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1. 发明授权

US5116956A Polyazo dye compounds having vinylsulfone type and pyridinium type fiber reactive groups 失效
标题翻译：具有乙烯基砜型和吡啶类型纤维反应性基团的聚氨酯染料化合物
公开(公告)号：US5116956A
公开(公告)日：1992-05-26
申请号：US524743
申请日：1990-05-17
申请人： Tetsuya Miyamoto , Kazufumi Yokogawa , Yutaka Kayane , Takashi Omura , Takeshi Washimi , Naoki Harada , Kingo Akahori
发明人： Tetsuya Miyamoto , Kazufumi Yokogawa , Yutaka Kayane , Takashi Omura , Takeshi Washimi , Naoki Harada , Kingo Akahori
IPC分类号： C09B62/44
CPC分类号： C09B62/4415
摘要： A polyazo compound of the following formula, ##STR1## wherein X is ##STR2## --NR.sub.2 R.sub.3, --OR.sub.4 or --SR.sub.5, in which R.sub.1 is hydrogen or alkyl, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, A is phenylene, naphthylene or alkylene, Z is a fiber-reactive group of --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Z' in which Z' is a splittable group, Y is pyridinio, and F is polyazo dye moiety carrying a fiber-reactive group like that represented by Z, which compound is useful for dyeing or printing fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.

2. 发明授权

US5112959A Polyazo dye compounds having plural vinylsulfone type fiber reactive groups in one molecule 失效
标题翻译：在一个分子中具有多种乙烯基纤维素类型的纤维反应组的聚氨基染料化合物
公开(公告)号：US5112959A
公开(公告)日：1992-05-12
申请号：US526708
申请日：1990-05-22
申请人： Tetsuya Miyamoto , Kazufumi Yokogawa , Yutaka Kayane , Takashi Omura , Takeshi Washimi , Naoki Harada , Kingo Akahori
发明人： Tetsuya Miyamoto , Kazufumi Yokogawa , Yutaka Kayane , Takashi Omura , Takeshi Washimi , Naoki Harada , Kingo Akahori
IPC分类号： C09B62/513
CPC分类号： C09B62/513
摘要： A polyazo compound of the following formula, ##STR1## wherein A is phenylene, naphthylene or alkylene, X is --NR.sub.2 R.sub.3, --OR.sub.4 or --SR.sub.5 in which R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are each hydrogen, alkyl, phenyl, naphthylene or benzyl, Z is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Z' in which Z' is a splittable group, R.sub.1 is hydrogen or alkyl, and F is polyazo dye moiety carrying a fiber reactive group like that represented by Z. This compound is useful for the dyeing or printing of fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.

3. 发明授权

US5104978A Monoazo red reactive dye compound having a vinylsulfone type fiber reactive group and a substituted triazinyl group 失效
标题翻译：具有乙烯基纤维素类型纤维反应性基团和取代的三嗪基的MONOAZO红色反应性染料化合物
公开(公告)号：US5104978A
公开(公告)日：1992-04-14
申请号：US439244
申请日：1989-11-20
申请人： Kingo Akahori , Masayuki Miki , Takashi Omura , Naoki Harada , Takeshi Washimi
发明人： Kingo Akahori , Masayuki Miki , Takashi Omura , Naoki Harada , Takeshi Washimi
IPC分类号： C09B62/44
CPC分类号： C09B62/4413
摘要： A monoazo compound represented by the following formula in the free acid form: ##STR1## wherein D is unsubstituted or substituted phenylene or naphthylene, X is unsubstituted or substituted pyridinio, Z is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 L in which L is a group capable of being split by the action of an alkali, and Y is --V--R in which V is --O-- or --S--, and R is hydrogen or which may be substituted alkyl, cyclohexyl, phenyl which may be substituted, naphthyl which may be substituted or benzyl which may be substituted, or ##STR2## in which R.sub.1 and R.sub.2 independently of one another are each hydrogen or unsubstituted or substituted alkyl, phenyl, naphthyl or benzyl, which is superior in solubility and useful for dyeing or printing fiber materials such as cellulose to a red color with superior build-up properties.

4. 发明授权

US5235046A Triazine compounds and method for dyeing or printing fiber materials using the same 失效
标题翻译：三氮唑化合物和使用该方法染色或印刷纤维材料的方法
公开(公告)号：US5235046A
公开(公告)日：1993-08-10
申请号：US793096
申请日：1991-11-18
申请人： Kingo Akahori , Masayuki Miki , Yutaka Kayane , Takeshi Washimi
发明人： Kingo Akahori , Masayuki Miki , Yutaka Kayane , Takeshi Washimi
IPC分类号： C09B62/04 , C09B62/085 , C09B62/503 , C09B62/505 , C09B62/51 , C09B62/513 , C09B62/515 , D06P1/38 , D06P1/384 , D06P3/66
CPC分类号： C09B62/503
摘要： A triazine compound which is useful for dyeing or printing materials containing hydroxyl group and/or amide group, and which has the following formula (I) or salts thereof ##STR1## wherein R represents hydrogen or unsubstituted or substituted alkyl; R.sub.1 represents hydrogen, an alkyl unsubstituted or substituted by carboxy, sulfo, alkoxy, halogeno, sulfato or hydroxy, or --Y--SO.sub.2 Z.sub.3 ; R.sub.2 represents hydrogen or unsubstituted or substituted alkyl; A represents unsubstituted or substituted phenylene or naphthylene; Y represents a divalent group which is C.sub.2 -C.sub.7 alkylene and so on; Z.sub.1, Z.sub.2 and Z.sub.3 independently of one another are each --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 Z' wherein Z' is a group capable of being split by the action of an alkali; and F is any one of the dye residue which is anthraquinone, azo, disazo, trisazo or phthalocyanine nucleus and so on, and a process for dyeing or printing fiber materials which comprises using said triazine compounds or salts thereof.

5. 发明授权

US5606092A Monoazo compounds and method for dyeing or printing fiber materials using the same 失效
标题翻译：单偶氮化合物和使用其的纤维材料的染色或印花方法
公开(公告)号：US5606092A
公开(公告)日：1997-02-25
申请号：US546321
申请日：1995-10-20
申请人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
发明人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
IPC分类号： C09B62/085 , C09B62/44 , C09B62/51 , D06P1/384 , C07C317/28 , C07C317/34
CPC分类号： C09B62/4413 , C09B62/51
摘要： A monoazo compound of the following formula, ##STR1## wherein D is phenylene or naphthylene; X is halogeno, pyridinio or ##STR2## B is --OR.sub.3, --SR.sub.4, ##STR3## in which R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, r is 0 or 1, and E is O, SO, SO.sub.2, CH.sub.2 or NR.sub.8, in which R.sub.8 is hydrogen or C.sub.1 -C.sub.4 alkyl; R, R.sub.1, R.sub.2 and R.sub.7 are each hydrogen or alkyl; A.sub.1, A.sub.2 and A.sub.3 are each phenylene, naphthylene or alkylene; Z.sub.1, Z.sub.2 and Z.sub.3 are each --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a splittable group; and p is 0 or 1; which compound is useful for dyeing or printing fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的单偶氮化合物，其中D是亚苯基或亚萘基; X是卤素，吡啶鎓或B是-OR 3，-SR 4，其中R 3，R 4，R 5和R 6各自是氢，烷基，苯基，萘基或苄基，r是0或1，E是 O，SO，SO 2，CH 2或NR 8，其中R 8是氢或C 1 -C 4烷基; R，R 1，R 2和R 7各自为氢或烷基; A1，A2和A3各自为亚苯基，亚萘基或亚烷基; Z 1，Z 2和Z 3各自为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y为可裂解基团; p为0或1; 该化合物可用于染色或印刷纤维材料以获得染色或印刷成具有优异的各种牢度性能的颜色的产品，具有优异的聚集性能。

6. 发明授权

US5488098A Monoazo compounds having vinylsulfone type fiber reactive group and method for dyeing or printing fiber materials using the same 失效
标题翻译：具有乙烯基砜型纤维反应性基团的单偶氮化合物和使用其的纤维材料的染色或印花方法
公开(公告)号：US5488098A
公开(公告)日：1996-01-30
申请号：US193646
申请日：1994-02-07
申请人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
发明人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
IPC分类号： C09B62/085 , C09B62/44 , C09B62/51 , D06P1/384
CPC分类号： C09B62/4413 , C09B62/51
摘要： A monoazo compound of the following formula, ##STR1## wherein D is phenylene or naphthylene; X is halogeno, pyridinio or ##STR2## B is --OR.sub.3, --SR.sub.4, ##STR3## in which R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, r is 0 or 1, and E is O, SO, SO.sub.2, CH.sub.2 or NR.sub.8, in which R.sub.8 is hydrogen or C.sub.1 -C.sub.4 alkyl; R, R.sub.1, R.sub.2 and R.sub.7 are each hydrogen or alkyl; A.sub.1, A.sub.2 and A.sub.3 are each phenylene, naphthylene or alkylene; Z.sub.1, Z.sub.2 and Z.sub.3 are each --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a splittable group; and p is 0 or 1; which compound is useful for dyeing or printing fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的单偶氮化合物，其中D是亚苯基或亚萘基; X是卤素，吡啶鎓或B是-OR 3，-SR 4，其中R 3，R 4，R 5和R 6各自是氢，烷基，苯基，萘基或苄基，r是0或1，E是 O，SO，SO 2，CH 2或NR 8，其中R 8是氢或C 1 -C 4烷基; R，R 1，R 2和R 7各自为氢或烷基; A1，A2和A3各自为亚苯基，亚萘基或亚烷基; Z 1，Z 2和Z 3各自为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y为可裂解基团; p为0或1; 该化合物可用于染色或印刷纤维材料以获得染色或印刷成具有优异的各种牢度性能的颜色的产品，具有优异的聚集性能。

7. 发明授权

US5359040A Monoazo compounds having naphthylazonaphtylamino group and use therefor for dyeing or printing fiber materials 失效
标题翻译：具有萘氮杂萘基氨基的单偶氮化合物，用于染色或印刷纤维材料
公开(公告)号：US5359040A
公开(公告)日：1994-10-25
申请号：US963553
申请日：1992-10-20
申请人： Kingo Akahori , Masayuki Miki , Takeshi Washimi , Yutaka Kayane
发明人： Kingo Akahori , Masayuki Miki , Takeshi Washimi , Yutaka Kayane
IPC分类号： C07D251/54 , C09B62/085 , C09B62/51 , D06P1/384
CPC分类号： C09B62/51
摘要： A monoazo compound represented by the following formula (I) in the free acid form: ##STR1## wherein X is an alkylamino, C.sub.5 -C.sub.7 cycloalkylamino, piperidino, pyrrolidino or morpholino group which is unsubstituted or substituted with a substituent other than sulfo, R is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 alkyl, R.sub.1 and R.sub.2 independently of one another are each hydrogen, methoxy, ethoxy, methyl, ethyl, chloro, bromo, nitro, carboxy or sulfo, Z is vinyl or -CH.sub.2 CH.sub.2 Y in which Y is a group which is split by the action of an alkali and p is 0 or 1. This compound is a reactive dye suitable for dyeing or printing fiber materials containing hydroxyl group and/or amide group in red color. This compound is high in dissolvability and can give dyed or printed products excellent in dyeability such as build-up property and various fastnesses.
摘要翻译：由游离酸形式的下式（I）表示的单偶氮化合物：其中X是未被取代或被取代基以外的取代基取代的烷基氨基，C 5 -C 7环烷基氨基，哌啶子基，吡咯烷子基或吗啉代基磺基，R为氢或未取代或取代的C 1 -C 4烷基，R 1和R 2各自独立地为氢，甲氧基，乙氧基，甲基，乙基，氯，溴，硝基，羧基或磺基，Z为乙烯基或-CH2CH2Y Y是通过碱的作用而分裂的基团，p是0或1.该化合物是适用于染色或印刷含有红色的羟基和/或酰胺基的纤维材料的活性染料。该化合物的溶解性高，可以赋予染色性，印染性等优异的染色性，例如聚集性和各种坚牢度。

8. 发明授权

US5637705A Bisazo compounds and use thereof as fiber reactive dyes 失效
标题翻译：双偶氮化合物及其作为纤维活性染料的用途
公开(公告)号：US5637705A
公开(公告)日：1997-06-10
申请号：US532510
申请日：1995-09-22
申请人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
发明人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
IPC分类号： C09B62/513 , C07D251/52 , C07D251/54
CPC分类号： C09B62/513
摘要： A bisazo compound of the following formula: ##STR1## wherein R.sup.1 and R.sup.3 are each hydrogen or alkyl; D is phenylene or naphthylene; one of X.sup.1 and X.sup.2 is NH.sub.2 and the other is OH; Z.sup.1 and Z.sup.2 are each --CH.dbd.CH.sub.2 or --CH.dbd.CH.sub.2 Z' in which Z' is a splittable group; B is monosulfophenylene, monosulfophenylene-methylene or mono- or di-sulfonaphthylene-methylene; U is phenylene or an aliphatic bridging group; and J is an amono-derivative group or, J may be alkoxy when X.sup.1 is OH and U is phenylene, and J may be alkoxy or phenoxy when X.sup.1 is OH and U is the aliphatic bridging group. This compound is useful for dyeing or printing fiber materials and gives a dyed or printed product having a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的双偶氮化合物：其中R 1和R 3各自为氢或烷基; D是亚苯基或亚萘基; X1和X2之一是NH2，另一个是OH; Z 1和Z 2各自为-CH = CH 2或-CH = CH 2 Z'，其中Z'为可裂组; B是单磺酰亚砜，单磺酰亚苯基 - 亚甲基或单 - 或二 - 磺基亚乙基 - 亚甲基; U是亚苯基或脂族桥基; 并且J是氨基衍生基团，或者当X1是OH且U是亚苯基时，J可以是烷氧基，当X 1是OH且U是脂族桥基时，J可以是烷氧基或苯氧基。该化合物可用于染色或印刷纤维材料，并提供具有优异的各种牢度性能的优异的成色性能的染色或印刷产品。

9. 发明授权

US5306814A Bisazo compounds having sulfophenylazonaphtylazophenylamino-s-triazinyl group and use thereof for dyeing or printing fiber materials 失效
标题翻译：具有磺基苯基偶氮萘基偶氮苯基氨基-s-三嗪基的双偶氮化合物及其用于染色或印刷纤维材料的用途
公开(公告)号：US5306814A
公开(公告)日：1994-04-26
申请号：US993713
申请日：1992-12-17
申请人： Kingo Akahori , Takeshi Washimi , Takashi Omura , Mahito Fujita
发明人： Kingo Akahori , Takeshi Washimi , Takashi Omura , Mahito Fujita
IPC分类号： C09B62/09 , C09B62/513 , D06P1/384
CPC分类号： C09B62/513 , C09B62/09
摘要： A bisazo compound represented by the following formula (I) in the free acid form: ##STR1## wherein R is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 alkyl; A is an unsubstituted or substituted phenylene or naphthylene group; Z is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a group capable of being split by the action of an alkali; X is --NR.sub.1 R.sub.2, C.sub.5 -C.sub.7 cycloalkylamino or ##STR2## in which Q is --CH.sub.2 --, --O--, --SO.sub.2 --, --SO-- or --NR.sub.3 -- in which R.sub.3 is hydrogen or C.sub.1 -C.sub.4 alkyl; and n is 1 or 2; R.sub.1 is hydrogen or unsubstituted or substituted alkyl; R.sub.2 is hydrogen or an unsubstituted or substituted alkyl or phenyl group; and m is 1 or 2, provided that when m is 2, X is ##STR3## This compound is suitable for dyeing and printing cellulose fiber, natural and synthetic polyamide fibers, polyurethane fiber, leather and mixed yarns thereof, to obtain dyed or printed products of a color fast to light and wetness with superior build-up property.
摘要翻译：由游离酸形式的下式（I）表示的双偶氮化合物：（*化学结构*）（I）（*化学结构*）其中R为氢或未取代或取代的C 1 -C 4烷基; A是未取代或取代的亚苯基或亚萘基; Z是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y是能够通过碱的作用而分裂的基团; X是-NR 1 R 2，C 5 -C 7环烷基氨基或（*化学结构*）其中Q是-CH 2 - ， - O - ， - SO 2 - ， - SO-或-NR 3 - ，其中R 3是氢或C 1 -C 4烷基; n为1或2; R1是氢或未取代或取代的烷基; R2是氢或未取代或取代的烷基或苯基; m为1或2，条件是当m为2时，X为（*化学结构*）该化合物适用于染色和印刷纤维素纤维，天然和合成聚酰胺纤维，聚氨酯纤维，皮革及其混纺纱线，以获得染色或印刷的产品，颜色快速，轻盈，具有优异的积聚性能。

10. 发明授权

US5478927A Bisazo compounds and use thereof as fiber reactive dyes 失效
标题翻译：双偶氮化合物及其作为纤维活性染料的用途
公开(公告)号：US5478927A
公开(公告)日：1995-12-26
申请号：US188755
申请日：1994-01-31
申请人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
发明人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
IPC分类号： C09B62/513 , D06P1/384
CPC分类号： C09B62/513
摘要： A bisazo compound of the following formula: ##STR1## wherein R.sup.1 and R.sup.3 are each hydrogen or alkyl; D is phenylene or naphthylene; one of X.sup.1 and X.sup.2 is NH.sub.2 and the other is OH; Z.sup.1 and Z.sup.2 are each --CH.dbd.CH.sub.2 or --CH.dbd.CH.sub.2 Z' in which Z' is a splittable group; B is monosulfophenylene, monosulfophenylene-methylene or mono- or di-sulfonaphthylene-methylene; U is phenylene or an aliphatic bridging group; and J is an amono-derivative group or, J may be alkoxy when X.sup.1 is OH and U is phenylene, and J may be alkoxy or phenoxy when X.sup.1 is OH and U is the aliphatic bridging group. This compound is useful for dyeing or printing fiber materials and gives a dyed or printed product having a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的双偶氮化合物：其中R 1和R 3各自为氢或烷基; D是亚苯基或亚萘基; X1和X2之一是NH2，另一个是OH; Z 1和Z 2各自为-CH = CH 2或-CH = CH 2 Z'，其中Z'为可裂组; B是单磺酰亚砜，单磺酰亚苯基 - 亚甲基或单 - 或二 - 磺基亚乙基 - 亚甲基; U是亚苯基或脂族桥基; 并且J是氨基衍生基团，或者当X1是OH且U是亚苯基时，J可以是烷氧基，当X 1是OH且U是脂族桥基时，J可以是烷氧基或苯氧基。该化合物可用于染色或印刷纤维材料，并提供具有优异的各种牢度性能的优异的成色性能的染色或印刷产品。

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