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    • 1. 发明授权
    • Process of manufacturing high strength aluminum foil
    • 制造高强度铝箔的工艺
    • US06533877B1
    • 2003-03-18
    • US09622488
    • 2000-12-06
    • Thomas L. DavissonLuc M. MontgrainSadashiv Nadkarni
    • Thomas L. DavissonLuc M. MontgrainSadashiv Nadkarni
    • C22F104
    • C22C21/00B21B1/40B21B3/003B21B2003/001C22F1/04
    • High strength foil having dead fold foil characteristics is produced without the rolling and other production problems encountered with prior high strength foils by controlling manganese content, interannealing temperatures and, optionally, final annealing temperatures. The alloy contains 0.05 to 0.15 %, preferably 0.095 to 0.125%, manganese by weight. Cold worked sheet is interannealed at a temperature of about 200° C. to about 260° C., preferably 230° to 250 ° C., to produce substantially fully recrystallized sheet while maintaining most of the manganese in solid solution. The interannealed sheet is rolled to final gauge and finally annealed, preferably at a temperature of about 250° C. to about 325° C., more preferably about 260° C. to about 325° C., to produce dead fold aluminum foil with a yield strength of at least 89.6 MPa (13 ksi), and ultimate tensile strength of at least 103.4 MPa (15 ksi) and a Mullen rating of at least 89.6 kPa (13 psi) at a gauge of 0.0015 cm (0.0006 inch).
    • 通过控制锰含量,中和退火温度和任选的最终退火温度,产生具有死折箔特性的高强度箔,而不会产生现有高强度箔遇到的轧制和其它生产问题。 合金含有0.05〜0.15重量%,优选为0.095〜0.125重量%。 冷加工片材在约200℃至约260℃,优选230℃至250℃的温度下进行脱水,以产生基本上完全重结晶的片材,同时将大部分锰保持在固溶体中。 将退火后的片材轧制成最终规格,最后退火,优选在约250℃至约325℃,更优选约260℃至约325℃的温度下进行退火,以产生具有 屈服强度至少为89.6MPa(13ksi),极限拉伸强度至少为103.4MPa(15ksi),马伦等级为0.006cm(0.0006英寸),至少为89.6kPa(13psi)。
    • 2. 发明授权
    • Aluminum alloy composition and method of manufacture
    • 铝合金组成及其制造方法
    • US06350532B1
    • 2002-02-26
    • US09381882
    • 2000-01-18
    • Thomas L. DavissonLuc MontgrainDaniel PulliamSadashiv Nadkarni
    • Thomas L. DavissonLuc MontgrainDaniel PulliamSadashiv Nadkarni
    • B21C3700
    • C22F1/04B21B3/003B21B2003/001C22C21/00Y10T428/12431
    • The invention relates to a recyclable aluminum foil. The foil is made of an alloy containing 0.2%-0.5% Si, 0.4%-0.8% Fe, 0.1%-0.3% Cu, and 0.05%-0.3% Mn by weight. with the balance aluminum and incidental impurities. The foil contains at least about 2% by weight of strengthening particulates and has at least about 0.1% by weight of the copper and/or manganese retained in solid solution. The invention also relates to a method of manufacturing a sheet of aluminum based on an alloy which involves continuously casting an alloy of the above composition to form a sheet of alloy, coiling said sheet of alloy, cold rolling the sheet of alloy, interannealing the alloy after a first pass of the cold rolling; and further cold rolling the alloy to a final desired gauge. The foil, which is suitable for household use, has improved strength due to a larger quantity of dispersoids fortified by elements in solid solution, and can be recycled with other alloy scrap.
    • 本发明涉及可回收的铝箔。 箔由含有0​​.2%-0.5%Si,0.4%-0.6%Fe,0.1%-0.3%Cu和0.05%-0.3%Mn的合金制成。 余量为铝和杂质。 箔包含至少约2重量%的强化颗粒,并且具有保留在固溶体中的至少约0.1重量%的铜和/或锰。 本发明还涉及一种制造基于合金的铝片的方法,该方法包括连续铸造上述组成的合金以形成合金片,卷绕所述合金片,冷轧合金片,将合金中间退火 经过第一次冷轧; 并进一步将合金冷轧至最终所需的规格。 适用于家庭用途的箔片由于固溶体中的元素强化而分散质量较大,因而具有改善的强度,并可与其他合金废料一起回收利用。
    • 6. 发明授权
    • Process for the preparation of hollow microspheres
    • 中空微球的制备方法
    • US4782097A
    • 1988-11-01
    • US100090
    • 1987-09-23
    • Mukesh JainSadashiv Nadkarni
    • Mukesh JainSadashiv Nadkarni
    • B01J13/12B01J13/20C08J3/14C08J9/08C08J9/32B01J13/02
    • B01J13/20B01J13/12C08J3/14C08J9/08
    • A process for forming hollow microspheres containing carbon or a polymer which is a carbon precursor. The process comprises forming a solution in a liquid solvent of a polymer having the following properties (a) a molecular weight of at least 10,000 and a long chain structure; (b) an ability to be coagulated by or precipitated from the solution by a non-solvent for the polymer; (c) an ability to form a continuous stretchable film when coagulated or precipitated from solution; (d) a chemical structure which is infusible or capable of being rendered infusible, and (e) a high carbon yield of at least 30% by weight upon being carbonized in a non-reactive atmosphere. An insoluble particulate blowing agent is incorporated into the solution and the solution is then divided into droplets and the droplets are introduced into a liquid bath containing a suitable non-solvent for the polymer. The non-solvent causes the polymer to precipitate or coagulate rapidly and simultaneously the blowing agent is decomposed to generate a gas within the droplets so that hollow microspheres are formed. The microspheres are then optionally subjected to carbonization in a non-reactive atmosphere at high temperature to convert the polymer to carbon. Uniformly-sized relatively large hollow microspheres can be produced by this process.
    • 一种形成含有碳或作为碳前体的聚合物的中空微球的方法。 该方法包括在具有以下特性(a)至少10,000的分子量和长链结构的聚合物的液体溶剂中形成溶液; (b)通过聚合物的非溶剂使溶液凝固或沉淀的能力; (c)当从溶液凝结或沉淀时形成连续拉伸膜的能力; (d)不熔或能够熔化的化学结构,和(e)在非反应性气氛中碳化时,至少30重量%的高碳产率。 将不溶性颗粒发泡剂并入溶液中,然后将溶液分成液滴,并将液滴引入包含用于聚合物的合适的非溶剂的液体浴中。 非溶剂使聚合物快速沉淀或凝结,同时发泡剂分解,在液滴内产生气体,形成中空微球体。 然后任选地在非反应性气氛中在高温下将微球碳化,以将聚合物转化为碳。 可以通过该方法制造均匀尺寸的相对较大的中空微球。
    • 7. 发明申请
    • Method of making metal surfaces wettable
    • 使金属表面可润湿的方法
    • US20070023115A1
    • 2007-02-01
    • US11472201
    • 2006-06-20
    • Adriano FerreiraThomas DavissonSadashiv Nadkarni
    • Adriano FerreiraThomas DavissonSadashiv Nadkarni
    • C22F1/04
    • C23C22/03C23C22/82
    • A method of treating a surface of a metal foil or sheet to make the surface wettable. The method comprises obtaining a metal foil or sheet having an oil-coated surface to be treated, applying a solution of phosphoric acid in a polar, non-aqueous, water-free solvent evenly to the surface at a rate of application in a range of at least 10 mg/ft2, the phosphoric acid being contained in the solution at a concentration such that the phosphoric acid contacts the surface in an amount of 0.5 to 2.0 mg/ft2; and removing the solvent by either drying the surface or heating the foil or sheet at an elevated temperature above ambient to evaporate the oil from the surface to be treated with the proviso that the elevated temperature does not fall in the range between 130 to 240° C. The resulting foil has a wettable surface and can be used, for example, for coating with a layer of another material (e.g. polymer or adhesive) and achieve high peel strength.
    • 一种处理金属箔或片的表面以使表面可润湿的方法。 该方法包括获得具有待处理的油涂层表面的金属箔或片材,在极性,非水性,无水溶剂中将磷酸溶液以适用的速度均匀地施加到表面上, 至少10mg / ft 2,磷酸以浓度使得磷酸以0.5-2.0mg / ft 2的量与表面接触, SUP>; 并且通过干燥表面或者在高于环境温度的高温下加热箔或片来除去溶剂,以便从被处理表面蒸发油,条件是升高的温度不在130-240℃的范围内 所得到的箔具有可润湿表面,并且可以用于例如用另一种材料(例如聚合物或粘合剂)层涂覆并实现高剥离强度。
    • 10. 发明授权
    • Process for producing silicon nitride
    • 氮化硅生产工艺
    • US4990471A
    • 1991-02-05
    • US262605
    • 1988-10-26
    • Mukesh K. JainSadashiv Nadkarni
    • Mukesh K. JainSadashiv Nadkarni
    • C01B21/068
    • C01B21/0685
    • A process for forming silicon nitride containing little or no silicon carbide. The process involves producing a uniform dispersion of finely divided silica particles in a polymer, heating the polymer/silica dispersion in a non-oxidizing atmosphere to carbonize the polymer, and heating the resulting carbonized product to a temperature in the range of 1300.degree.-1800.degree. C. in a non-oxidizing nitrogen-containing atmosphere. This latter heating step is carried out in the presence of a metal oxide (preferably alumina which is capable, in the reaction conditions, of reducing the amount of silicon carbide formed as an undesired by-product.
    • 一种形成少量或不含碳化硅的氮化硅的方法。 该方法包括在聚合物中产生细分二氧化硅颗粒的均匀分散体,在非氧化气氛中加热聚合物/二氧化硅分散体以使聚合物碳化,并将所得碳化产物加热至1300-11800℃的温度 在非氧化性含氮气氛中。 后一加热步骤在金属氧化物(优选氧化铝)的存在下进行,氧化铝在反应条件下能够减少作为不期望的副产物形成的碳化硅的量。