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1. 发明授权

US07642382B2 Processes for preparing ethylamines 失效
标题翻译：制备乙胺的方法
公开(公告)号：US07642382B2
公开(公告)日：2010-01-05
申请号：US11908820
申请日：2006-03-14
申请人： Till Gerlach , Frank Haese , Anton Meier , Johann-Peter Melder , Heinz Rütter
发明人： Till Gerlach , Frank Haese , Anton Meier , Johann-Peter Melder , Heinz Rütter
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , C07C211/05
摘要： Processes comprising: (a) providing a first reactant comprising a bioethanol; and (b) reacting the first reactant with a second reactant comprising a component selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of hydrogen and a catalytically effective amount of a heterogeneous hydrogenation/dehydrogenation catalyst to form an ethylamine; wherein the catalyst has been activated at a temperature of 100 to 500° C. for at least 25 minutes; wherein prior to activation the catalyst comprises: (i) 20 to 65% by weight of a support material comprising one or both of zirconium dioxide (ZrO2) and aluminum oxide (Al2O3), (ii) 1 to 30% by weight of oxygen-comprising compounds of copper, calculated as CuO, and (iii) 21 to 70% by weight of oxygen-comprising compounds of nickel, calculated as NiO; and wherein after activation the catalyst has a CO uptake capacity of >110 μmol of CO/g of the catalyst.
摘要翻译：方法包括：（a）提供包含生物乙醇的第一反应物; 和（b）使第一反应物与包含选自氨，伯胺，仲胺及其混合物的组分的第二反应物在氢气和催化有效量的非均相氢化/脱氢催化剂存在下反应至形成乙胺; 其中所述催化剂已经在100至500℃的温度下活化至少25分钟; 其中在活化之前，催化剂包括：（i）20至65重量％的包含二氧化锆（ZrO 2）和氧化铝（Al 2 O 3）中的一种或两种的载体材料，（ii）1至30重量％包括以CuO计算的铜化合物，和（iii）以NiO计算的含有21重量％的含氧化合物的镍; 并且其中在活化后，催化剂的CO吸收能力为> 110molol的CO / g催化剂。

2. 发明申请

US20090234163A1 Method for producing an ethylamine 失效
标题翻译：乙胺的制造方法
公开(公告)号：US20090234163A1
公开(公告)日：2009-09-17
申请号：US11908820
申请日：2006-03-14
申请人： Till Gerlach , Frank Haese , Anton Meier , Johann-Peter Melder , Heinz Rütter
发明人： Till Gerlach , Frank Haese , Anton Meier , Johann-Peter Melder , Heinz Rütter
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , C07C211/05
摘要： Processes comprising: (a) providing a first reactant comprising a bioethanol; and (b) reacting the first reactant with a second reactant comprising a component selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of hydrogen and a catalytically effective amount of a heterogeneous hydrogenation/dehydrogenation catalyst to form an ethylamine; wherein the catalyst has been activated at a temperature of 100 to 500° C. for at least 25 minutes; wherein prior to activation the catalyst comprises: (i) 20 to 65% by weight of a support material comprising one or both of zirconium dioxide (ZrO2) and aluminum oxide (Al2O3), (ii) 1 to 30% by weight of oxygen-comprising compounds of copper, calculated as CuO, and (iii) 21 to 70% by weight of oxygen-comprising compounds of nickel, calculated as NiO; and wherein after activation the catalyst has a CO uptake capacity of >110 μmol of CO/g of the catalyst.
摘要翻译：方法包括：（a）提供包含生物乙醇的第一反应物; 和（b）使第一反应物与包含选自氨，伯胺，仲胺及其混合物的组分的第二反应物在氢气和催化有效量的非均相氢化/脱氢催化剂存在下反应至形成乙胺; 其中所述催化剂已经在100至500℃的温度下活化至少25分钟; 其中在活化之前，催化剂包括：（i）20至65重量％的包含二氧化锆（ZrO 2）和氧化铝（Al 2 O 3）中的一种或两种的载体材料，（ii）1至30重量％包括以CuO计算的铜化合物，和（iii）以NiO计算的含有21重量％的含氧化合物的镍; 并且其中在活化后，催化剂的CO吸收能力为> 110molol的CO / g催化剂。

3. 发明授权

US07563933B2 Method for producing an ethylamine 失效
标题翻译：乙胺的制造方法
公开(公告)号：US07563933B2
公开(公告)日：2009-07-21
申请号：US10581733
申请日：2004-12-22
申请人： Anton Meier , Johann-Peter Melder , Till Gerlach , Frank Haese
发明人： Anton Meier , Johann-Peter Melder , Till Gerlach , Frank Haese
IPC分类号： C07C209/16
CPC分类号： B01J20/0233 , B01D15/00 , B01J8/0285 , B01J8/0292 , B01J20/0296 , B01J20/186 , B01J20/3204 , B01J20/3236 , B01J23/755 , C07C29/76 , C07C209/16 , Y02E50/17 , C07C211/05 , C07C31/08
摘要： Process for preparing an ethylamine by reacting ethanol with ammonia, a primary amine or a secondary amine in the presence of hydrogen and a heterogeneous catalyst, in which a biochemically prepared ethanol (bioethanol) in which the concentration of sulfur and/or sulfur-containing compounds has been reduced beforehand by bringing it into contact with an adsorbent is used.
摘要翻译：在氢气和非均相催化剂存在下，使乙醇与氨，伯胺或仲胺反应制备乙胺的方法，其中生物化学制备的乙醇（生物乙醇），其中硫和/或含硫化合物的浓度通过使其与吸附剂接触而预先减少。

4. 发明申请

US20070112218A1 Method for producing a ethylamine 失效
标题翻译：乙胺的制造方法
公开(公告)号：US20070112218A1
公开(公告)日：2007-05-17
申请号：US10581733
申请日：2004-12-22
申请人： Anton Meier , Johann-Peter Melder , Till Gerlach , Frank Haese
发明人： Anton Meier , Johann-Peter Melder , Till Gerlach , Frank Haese
IPC分类号： C07C209/14
CPC分类号： B01J20/0233 , B01D15/00 , B01J8/0285 , B01J8/0292 , B01J20/0296 , B01J20/186 , B01J20/3204 , B01J20/3236 , B01J23/755 , C07C29/76 , C07C209/16 , Y02E50/17 , C07C211/05 , C07C31/08
摘要： Process for preparing an ethylamine by reacting ethanol with ammonia, a primary amine or a secondary amine in the presence of hydrogen and a heterogeneous catalyst, in which a biochemically prepared ethanol (bioethanol) in which the concentration of sulfur and/or sulfur-containing compounds has been reduced beforehand by bringing it into contact with an adsorbent is used.
摘要翻译：在氢气和非均相催化剂存在下，使乙醇与氨，伯胺或仲胺反应制备乙胺的方法，其中生物化学制备的乙醇（生物乙醇），其中硫和/或含硫化合物的浓度通过使其与吸附剂接触而预先减少。

5. 发明申请

US20070167530A1 Method for depletion of sulphur and/or compounds containing sulphur from a biochemically produced organic compound 审中-公开
标题翻译：从生物化学生产的有机化合物中消耗硫和/或含硫化合物的方法
公开(公告)号：US20070167530A1
公开(公告)日：2007-07-19
申请号：US10583409
申请日：2004-12-22
申请人： Till Gerlach , Johann-Peter Melder , Bram Hoffer , Anton Meier
发明人： Till Gerlach , Johann-Peter Melder , Bram Hoffer , Anton Meier
IPC分类号： A61K31/045 , C12P7/06 , C07C29/76
CPC分类号： B01J20/103 , B01D15/00 , B01J20/08 , B01J20/18 , B01J20/186 , B01J20/20 , C10G25/003 , C10G25/05 , Y02E50/17
摘要： Method of reducing the concentration of sulfur and/or a sulfur-containing compound in a biochemically prepared organic compound by bringing the respective organic compound into contact with an adsorbent. Ethanol which has a particular specification and can be prepared by the abovementioned method, and its use as solvent, disinfectant, as component in pharmaceutical or cosmetic products or in foodstuffs or in cleaners, as feed in steam reforming processes for the synthesis of hydrogen or in fuel cells, or as building block in chemical synthesis.
摘要翻译：通过使各有机化合物与吸附剂接触来降低生物化学制备的有机化合物中硫和/或含硫化合物的浓度的方法。具有特定规格并且可以通过上述方法制备的乙醇及其作为溶剂，消毒剂，作为药物或化妆品中的组分或在食品或清洁剂中的组分的用途，作为用于合成氢气的蒸汽重整方法中的进料燃料电池，或作为化学合成的组成部分。

6. 发明授权

US07119231B2 Method for producing alkanolamines 有权
公开(公告)号：US07119231B2
公开(公告)日：2006-10-10
申请号：US10297052
申请日：2001-06-07
申请人： Matthias Frauenkron , Ulrich Müller , Wolfgang Harder , Jörg Unger , Johann-Peter Melder , Anton Meier , Walter Himmel
发明人： Matthias Frauenkron , Ulrich Müller , Wolfgang Harder , Jörg Unger , Johann-Peter Melder , Anton Meier , Walter Himmel
IPC分类号： C07C213/04
CPC分类号： C07C213/04 , Y02P20/582 , C07C215/08 , C07C215/12
摘要： At least one alkanolamine is prepared by reacting ammonia with alkylene oxide in a reaction space in the presence of a catalyst to give monoalkanolamine or dialkanolamine or trialkanolamine or a mixture of two or three of these compounds, the distribution of the various alkanolamines within the product spectrum being controlled by means of the temperature in the reaction space, by a process in which the temperature is established by regulating the temperature profile in the reaction space.

7. 发明授权

US09086191B2 Method for safely preventing backflowing in the conveying of a fluid 有权
标题翻译：用于在流体输送中安全防止回流的方法
公开(公告)号：US09086191B2
公开(公告)日：2015-07-21
申请号：US13001467
申请日：2009-06-16
申请人： Franz Borgel , Alfred Krause , Mirko Kreitschmann , Anton Meier , Frank-Friedrich Pape , Wolfgang Reif , Michael Salla
发明人： Franz Borgel , Alfred Krause , Mirko Kreitschmann , Anton Meier , Frank-Friedrich Pape , Wolfgang Reif , Michael Salla
IPC分类号： F17D1/08 , F17D1/14 , F16K15/00
CPC分类号： F17D1/14 , F16K15/00 , Y10T137/0396
摘要： A method for reliably avoiding backflow in the transport of a liquid under pressure via a transport pipe (1), in which a shut-off device (2) with differential pressure switching is arranged, into a container (3) which is under pressure and which comprises the liquid to be transported and/or another liquid is proposed, wherein a pressure accumulator (4) which is filled with the liquid to be transported up to a certain level and above the liquid level, in direct contact with the liquid to be transported, with an inert gas is arranged in the transport pipe (1) upstream from the shut-off device (2) in the transport direction, the inert gas being provided in the pressure accumulator (4) under an excess pressure and in an amount relative to the container (3) to be filled which are designed so that, in the case of a drop in the pressure in the transport pipe (1), the inert gas ensures a positive pressure difference in the transport pipe (1) to the container (3) over a period which is at least as long as the reaction time of the shut-off device (2) and the shut-off device (2) has an emptying pipe (6) with emptying valve (7).
摘要翻译：一种用于可靠地避免在压力下输送液体的回流的方法，该输送管（1）具有压差切换的切断装置（2），其中所述输送管（1）设置在处于压力下的容器（3）中，其包括待运输的液体和/或另一种液体，其中填充有待运输的液体达到一定水平并高于液面的压力蓄积器（4）与液体直接接触在输送方向上从切断装置（2）的上游配置有惰性气体输送的惰性气体，惰性气体在过压压力下设置在蓄压器（4）中，相对于被填充的容器（3），其被设计成使得在输送管（1）中的压力下降的情况下，惰性气体确保输送管（1）中的正压差容器（3）至少在一段时间内只要关闭装置（2）和切断装置（2）的反应时间具有排空阀（7）的排空管（6）。

8. 发明申请

US20120157719A1 TUBE BUNDLE REACTOR FOR UNCATALYZED OR HOMOGENEOUSLY CATALYZED REACTIONS 有权
标题翻译：用于未加氢化或均相催化反应的管组反应器
公开(公告)号：US20120157719A1
公开(公告)日：2012-06-21
申请号：US13380207
申请日：2010-01-19
申请人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerliing , Beatrice Rössler-Feigel , Anton Meier , Christian Müller
发明人： Joaquim Henrique Teles , Peter Resch , Wilhelm Ruppel , Ulrike Wegerle , Wolfgang Gerliing , Beatrice Rössler-Feigel , Anton Meier , Christian Müller
IPC分类号： C07C45/00 , B01J19/00
CPC分类号： B01J19/2425 , B01J4/001 , B01J19/006 , B01J2219/00085 , B01J2219/00166 , F28D7/16 , F28F9/0265 , F28F9/0275 , F28F9/0278 , Y02P20/582
摘要： The invention relates to a tube bundle reactor with a flat feed hood. Alternatively, the release hood may also have a flat design. The flat design reduces the heat of reaction which arises in the hood in the case of reaction types which take place not only in the tube bundle (uncatalyzed reactions and reactions with homogeneously distributed catalyst). This greatly suppresses undesired reactions which already take place in the hood owing to accumulated heat, which achieves a higher selectivity in the case of thermally sensitive reactions. In addition, the thermal distribution within the hoods can be controlled precisely.The tube bundle reactor comprises a tube bundle which has a feed end which is connected to a feed hood of the tube bundle reactor, wherein the feed hood is configured in a flat design with a cross-sectional area at the feed end and an internal volume, and the ratio of internal volume to cross-sectional area is less than 0.35 m. The invention is further implemented by means of a process for operating a tube bundle reactor, comprising: introducing a reactant mixture into a tube bundle and converting at least a proportion of the reactant mixture within the tube bundle to a product. The introducing comprises: feeding the reactant mixture into an interior of a feed hood of the tube bundle reactor and passing the reactant mixture on into a feed end of the tube bundle in the form of a fluid stream. The fluid stream has a cross-sectional area on entry into the feed end, and the interior of the feed hood through which the fluid stream flows has an internal volume; where the ratio of internal volume to cross-sectional area is less than 0.35 m.
摘要翻译：本发明涉及具有扁平进料罩的管束反应器。或者，释放罩也可以具有平坦的设计。在反应类型不仅在管束（未催化的反应和具有均匀分布的催化剂的反应）的情况下，扁平设计减少了发动机罩中产生的反应热。这大大地抑制了由于积热而在罩中发生的不期望的反应，这在热敏反应的情况下实现了更高的选择性。此外，可以精确地控制罩内的热分布。管束反应器包括管束，其具有连接到管束反应器的进料罩的进料端，其中进料罩构造成平坦设计，在进料端具有横截面积，内部体积，内部体积与横截面积的比值小于0.35μm。通过用于操作管束反应器的方法进一步实现本发明，其包括：将反应物混合物引入管束并将至少一部分管束内的反应物混合物转化成产物。引入包括：将反应物混合物进料到管束反应器的进料罩的内部，并将反应物混合物以流体流的形式送入管束的进料端。流体流在进入进料端时具有横截面面积，流体流流过的进料罩的内部具有内部容积; 其中内部体积与横截面积的比值小于0.35μm。

9. 发明授权

US4461898A Process for the preparation of novel light stabilizers 失效
标题翻译：制备新型光稳定剂的方法
公开(公告)号：US4461898A
公开(公告)日：1984-07-24
申请号：US437929
申请日：1982-11-01
申请人： Anton Meier , Eduard Troxler
发明人： Anton Meier , Eduard Troxler
IPC分类号： C07D211/46 , C08K5/3432 , C08K5/3435 , C09D7/12 , C07D401/12 , C07D401/06 , C08K5/34
CPC分类号： C07D211/46 , C08K5/3435
摘要： Mixtures of esters of polyalkylpiperidine derivatives, of the formulae I and II ##STR1## in which the proportions of I to II are 95 to 70% by weight and 5 to 30% by weight, are obtained by reacting about 2 mols of a piperidine of the formula III ##STR2## with 0.9 to 1.3 mols of a diester of the formula IV ##STR3## in the melt at between 100.degree. and 145.degree. C., in the presence of an alkali metal amide as a catalyst.The mixtures of esters thus obtained are very suitable as light stabilizers for plastics.
摘要翻译：得到式I和II的多烷基哌啶衍生物的酯的混合物，其中I至II的比例为95至70重量％和5至30重量％，其中得到通过使约2摩尔的式III（III）的哌啶与熔体中的0.9至1.3摩尔的式IV（II）的二酯在100-145℃之间，在碱金属酰胺作为催化剂的存在。由此获得的酯的混合物非常适合作为塑料的光稳定剂。

10. 发明申请

US20100191018A1 PROCESS FOR PREPARING PURE CYCLODODECANONE 有权
标题翻译：制备纯环己酮的方法
公开(公告)号：US20100191018A1
公开(公告)日：2010-07-29
申请号：US12694815
申请日：2010-01-27
申请人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
发明人： Joaquim Henrique Teles , Beatrice Rößler-Feigel , Alexander Hauk , Anton Meier , Christian Müller , Michael Schelper , Tanja Kirchner , Susanne Szeschkus , Rolf Pinkos , Gerd-Dieter Tebben
IPC分类号： C07C45/27
CPC分类号： C07C45/82 , C07C45/28 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： The present invention relates to a process for preparing at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group, at least comprising the stages: (a1) oxidation of a composition (A), at least comprising one cyclic olefin with Z cycles and 7 to 16 carbon atoms and at least two C—C double bonds, by means of dinitrogen monoxide to give a composition (A1), (a2) separating off the at least one cyclic olefin with Z cycles and 7 to 16 carbon atoms with at least two C—C double bonds from the composition (A1) in order to obtain a composition (A2), and (b) distillative treatment of the composition (A2) from step (a2) in order to obtain a composition (B), comprising the at least one cyclic compound with Z cycles and 7 to 16 carbon atoms with a keto group and less than 1.0% by weight of the at least one compound with Z−1 cycles and 7 to 16 carbon atoms with at least one aldehyde group, where Z can be 1, 2, 3 or 4.
摘要翻译：本发明涉及一种制备具有Z环和至少具有7至16个碳原子的酮基的至少一种环状化合物的方法，至少包括以下步骤：（a1）组合物（A）的氧化，至少包含一个环状烯烃，Z循环和7至16个碳原子和至少两个C-C双键，借助于一氧化二氮，得到组合物（A1），（a2）以Z循环分离至少一种环状烯烃， 16个碳原子与来自组合物（A1）的至少两个C-C双键，以获得组合物（A2），和（b）从步骤（a2）中的组合物（A2）的蒸馏处理，以获得组合物（B），其包含至少一种Z循环的环状化合物和具有酮基的7至16个碳原子和小于1.0重量％的至少一种具有Z-1循环和7至16个碳原子的化合物，至少一个醛基，其中Z可以是1,2,3或4个。

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