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1. 发明授权

US07304179B2 Method for producing methacrylic acid 有权
标题翻译：生产甲基丙烯酸的方法
公开(公告)号：US07304179B2
公开(公告)日：2007-12-04
申请号：US10569371
申请日：2004-08-27
申请人： Tomomichi Hino , Akira Ogawa
发明人： Tomomichi Hino , Akira Ogawa
IPC分类号： C07C51/16
CPC分类号： C07C51/252 , C07C57/04
摘要： The present invention provides a method for producing methacrylic acid through gas-phase catalytic oxidation of methacrolein or a methacrolein-containing gas with molecular oxygen or a gas containing molecular oxygen by the use of a fixed-bed multitubular reactor comprising a plurality of reaction tubes each having a catalyst layer therein, wherein the above catalyst layer is divided in the direction of the tube axis of a reaction tube into two or more layers, to thereby provide a plurality of reaction zones, and the catalyst is caused to be present in the catalyst layer in such a way that a reaction load ratio CRc(i) per unit mass of the catalyst in each reaction zone becomes 0.8 to 1.0.
摘要翻译：本发明提供了一种通过使用固定床多管反应器通过气相催化氧化甲基丙烯醛或含有异丁烯醛的气体与分子氧或含分子氧的气体来生产甲基丙烯酸的方法，所述固定床多管反应器包括多个反应管在其中具有催化剂层，其中将上述催化剂层沿反应管的管轴方向分成两层或更多层，从而提供多个反应区，并且催化剂存在于催化剂中层，使得各反应区域中的催化剂的每单位质量的反应负荷比CRc（i）为0.8〜1.0。

2. 发明授权

US07462262B2 Vertical multitubular heat exchanger and distillation column system including the same 有权
标题翻译：立式多管式换热器和蒸馏塔系统包括相同
公开(公告)号：US07462262B2
公开(公告)日：2008-12-09
申请号：US10919293
申请日：2004-08-17
申请人： Tomomichi Hino , Akira Ogawa , Shigetoshi Shimauchi , Toshihiro Sato , Yasuhiro Kabu
发明人： Tomomichi Hino , Akira Ogawa , Shigetoshi Shimauchi , Toshihiro Sato , Yasuhiro Kabu
IPC分类号： B01D3/04 , F28F9/02 , F28D7/16
CPC分类号： F28F9/02 , B01D1/06 , B01D3/322 , F28F9/18
摘要： A vertical multitubular heat exchanger that can prevent clogging of a polymerized material and is continuously operable for an extended period of time is provided. The vertical multitubular heat exchanger (1) of the present invention introduces a process fluid containing an easily-polymerizable substance into heat exchanger tubes (28) to perform heat exchange. The vertical multitubular heat exchanger (1) includes a shell (2) extending in a vertical direction, an upper tube sheet (8) and a lower tube sheet (10) respectively disposed at the upper portion (4) and the lower portion (6) of the shell (2), and a plurality of heat exchanger tubes (28) whose outer circumferences (26) of both ends are respectively fixed to the upper tube sheet (8) and the lower tube sheet (10). An upper surface (34) of the upper tube sheet (8) is formed to be sloped and at least one of the heat exchanger tubes (28) is disposed in the vicinity of the lowest position of the upper surface (34) of the upper tube sheet (8).
摘要翻译：提供了可以防止聚合材料堵塞并且可延长连续可操作的垂直多管式热交换器。本发明的立式多管式热交换器（1）将含有易聚合物质的工艺流体引入热交换器管（28）进行热交换。垂直多管式热交换器（1）包括沿垂直方向延伸的壳体（2），分别设置在上部分（4）和下部分（6）处的上管板（8）和下管板（10））和两个外周（26）分别固定在上管板（8）和下管板（10）上的多个热交换器管（28）。上管板（8）的上表面（34）形成为倾斜的，并且至少一个热交换器管（28）设置在上管（28）的上表面（34）的最下位置附近管板（8）。

3. 发明申请

US20060264668A1 Method for producing methacrylic acid 有权
标题翻译：生产甲基丙烯酸的方法
公开(公告)号：US20060264668A1
公开(公告)日：2006-11-23
申请号：US10569371
申请日：2004-08-27
申请人： Tomomichi Hino , Akira Ogawa
发明人： Tomomichi Hino , Akira Ogawa
IPC分类号： C07C51/16 , G06F19/00
CPC分类号： C07C51/252 , C07C57/04
摘要： The present invention provides a method for producing methacrylic acid through gas-phase catalytic oxidation of methacrolein or a methacrolein-containing gas with molecular oxygen or a gas containing molecular oxygen by the use of a fixed-bed multitubular reactor comprising a plurality of reaction tubes each having a catalyst layer therein, wherein the above catalyst layer is divided in the direction of the tube axis of a reaction tube into two or more layers, to thereby provide a plurality of reaction zones, and the catalyst is caused to be present in the catalyst layer in such a way that a reaction load ratio CRc(i) per unit mass of the catalyst in each reaction zone becomes 0.8 to 1.0.
摘要翻译：本发明提供了一种通过使用固定床多管反应器通过气相催化氧化甲基丙烯醛或含有异丁烯醛的气体与分子氧或含分子氧的气体来生产甲基丙烯酸的方法，所述固定床多管反应器包括多个反应管在其中具有催化剂层，其中将上述催化剂层沿反应管的管轴方向分成两层或更多层，从而提供多个反应区，并且催化剂存在于催化剂中层，使得各反应区域中的催化剂的每单位质量的反应负荷比CRc（i）为0.8〜1.0。

4. 发明申请

US20050040023A1 Vertical multitubular heat exchanger and distillation column system including the same 有权
标题翻译：立式多管式换热器和蒸馏塔系统包括相同
公开(公告)号：US20050040023A1
公开(公告)日：2005-02-24
申请号：US10919293
申请日：2004-08-17
申请人： Tomomichi Hino , Akira Ogawa , Shigetoshi Shimauchi , Toshihiro Sato , Yasuhiro Kabu
发明人： Tomomichi Hino , Akira Ogawa , Shigetoshi Shimauchi , Toshihiro Sato , Yasuhiro Kabu
IPC分类号： B01D1/06 , B01D3/32 , F28D7/16 , F28F9/02 , F28F9/18 , F28F19/01 , C10B1/00
CPC分类号： F28F9/02 , B01D1/06 , B01D3/322 , F28F9/18
摘要： A vertical multitubular heat exchanger that can prevent clogging of a polymerized material and is continuously operable for an extended period of time is provided. The vertical multitubular heat exchanger (1) of the present invention introduces a process fluid containing an easily-polymerizable substance into heat exchanger tubes (28) to perform heat exchange. The vertical multitubular heat exchanger (1) includes a shell (2) extending in a vertical direction, an upper tube sheet (8) and a lower tube sheet (10) respectively disposed at the upper portion (4) and the lower portion (6) of the shell (2), and a plurality of heat exchanger tubes (28) whose outer circumferences (26) of both ends are respectively fixed to the upper tube sheet (8) and the lower tube sheet (10). An upper surface (34) of the upper tube sheet (8) is formed to be sloped and at least one of the heat exchanger tubes (28) is disposed in the vicinity of the lowest position of the upper surface (34) of the upper tube sheet (8).
摘要翻译：提供了可以防止聚合材料堵塞并且可延长连续可操作的垂直多管式热交换器。本发明的立式多管式热交换器（1）将含有易聚合物质的工艺流体引入热交换器管（28）进行热交换。垂直多管式热交换器（1）包括沿垂直方向延伸的壳体（2），分别设置在上部分（4）和下部分（6）处的上管板（8）和下管板（10））和两个外周（26）分别固定在上管板（8）和下管板（10）上的多个热交换器管（28）。上管板（8）的上表面（34）形成为倾斜的，并且至少一个热交换器管（28）设置在上管（28）的上表面（34）的最下位置附近管板（8）。

5. 发明申请

US20070161819A1 Process for producing catalyst for methacrylic acid synthesis 有权
标题翻译：用于生产甲基丙烯酸合成催化剂的方法
公开(公告)号：US20070161819A1
公开(公告)日：2007-07-12
申请号：US11631107
申请日：2005-06-24
申请人： Tomoki Fukui , Hiroyuki Naitou , Tomomichi Hino
发明人： Tomoki Fukui , Hiroyuki Naitou , Tomomichi Hino
IPC分类号： C07C51/16 , B01J27/19
CPC分类号： C07C51/252 , B01J23/002 , B01J27/19 , B01J27/199 , B01J37/0009 , B01J37/0045 , B01J37/0236 , B01J2523/00 , C07C57/04 , B01J2523/15 , B01J2523/17 , B01J2523/51 , B01J2523/55 , B01J2523/68 , B01J2523/842
摘要： The present invention provides a method for producing a catalyst for use in synthesizing methacrylic acid which can produce methacrylic acid in high yield, the catalyst for use in synthesizing methacrylic acid which can produce methacrylic acid in high yield and a method for producing methacrylic acid in high yield through gas-phase catalytic oxidation of methacrolein with molecular oxygen. The method for producing the catalyst containing molybdenum and phosphorus for use in synthesizing methacrylic acid is composed of the steps of: preparing a slurry containing at least molybdenum and phosphorus and having specific viscosity in the range of 2.5×10−4 to 7.0×10−4 m2/s, which is a value obtained by dividing viscosity (unit: kg/(m·s)) by specific gravity (unit: kg/m3); obtaining a dried material by drying the slurry; and calcining the dried material at 300 to 500° C.
摘要翻译：本发明提供一种用于合成能够高产率生产甲基丙烯酸的甲基丙烯酸的催化剂的制备方法，用于合成能够高产率生产甲基丙烯酸的甲基丙烯酸的催化剂和高产甲基丙烯酸的方法通过气相催化氧化甲基丙烯醛与分子氧产生。用于合成甲基丙烯酸的含钼和磷的催化剂的制备方法包括以下步骤：制备至少含有钼和磷的浆料，其比粘度范围为2.5×10 -4 通过将粘度（单位：kg /（ms））除以比重得到的值（单位：kg / s）为7.0×10 -4个/秒， m 3）; 通过干燥浆料获得干燥的材料; 并在300〜500℃下煅烧干燥物。

6. 发明授权

US07557061B2 Process for producing catalyst for methacrylic acid synthesis 有权
标题翻译：用于生产甲基丙烯酸合成催化剂的方法
公开(公告)号：US07557061B2
公开(公告)日：2009-07-07
申请号：US11631107
申请日：2005-06-24
申请人： Tomoki Fukui , Hiroyuki Naitou , Tomomichi Hino
发明人： Tomoki Fukui , Hiroyuki Naitou , Tomomichi Hino
IPC分类号： B01J27/19 , C07C51/16
CPC分类号： C07C51/252 , B01J23/002 , B01J27/19 , B01J27/199 , B01J37/0009 , B01J37/0045 , B01J37/0236 , B01J2523/00 , C07C57/04 , B01J2523/15 , B01J2523/17 , B01J2523/51 , B01J2523/55 , B01J2523/68 , B01J2523/842
摘要： The present invention provides a method for producing a catalyst for use in synthesizing methacrylic acid which can produce methacrylic acid in high yield, the catalyst for use in synthesizing methacrylic acid which can produce methacrylic acid in high yield and a method for producing methacrylic acid in high yield through gas-phase catalytic oxidation of methacrolein with molecular oxygen. The method for producing the catalyst containing molybdenum and phosphorus for use in synthesizing methacrylic acid is composed of the steps of: preparing a slurry containing at least molybdenum and phosphorus and having specific viscosity in the range of 2.5×10−4 to 7.0×10−4 m2/s, which is a value obtained by dividing viscosity (unit: kg/(m·s)) by specific gravity (unit: kg/m3); obtaining a dried material by drying the slurry; and calcining the dried material at 300 to 500° C.
摘要翻译：本发明提供一种用于合成可以高产率生产甲基丙烯酸的甲基丙烯酸的催化剂的制备方法，用于合成可高产率生产甲基丙烯酸的甲基丙烯酸的催化剂和高产甲基丙烯酸的方法通过气相催化氧化甲基丙烯醛与分子氧产生。用于合成甲基丙烯酸的含有钼和磷的催化剂的制备方法包括以下步骤：制备至少含有钼和磷的浆料，其比粘度在2.5×10 -4至7.0×10 -4 m 2的范围内 / s，它是通过用粘度（单位：kg /（ms））除以比重（单位：kg / m3）获得的值; 通过干燥浆料获得干燥的材料; 并在300〜500℃下煅烧干燥物。

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