脂组合物是通过在至少一种选自组分（ⅰ），（ⅱ）和（ⅲ）的组分存在下，加热环状聚芳硫醚来制备的。

4. 发明公开

US20240166875A1 POLYPHENYLENE SULFIDE RESIN COMPOSITION AND MOLDED PRODUCT FORMED FROM SAME 审中-公开
公开(公告)号：US20240166875A1
公开(公告)日：2024-05-23
申请号：US18283672
申请日：2022-03-15
申请人： Toray Industries, Inc.
发明人： Tomohiro Hirase , Hiroyuki Isago , Takeshi Unohara , Shunsuke Horiuchi
IPC分类号： C08L81/02 , F16L11/04
CPC分类号： C08L81/02 , F16L11/04 , C08L2201/02 , C08L2207/02 , C08L2207/53
摘要： A polyphenylene sulfide resin composition includes (a) a polyphenylene sulfide resin and (b) a silicone-based polymer; the content of the component (b) is not less than 3 parts by weight and not more than 40 parts by weight with respect to 100 parts by weight of the component (a); in terms of morphology (phase structure), the polyphenylene sulfide resin composition has a phase-separated structure wherein the component (a) forms a continuous phase and the component (b) forms a dispersed phase in which the component (b) is dispersed with a number average dispersion diameter of not more than 3.0 μm; a test specimen obtained by injection molding of the polyphenylene sulfide resin composition at a cylinder temperature of 310° C. and a mold temperature of 145° C. has a flexural modulus of not more than 3.0 GPa as determined by a flexural test according to ISO 178.

5. 发明申请

US20170130005A1 POLYARYLENE SULFIDE AND METHOD FOR PRODUCING SAME (AS AMENDED) 审中-公开
公开(公告)号：US20170130005A1
公开(公告)日：2017-05-11
申请号：US15321952
申请日：2015-06-30
申请人： TORAY INDUSTRIES, INC.
发明人： Shingo Takechi , Tomoyuki Odashima , Shunsuke Horiuchi
IPC分类号： C08G75/0259 , C08G75/0281 , C08G75/0213
CPC分类号： C08G75/0259 , C08G75/02 , C08G75/0213 , C08G75/0281
摘要： There is provided a polyarylene sulfide configured to satisfy (1) to (4): (1) having a weight-average molecular weight of not less than 10000; (2) having a polydispersity of not greater than 2.5, wherein the polydispersity is expressed by a ratio of the weight-average molecular weight to a number-average molecular weight; (3) having a weight reduction on heating that satisfies an expression of ΔWr=(W1−W2)/W1×100≦0.18(%) (where ΔWr denotes a weight reduction ratio (%) and is a value calculated from a sample weight (W2) at temperature reaching 330° C. relative to a sample weight (W1) at temperature reaching 100° C. in thermogravimetric analysis at a temperature rise rate of 20° C./minute in a non-oxidizing atmosphere at ordinary pressure); and (4) having a nitrogen content of not greater than 200 ppm.

6. 发明授权

US10106655B2 Polyphenylene sulfide fiber 有权
公开(公告)号：US10106655B2
公开(公告)日：2018-10-23
申请号：US15515519
申请日：2015-09-24
申请人： Toray Industries, Inc.
发明人： Hiroo Katsuta , Reo Mitsunaga , Daisuke Yamamoto , Shunsuke Horiuchi , Yoshitsugu Funatsu
IPC分类号： C08G75/00 , C08G75/16 , C08K5/375 , C08L23/32 , D01D5/12 , D01F6/76 , B01D39/08 , C08G75/02
摘要： A poly(phenylene sulfide) fiber changes little in fiber structure and has excellent long-term heat resistance. Namely, the poly(phenylene sulfide) fiber has a degree of crystallization of 45.0% or higher, a content of movable amorphous components of 15.0% or less, and a weight-average molecular weight of 300,000 or less.

7. 发明授权

US09029484B2 Production method of polyarylene sulfide, cyclic polyarylene sulfide pellet and production method thereof 有权
标题翻译：聚芳硫醚，环状聚芳硫醚丸的制造方法及其制造方法
公开(公告)号：US09029484B2
公开(公告)日：2015-05-12
申请号：US14381803
申请日：2013-02-27
申请人： Toray Industries, Inc.
发明人： Akinori Kanomata , Yosuke Nishimura , Shunsuke Horiuchi , Shu Kaiho , Kazusada Takeda , Koji Yamauchi , Junya Suzuki
IPC分类号： C08F283/00 , C08G75/14 , C08G75/06 , C08J3/12 , B29B13/00
CPC分类号： C08G75/14 , B29B13/00 , C08G75/02 , C08G75/06 , C08J3/12 , C08J2381/04
摘要： A production method includes a process (I) of heating a cyclic polyarylene sulfide composition under reduced pressure and a process (II) of heating and polymerizing a cyclic polyarylene sulfide composition. This simple method allows for production of a polyarylene sulfide of the higher molecular weight and can produce a polyarylene sulfide having a narrow molecular weight distribution, low gas generation and high industrial usability. Additionally, pelletization after the process (I) can produce a cyclic polyarylene sulfide pellet having ease of conveyance, excellent molding processability, less gas generation amount and high industrial usability.
摘要翻译：制备方法包括在减压下加热环状聚芳硫醚组合物的方法（I）和加热和聚合环状聚芳硫醚组合物的方法（II）。这种简单的方法允许生产较高分子量的聚芳硫醚，并且可以生产具有窄分子量分布，低气体产生和高工业可用性的聚芳硫醚。另外，工序（I）之后的造粒可以制造出具有易于输送，优异的成型加工性，较少气体产生量和高工业可用性的环状聚芳硫醚丸粒。

8. 发明申请

US20150057429A1 PRODUCTION METHOD OF POLYARYLENE SULFIDE, CYCLIC POLYARYLENE SULFIDE PELLET AND PRODUCTION METHOD THEREOF 有权
标题翻译：聚亚烷基硫化物，环状聚亚烷基硫酸酯粒料的生产方法及其生产方法
公开(公告)号：US20150057429A1
公开(公告)日：2015-02-26
申请号：US14381803
申请日：2013-02-27
申请人： Toray Industries, Inc.
发明人： Akinori Kanomata , Yosuke Nishimura , Shunsuke Horiuchi , Shu Kaiho , Kazusada Takeda , Koji Yamauchi , Junya Suzuki
IPC分类号： C08G75/14 , C08J3/12
CPC分类号： C08G75/14 , B29B13/00 , C08G75/02 , C08G75/06 , C08J3/12 , C08J2381/04
摘要： A production method includes a process (I) of heating a cyclic polyarylene sulfide composition under reduced pressure and a process (II) of heating and polymerizing a cyclic polyarylene sulfide composition. This simple method allows for production of a polyarylene sulfide of the higher molecular weight and can produce a polyarylene sulfide having a narrow molecular weight distribution, low gas generation and high industrial usability. Additionally, pelletization after the process (I) can produce a cyclic polyarylene sulfide pellet having ease of conveyance, excellent molding processability, less gas generation amount and high industrial usability.
摘要翻译：制备方法包括在减压下加热环状聚芳硫醚组合物的方法（I）和加热和聚合环状聚芳硫醚组合物的方法（II）。这种简单的方法允许生产较高分子量的聚芳硫醚，并且可以生产具有窄分子量分布，低气体产生和高工业可用性的聚芳硫醚。另外，工序（I）之后的造粒可以制造出具有易于输送，优异的成型加工性，较少气体产生量和高工业可用性的环状聚芳硫醚丸粒。

9. 发明申请

US20140256907A1 PRODUCTION METHOD OF CYCLIC POLYARYLENE SULFIDE 有权
标题翻译：环状聚亚烷基硫酸盐的生产方法
公开(公告)号：US20140256907A1
公开(公告)日：2014-09-11
申请号：US14353204
申请日：2012-10-22
申请人： TORAY INDUSTRIES, INC.
发明人： Tomoyuki Odashima , Shunsuke Horiuchi , Naoto Kumagai , Koji Yamauchi
IPC分类号： C08G75/14
CPC分类号： C08G75/14 , C07D341/00 , C08G75/02
摘要： There is provided a production method of a cyclic polyarylene sulfide from a reaction mixture including at least a sulfidizing agent (a), a dihalogenated aromatic compound (b) and an organic polar solvent (c). The production method includes: a process 1 of heating the reaction mixture having an arylene unit of not less than 0.80 mol but less than 1.05 mol per 1 mol of the sulfur content in the reaction mixture; and subsequent to the process 1, a process 2 of further causing the reaction to proceed after addition of the dihalogenated aromatic compound (b) to have the arylene unit of not less than 1.05 mol and not greater than 1.50 mol per 1 mol of the sulfur content in the reaction mixture.
摘要翻译：提供了由至少包含硫化剂（a），二卤化芳香族化合物（b）和有机极性溶剂（c）的反应混合物构成的环状聚芳硫醚的制造方法。该制备方法包括：加热反应混合物的反应混合物的方法1，该反应混合物具有相对于反应混合物中每1摩尔硫含量为0.80摩尔但小于1.05摩尔的亚芳基单元; 在方法1之后，进一步使加入二卤代芳族化合物（b）后使反应进行的方法2具有相对于每1摩尔硫为1.05摩尔且不大于1.50摩尔的亚芳基单元反应混合物中的含量。

10. 发明授权

US10294330B2 Polyphenylene sulfide resin composition and method of manufacturing same 有权
公开(公告)号：US10294330B2
公开(公告)日：2019-05-21
申请号：US15748584
申请日：2016-07-22
申请人： Toray Industries, Inc.
发明人： Hidenobu Takao , Shu Kaiho , Shunsuke Horiuchi
IPC分类号： C08K3/08 , C08L81/02 , C08G75/0209
摘要： A polyphenylene sulfide resin composition includes a polyphenylene sulfide resin (a) of 90 to 50% by weight and a polyphenylene sulfide resin (b) and/or a polyphenylene sulfide resin (c) of the total of 10 to 50% by weight blended with the polyphenylene sulfide resin (a), relative to the total of the polyphenylene sulfide resins (a) to (c) as 100% by weight, in which the polyphenylene sulfide resin composition has a change rate of viscosity of 1.5 times or less when the composition is heated at 320° C. for 5 hours.

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