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1. 发明申请

US20070166543A1 Metal oxide phosphor microparticle and process for producing the same; utilizing the same, dispersion liquid, fluorescence conversion membrane, method of separating metal oxide phosphor microparticle, fluorescent liquid, fluorescent paste, phosphor and process for producing the same; and fluorescence converter 审中-公开
标题翻译：金属氧化物荧光体微粒及其制造方法; 利用其分散液，荧光转换膜，分离金属氧化物荧光体微粒的方法，荧光液体，荧光膏，荧光体及其制造方法; 和荧光转换器
公开(公告)号：US20070166543A1
公开(公告)日：2007-07-19
申请号：US10587631
申请日：2005-01-26
申请人： Tetsuhiko Isobe , Ryo Kasuya , Aya Kawano , Hitoshi Kuma , Junichi Katano
发明人： Tetsuhiko Isobe , Ryo Kasuya , Aya Kawano , Hitoshi Kuma , Junichi Katano
IPC分类号： B32B5/16
CPC分类号： C09K11/7774 , C09K11/02 , H01L27/322 , H05B33/14 , Y10S977/783 , Y10S977/786 , Y10T428/25 , Y10T428/256 , Y10T428/2991
摘要： In accordance with the present invention, there are provided metal oxide-based phosphor microfine particles comprising a matrix crystal made of a metal oxide and a metal element doped as an emission center into the matrix crystal, wherein the microfine particles are provided with an organic group coordinated to a surface thereof, have a small particle size as well as a high affinity to and a high dispersibility in light-transmittable resins, and are inhibited from scattering light emitted from a light source; a process for producing the metal oxide-based phosphor microfine particles; a dispersion of the metal oxide-based phosphor microfine particles; a fluorescent conversion film; a method of separating the metal oxide-based phosphor microfine particles; a fluorescent liquid; a fluorescent paste; a phosphor; a process for producing the phosphor; and a fluorescent converter.
摘要翻译：根据本发明，提供了金属氧化物系荧光体微粒子，其包含由金属氧化物构成的基体晶体和掺杂到基体晶体中作为发光中心的金属元素，其中，所述微细粒子设置有有机基团与其表面配位，具有小的粒径以及对可透光树脂的高亲和力和高分散性，并且被抑制从光源发射的光散射; 金属氧化物系荧光体微粒子的制造方法; 金属氧化物系荧光体微粒子的分散液; 荧光转换膜; 分离金属氧化物系荧光体微粒子的方法; 荧光液体荧光膏; 磷光体荧光体的制造方法; 和荧光转换器。

2. 发明申请

US20090127510A1 Fine particle and red fluorescence conversion medium using the same 审中-公开
标题翻译：细颗粒和红色荧光转化介质使用相同
公开(公告)号：US20090127510A1
公开(公告)日：2009-05-21
申请号：US11920831
申请日：2006-05-10
申请人： Tetsuhiko Isobe , Ryo Kasuya , Junichi Katano
发明人： Tetsuhiko Isobe , Ryo Kasuya , Junichi Katano
IPC分类号： C09K11/02 , B32B5/16
CPC分类号： C09K11/7708 , C09D11/50 , C09K11/7736 , Y10T428/2982
摘要： Particles including at least a metal oxide represented by the following formula and having a number-average particle diameter of 100 nm or less; AxLyMzOu wherein A is an alkali metal selected from Li, Na, K, Cs and Rb, or silver; L is a trivalent rare earth element selected from Sc, Y, La, Ce, Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb and Lu; M is W, Mo, Cr, Mn, Ru, Os, Ir or Re; x is 0 to 2; y is 0.5 to 2; z is 0.5 to 4; and u is 5 to 10.
摘要翻译：至少包含由下式表示的数均粒径为100nm以下的金属氧化物的粒子; <？in-line-formula description =“In-line Formulas”end =“lead”？> AxLyMzOu <？in-line-formula description =“In-line Formulas”end =“tail”？>其中A是碱选自Li，Na，K，Cs和Rb的金属或银; L是选自Sc，Y，La，Ce，Pr，Nd，Pm，Sm，Eu，Gd，Tb，Dy，Ho，Er，Tm，Yb和Lu中的三价稀土元素; M是W，Mo，Cr，Mn，Ru，Os，Ir或Re; x为0〜2; y为0.5〜2; z为0.5〜4; 你是5到10。

3. 发明授权

US07883641B2 Metal oxide phosphor microparticle and process for producing the same; utilizing the same, dispersion liquid, fluorescence conversion membrane, method of separating metal oxide phosphor microparticle, fluorescent liquid, fluorescent paste, phosphor and process for producing the same; and fluorescence converter 失效
标题翻译：金属氧化物荧光体微粒及其制造方法; 利用其分散液，荧光转换膜，分离金属氧化物荧光体微粒的方法，荧光液体，荧光膏，荧光体及其制造方法; 和荧光转换器
公开(公告)号：US07883641B2
公开(公告)日：2011-02-08
申请号：US12546162
申请日：2009-08-24
申请人： Tetsuhiko Isobe , Ryo Kasuya , Aya Kawano , Hitoshi Kuma , Junichi Katano
发明人： Tetsuhiko Isobe , Ryo Kasuya , Aya Kawano , Hitoshi Kuma , Junichi Katano
IPC分类号： C09K11/08
CPC分类号： C09K11/7774 , C09K11/02 , H01L27/322 , H05B33/14 , Y10S977/783 , Y10S977/786 , Y10T428/25 , Y10T428/256 , Y10T428/2991
摘要： In accordance with the present invention, there are provided metal oxide-based phosphor microfine particles comprising a matrix crystal made of a metal oxide and a metal element doped as an emission center into the matrix crystal, wherein the microfine particles are provided with an organic group coordinated to a surface thereof, have a small particle size as well as a high affinity to and a high dispersibility in light-transmittable resins, and are inhibited from scattering light emitted from a light source; a process for producing the metal oxide-based phosphor microfine particles; a dispersion of the metal oxide-based phosphor microfine particles; a fluorescent conversion film; a method of separating the metal oxide-based phosphor microfine particles; a fluorescent liquid; a fluorescent paste; a phosphor; a process for producing the phosphor; and a fluorescent converter.
摘要翻译：根据本发明，提供了金属氧化物系荧光体微粒子，其包含由金属氧化物构成的基体晶体和掺杂到基体晶体中作为发光中心的金属元素，其中，所述微细粒子设置有有机基团与其表面配位，具有小的粒径以及对可透光树脂的高亲和力和高分散性，并且被抑制从光源发射的光散射; 金属氧化物系荧光体微粒子的制造方法; 金属氧化物系荧光体微粒子的分散液; 荧光转换膜; 分离金属氧化物系荧光体微粒子的方法; 荧光液体荧光膏; 磷光体荧光体的制造方法; 和荧光转换器。

4. 发明申请

US20060011890A1 Phosphor and production process for the same 失效
标题翻译：磷光体和生产工艺相同
公开(公告)号：US20060011890A1
公开(公告)日：2006-01-19
申请号：US11038112
申请日：2005-01-21
申请人： Tetsuhiko Isobe
发明人： Tetsuhiko Isobe
IPC分类号： C09K11/02 , C09K11/08 , C09K11/54
CPC分类号： C09K11/02 , C09K11/574 , Y02P20/544 , Y10S977/811 , Y10S977/834 , Y10T428/2991 , Y10T428/2998
摘要： The object of the present invention is to provide a phosphor which is excellent in transparency, light transmittance, luminescence efficiency and luminescent intensity and at the same time, processes for producing the phosphor. Preferred embodiments of the invention include a phosphor characterized in that phosphor particles represented by the general formula [(L)a(M)b(N)cOd:Y] are covered with an organic compound bearing at least one functional group at a terminal or side chain, wherein L is a metallic element such as Zn; M is a metallic element such as Al; N is Si or Ge; O is oxygen; Y is at least one activating agent such as Mn2+, Eu2+, Cu2+ or Yb2+; and a, b, c and d are each a value satisfying the relationships 0
摘要翻译：本发明的目的是提供透明性，透光率，发光效率和发光强度优异的荧光体，同时提供荧光体的制造方法。本发明的优选实施方案包括一种荧光体，其特征在于由通式[（L）a（M）b（N） Y]被末端或侧链具有至少一个官能团的有机化合物覆盖，其中L是诸如Zn的金属元素; M是金属元素，如Al; N是Si或Ge; O是氧; Y是至少一种活化剂，例如Mn 2+，Eu 2+，Cu 2+，或者Yb 2+， SUP>; 并且a，b，c和d分别是满足关系0

5. 发明授权

US06447698B1 Method for producing light-emitting substance 失效
标题翻译：发光物质的制造方法
公开(公告)号：US06447698B1
公开(公告)日：2002-09-10
申请号：US09398753
申请日：1999-09-17
申请人： Masaru Ihara , Igarashi Takahiro , Tsuneo Kusunoki , Katsutoshi Ohno , Mamoru Senna , Tetsuhiko Isobe , Miho Konishi
发明人： Masaru Ihara , Igarashi Takahiro , Tsuneo Kusunoki , Katsutoshi Ohno , Mamoru Senna , Tetsuhiko Isobe , Miho Konishi
IPC分类号： C09K1102
CPC分类号： C09K11/574
摘要： A manufacturing method for a nanocrystal light emission substance having a nano structure crystal, doped with an activator and cured with ultraviolet light. The nanocrystal light emission substance is synthesized by a liquid phase co-precipitation process. During the liquid phase reaction, an organic acid, such as acrylic acid or methacrylic acid, is added. Alternatively, a high molecular organic acid, such as polyacrylic or polymethacrylic acid, polystyrene, is added after the liquid phase reaction. The resulting substance is then cured with ultraviolet light.
摘要翻译：具有纳米结构晶体的纳米晶体发光物质的制造方法，掺杂有活化剂并用紫外光固化。通过液相共沉淀法合成纳米晶体发光物质。在液相反应期间，加入有机酸，如丙烯酸或甲基丙烯酸。或者，在液相反应之后加入高分子有机酸，例如聚丙烯酸或聚甲基丙烯酸，聚苯乙烯。然后将所得物质用紫外光固化。

6. 发明授权

US07303697B2 Phosphor and production process for the same 失效
标题翻译：磷光体和生产工艺相同
公开(公告)号：US07303697B2
公开(公告)日：2007-12-04
申请号：US11038112
申请日：2005-01-21
申请人： Tetsuhiko Isobe
发明人： Tetsuhiko Isobe
IPC分类号： C09K11/59 , C09K11/66
CPC分类号： C09K11/02 , C09K11/574 , Y02P20/544 , Y10S977/811 , Y10S977/834 , Y10T428/2991 , Y10T428/2998
摘要： The object of the present invention is to provide a phosphor which is excellent in transparency, light transmittance, luminescence efficiency and luminescent intensity and at the same time, processes for producing the phosphor. Preferred embodiments of the invention include a phosphor characterized in that phosphor particles represented by the general formula [(L)a(M)b(N)cOd:Y] are covered with an organic compound bearing at least one functional group at a terminal or side chain, wherein L is a metallic element such as Zn; M is a metallic element such as Al; N is Si or Ge; O is oxygen; Y is at least one activating agent such as Mn2+, Eu2+, Cu2+ or Yb2+; and a, b, c and d are each a value satisfying the relationships 0
摘要翻译：本发明的目的是提供透明性，透光率，发光效率和发光强度优异的荧光体，同时提供荧光体的制造方法。本发明的优选实施方案包括一种荧光体，其特征在于由通式[（L）a（M）b（N） Y]被末端或侧链具有至少一个官能团的有机化合物覆盖，其中L是诸如Zn的金属元素; M是金属元素，如Al; N是Si或Ge; O是氧; Y是至少一种活化剂，例如Mn 2+，Eu 2+，Cu 2+，或者Yb 2+， SUP>; 并且a，b，c和d分别是满足关系0

7. 发明授权

US06569396B1 Method for producing calcium phosphate powder 失效
标题翻译：磷酸钙粉末的制造方法
公开(公告)号：US06569396B1
公开(公告)日：2003-05-27
申请号：US09701193
申请日：2000-11-27
申请人： Shouhan Yanagi , Mamoru Senna , Tetsuhiko Isobe , Manabu Kanayama
发明人： Shouhan Yanagi , Mamoru Senna , Tetsuhiko Isobe , Manabu Kanayama
IPC分类号： C01B2532
CPC分类号： C01B25/32 , C01B25/324
摘要： The present invention provides a method of manufacturing calcium phosphate powder comprising the steps of preparing a mixed material by mixing calcium hydroxide (Ca(OH)2) powder and calcium hydrogenphosphate powder so that a molar ratio (Ca/P) of calcium to phosphor is set to a range of 1.45-1.72; conducting a mixing/milling treatment to the mixed material to cause a soft-mechanochemical compositing reaction thereby to prepare a calcium phosphate precursor; and conducting a heat treatment to thus obtained precursor at a temperature of 600° C. or more thereby to prepare calcium phosphate powder. According to the present invention, the manufacturing process is simple and the manufacturing cost can be remarkably reduced. In addition, fine calcium phosphate powder excellent in characteristics can be easily manufactured in a short time.
摘要翻译：本发明提供一种磷酸钙粉末的制造方法，其特征在于，通过混合氢氧化钙（Ca（OH）2）粉末和磷酸氢钙粉末，使钙与磷的摩尔比（Ca / P）为设定在1.45-1.72的范围内; 对混合材料进行混合/研磨处理以引起软化机械复合反应，从而制备磷酸钙前体; 在600℃以上的温度下进行如此得到的前体的热处理，制作磷酸钙粉末。根据本发明，制造过程简单，制造成本显着降低。另外，能够在短时间内容易地制造出特性优异的细小的磷酸钙粉末。

8. 发明授权

US06416590B1 Solder powder and method for preparing the same and solder paste 失效
标题翻译：焊粉及其制备方法及焊膏
公开(公告)号：US06416590B1
公开(公告)日：2002-07-09
申请号：US09720722
申请日：2000-12-28
申请人： Masahiko Hirata , Takashi Ohashi , Hisahiko Yoshida , Hiroji Noguchi , Takao Hisazumi , Mamoru Senna , Tetsuhiko Isobe
发明人： Masahiko Hirata , Takashi Ohashi , Hisahiko Yoshida , Hiroji Noguchi , Takao Hisazumi , Mamoru Senna , Tetsuhiko Isobe
IPC分类号： B22F102
CPC分类号： B23K35/0244 , B23K35/025 , B23K35/3618 , H05K3/3463 , H05K3/3484
摘要： An organic acid salt is deposited on the surface of a solder powder containing Sn and Zn. Alternatively, 0.5 to 10 wt. % of a nonionic surfactant is added to a flux. By a method comprising such a procedure, provided are a lead-free solder powder and solder paste having good soldering characteristics wherein the reaction of an activating component with an alloy component in a flux is suppressed.
摘要翻译：在含有Sn和Zn的焊料粉末的表面上沉积有机酸盐。或者，0.5至10wt。将％的非离子表面活性剂加入助熔剂中。通过包括这种方法的方法，提供了具有良好焊接特性的无铅焊料粉末和焊膏，其中活化组分与助熔剂中的合金组分的反应被抑制。

9. 发明申请

US20080124806A1 FLUORESCENT LABELING REAGENT 失效
标题翻译：荧光标签试剂
公开(公告)号：US20080124806A1
公开(公告)日：2008-05-29
申请号：US11678885
申请日：2007-02-26
申请人： Kunihiro Noda , Ryo Asakura , Daisuke Saito , Tetsuhiko Isobe , Tomohiro Takagi , Hideki Aizawa , Michio Ohkubo
发明人： Kunihiro Noda , Ryo Asakura , Daisuke Saito , Tetsuhiko Isobe , Tomohiro Takagi , Hideki Aizawa , Michio Ohkubo
IPC分类号： G01N37/00
CPC分类号： G01N33/582 , B82Y15/00 , G01N33/585 , G01N33/588 , Y10T436/13
摘要： A fluorescent labeling reagent of the present invention includes an inorganic fluorescent particle and a material (A) having a material (B) of biological origin adsorbed or bound thereto. The inorganic fluorescent particle is integrated with the material (A) so as to form the reagent of the present invention. The inorganic fluorescent particle used in the present invention is capable of emitting light with a wavelength of 650 nm to 1600 nm in the infrared region or the near-infrared region which can be detected by means of Si-CCD or InGaAs-PD and can penetrate an H2O rich sample when excited by light with a wavelength of 650 nm or longer which has the shortest transparent wavelength of AlInGaP-LD including oxygen adsorption type hemoglobin used for DVDs etc.
摘要翻译：本发明的荧光标记试剂包括无机荧光颗粒和具有吸附或结合生物学原料的材料（B）的材料（A）。将无机荧光颗粒与材料（A）整合以形成本发明的试剂。本发明中使用的无机荧光粒子能够通过Si-CCD或InGaAs-PD检测的红外区域或近红外区域发射波长为650nm〜1600nm的光，并能够穿透当具有波长为650nm或更长的光，其具有包括用于DVD等的氧吸附型血红蛋白的AlInGaP-LD的最短透明波长激发时，富含H 2 O 2的样品。

10. 发明申请

US20060234417A1 Composite nanoparticle and process for producing the same 失效
标题翻译：复合纳米颗粒及其制备方法
公开(公告)号：US20060234417A1
公开(公告)日：2006-10-19
申请号：US10521233
申请日：2003-07-16
申请人： Tetsuhiko Isobe , Yasushi Hattori , Shigeo Itoh , Hisamitsu Takahashi
发明人： Tetsuhiko Isobe , Yasushi Hattori , Shigeo Itoh , Hisamitsu Takahashi
IPC分类号： H01L51/40
CPC分类号： H05B33/14 , C09K11/574 , C09K11/576 , C09K11/586 , C09K11/612 , C09K11/642 , C09K11/663 , C09K11/7421 , C09K11/7703 , C09K11/7718 , C09K11/7731 , C09K11/7761 , C09K11/7786 , Y10S977/824
摘要： There is provided composite nano-particles comprising nano-crystal particles dispersed stably and individually in suspension in high concentration without mutual aggregation of the nano-particles. A determined amount of pure water or deionized water is poured into a reactor, into which is introduced nitrogen gas at rate of 300 cm3/min for a given time while agitating with a stirrer to remove dissolved oxygen in the pure water, allowing to stand in an atmosphere of nitrogen. Next, the inside of the reactor is maintained in an atmosphere of nitrogen and sodium citrate as a dispersion-stabilizing agent, an aqueous solution of MPS as a surface-modifying agent, an anion aqueous solution for co-precipitation as a nano-crystal and a cation aqueous solution are added, in that order. Then, an aqueous solution of sodium silicate is added to the reactor, which is then allowed to stand in the dark place in an atmosphere of nitrogen after agitation. At that time, a vitrification-inhibiting agent may be added in order to inhibit the growth of glass layer.
摘要翻译：提供了包含纳米晶体颗粒的复合纳米颗粒，其以高浓度稳定地和单独地分散悬浮而没有纳米颗粒的相互聚集。将一定量的纯水或去离子水倒入反应器中，其中以300cm 3 / min的速率将氮气引入给定时间，同时用搅拌器搅拌以除去溶解氧纯水，允许在氮气氛中站立。接下来，将反应器内部保持在作为分散稳定剂的氮和柠檬酸钠的气氛中，作为表面改性剂的MPS的水溶液，作为纳米晶体共沉淀的阴离子水溶液和依次加入阳离子水溶液。然后，向反应器中加入硅酸钠水溶液，然后在搅拌后在氮气气氛中在黑暗的位置放置。此时，为了抑制玻璃层的生长，可以添加玻璃化抑制剂。

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