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1. 发明授权

US4931198A Magnetic particles composed mainly of FeC and a process for preparing same 失效
标题翻译：主要由FeC组成的磁性颗粒及其制备方法
公开(公告)号：US4931198A
公开(公告)日：1990-06-05
申请号：US408955
申请日：1989-09-18
申请人： Takuya Arase , Katsushi Tokunaga , Shigeo Daimon
发明人： Takuya Arase , Katsushi Tokunaga , Shigeo Daimon
IPC分类号： H01F1/11 , B01J23/22 , C01B31/30 , G11B5/706
CPC分类号： G11B5/70626 , B01J23/22 , C01B31/303 , C01P2002/72 , C01P2002/74 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2006/42
摘要： Particles containing FeC are prepared by mixing (a) a boron compound or alkaline earth metal compound with (b) iron oxyhydroxide or iron oxide particles, or coating the former compound (a) to the latter particles (b), and then carburizing the mixture or coated particles with a carburizing agent.

2. 发明授权

US5660927A Acicular metal iron fine particles, process for preparing same, magnetic coating composition and magnetic recording medium containing same 失效
标题翻译：针状金属铁微粒，其制备方法，磁性涂料组合物和含有其的磁记录介质
公开(公告)号：US5660927A
公开(公告)日：1997-08-26
申请号：US281657
申请日：1994-07-28
申请人： Takuya Arase , Yoshiyuki Shibuya , Ikuo Kitamura , Shigeo Daimon
发明人： Takuya Arase , Yoshiyuki Shibuya , Ikuo Kitamura , Shigeo Daimon
IPC分类号： G11B5/706 , G11B5/714 , G11B5/66
CPC分类号： G11B5/70626 , G11B5/70615 , G11B5/714 , Y10S428/90 , Y10T428/256 , Y10T428/257
摘要： The present invention provides acicular fine particles made up of iron and carbon, and these acicular metal iron fine particles can be prepared by contacting acicular iron carbide fine particles with a reducing agent containing no carbon atom. Further, the present invention provides a magnetic coating composition and magnetic recording medium containing the above acicular metal iron fine particles.
摘要翻译：本发明提供由铁和碳构成的针状细颗粒，并且可以通过使针状碳化铁微粒与不含碳原子的还原剂接触来制备这些针状金属铁微粒。此外，本发明提供一种磁性涂料组合物和含有上述针状金属铁微粒的磁记录介质。

3. 发明授权

US4900464A Particles containing iron carbide 失效
标题翻译：含有碳化铁的颗粒
公开(公告)号：US4900464A
公开(公告)日：1990-02-13
申请号：US944163
申请日：1986-12-22
申请人： Takuya Arase , Yoshiyuki Shibuya , Shigeo Daimon
发明人： Takuya Arase , Yoshiyuki Shibuya , Shigeo Daimon
IPC分类号： B01J27/22 , C01B31/30 , G11B5/706
CPC分类号： B01J27/22 , C01B31/301 , G11B5/70615 , G11B5/70626 , G11B5/70642 , C01P2002/72 , C01P2002/77 , C01P2004/10 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2006/42 , C01P2006/80
摘要： The present invention provides acicular particles (A) containing an iron carbide, which have (a) a free carbon content of at most 20 wt. %, and (b) an Fe.sub.5 C.sub.2 ratio(x) of at least 70% and a coercive force of 3x+300 to 7x+270 Oe, the ratio(x) being expressed by ##EQU1## wherein S1 is the X-ray diffraction strength of Fe.sub.5 C.sub.2, and S2 is the X-ray diffraction strength of Fe.sub.3 O.sub.4. The invention further provides particles (B) containing nickel and an iron carbide. The invention further provides acicular particles containing an iron carbide which are obtained by heating an aqueous dispersion of ferric hydroxide in an alkaline system in the presence of a water-soluble compound capable of coordinating to iron to obtain acicular .alpha.-ferric oxide and contacting the product with a carbon-containing reducing-and-carburizing agent or with a mixture of the agent and a carbon-free reducing agent, with or without contacting the product with the carbon-free reducing agent. These particles (A) to (C) are controllable in coercive force and usable for magnetic record media of various standards.

4. 发明授权

US5552072A Coated acicular fine particulate materials, processes for preparing same and use thereof 失效
标题翻译：涂覆的针状细颗粒材料，其制备方法及其用途
公开(公告)号：US5552072A
公开(公告)日：1996-09-03
申请号：US318877
申请日：1994-10-18
申请人： Takuya Arase , Fumihiro Kamiya , Masayuki Tsuji , Tadashi Ino , Ikuo Kitamura , Yoshiyuki Shibuya , Shigeo Daimon
发明人： Takuya Arase , Fumihiro Kamiya , Masayuki Tsuji , Tadashi Ino , Ikuo Kitamura , Yoshiyuki Shibuya , Shigeo Daimon
IPC分类号： B22F1/00 , C01B31/30 , G11B5/706 , C04B35/00
CPC分类号： B22F1/004 , C01B31/301 , G11B5/706 , G11B5/70605 , G11B5/70615 , C01P2004/10 , C01P2004/54 , C01P2004/62 , C01P2004/80 , C01P2006/42 , C01P2006/80 , Y10T428/2991
摘要： An acicular fine particulate material which is coated with a compound containing at least one element selected from among elements of Groups III and IV of the Periodic Table in Periods 5 and 6, the acicular fine particulate material being one of (i) an acicular fine particulate material containing iron carbide, (ii) an acicular fine particulate material containing iron carbide, metallic iron and carbon, and (iii) an acicular fine particulate metallic iron containing carbon, is prepared by a promoted reduction reaction while being effectively prevented from sintering and consequently affords magnetic recording media having a high recording density.
摘要翻译： PCT No.PCT / JP94 / 00242 Sec。 371日期：1994年10月18日 102（e）日期1994年10月18日PCT 1994年2月17日PCT PCT。公开号WO94 / 19276 日期1994年9月1日针对在第5和6周期中涂覆有选自元素周期表第III和IV族元素中的至少一种元素的化合物的针状细颗粒材料，针状细颗粒材料是（i ）含有碳化铁的针状细颗粒材料，（ii）含有碳化铁，金属铁和碳的针状细颗粒材料和（iii）通过促进还原反应而有效地制备含有碳的针状细颗粒金属铁防止烧结，从而提供具有高记录密度的磁记录介质。

5. 发明授权

US5443666A Acicular fine particles containing metallic iron, iron carbide and carbon, process thereof, and magnetic coating composition and magnetic recording medium containing the same 失效
标题翻译：包含金属铁，碳化铁和碳的针状细颗粒，其工艺和磁性涂料组合物以及含有它们的磁记录介质
公开(公告)号：US5443666A
公开(公告)日：1995-08-22
申请号：US117169
申请日：1993-09-17
申请人： Ikuo Kiatamura , Takuya Arase , Fumihiro Kamiya , Shigeo Daimon
发明人： Ikuo Kiatamura , Takuya Arase , Fumihiro Kamiya , Shigeo Daimon
IPC分类号： B22F1/00 , C01B31/30 , C22C33/02 , G11B5/706 , G11B5/714 , H01F1/06 , H01F1/09 , H01F1/03
CPC分类号： C22C33/0292 , B22F1/004 , C01B31/301 , G11B5/70615 , G11B5/70626 , G11B5/714 , H01F1/065 , H01F1/09 , C01P2002/72 , C01P2004/10 , C01P2004/52 , C01P2004/62 , C01P2004/80 , C01P2006/12 , C01P2006/80
摘要： The present invention provides an acicular fine particles obtained by reducing an iron carbide starting material and containing metal iron, iron carbide and free carbon, the acicular fine particles having a mean particle size (long axis) of 0.1 to 0.5 .mu.m and an average axial ratio of 3 to 15 and containing 15 to 80 wt. % of metal iron, 10 to 75 wt. % of iron carbide and 5 to 13 wt. % of free carbon, process thereof, magnetic coating composition and magnetic recording medium containing the same.
摘要翻译： PCT No.PCT / JP93 / 00060 Sec。 371日期：1993年9月17日 102（e）1993年9月17日PCT 1993年11月20日PCT公布。公开号WO93 / 14896 日期：1993年5月8日本发明提供一种通过还原铁素体原料并含有金属铁，碳化铁和游离碳而得到的针状细粒，针状细粒的平均粒径（长轴）为0.1〜0.5 平均轴比为3〜15，含有15〜80重量％％的金属铁，10〜75wt。％的碳化铁和5〜13wt。游离碳的％，其工艺，磁性涂料组合物和含有它们的磁记录介质。

6. 发明授权

US5437805A Particles containing iron carbide 失效
标题翻译：含有碳化铁的颗粒
公开(公告)号：US5437805A
公开(公告)日：1995-08-01
申请号：US134873
申请日：1993-10-12
申请人： Takuya Arase , Yoshiyuki Shibuya , Shigeo Daimon
发明人： Takuya Arase , Yoshiyuki Shibuya , Shigeo Daimon
IPC分类号： B01J27/22 , C01B31/30 , G11B5/706
CPC分类号： B01J27/22 , C01B31/301 , G11B5/70615 , G11B5/70626 , G11B5/70642 , C01P2002/72 , C01P2002/77 , C01P2004/10 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2006/42 , C01P2006/80
摘要： The present invention provides acicular particles (A) containing an iron carbide, which have (a) a free carbon content of at most 20 wt. %, and (b) and Fe.sub.5 C.sub.2 ratio(x) of at least 70% and a coercive force of 3.times.+300 to 7.times.+270 Oe, the ratio(x) being expressed by ##EQU1## where S1 is the X-ray diffraction strength of Fe.sub.5 C.sub.2, and S2 is the X-ray diffraction strength of Fe.sub.3 O.sub.4.The invention further provides particles (B) containing nickel and an iron carbide.The invention further provides acicular particles containing an iron carbide which are obtained by heating an aqueous dispersion of ferric hydroxide in an alkaline system in the presence of a water-soluble compound capable of coordinating to iron to obtain acicular .alpha.-ferric oxide and contacting the product with a carbon-containing reducing-and-carburizing agent or with a mixture of the agent and a carbon-free reducing agent, with or without contacting the product with the carbon-free reducing agent.These particles (A) and (C) are controllable in coercive force and usable for magnetic record media of various standards.
摘要翻译：本发明提供了含有碳化铁的针状粒子（A），其具有（a）游离碳含量至多为20重量％％，（b）和Fe5C2比（x）至少为70％，矫顽力为3x + 300〜7×270ee，比例（x）由表示，其中S1为X射线衍射 Fe5C2的强度，S2是Fe3O4的X射线衍射强度。本发明还提供含有镍和碳化铁的颗粒（B）。本发明还提供了含有碳化铁的针状颗粒，其通过在碱性体系中在能够与铁配位的水溶性化合物的存在下加热氢氧化铁的水分散体而获得，得到针状的α-氧化铁并与产物接触与含碳还原和渗碳剂或与该试剂和不含碳的还原剂的混合物，与或不使该产物与无碳还原剂接触。这些颗粒（A）和（C）在矫顽力方面是可控的，可用于各种标准的磁记录介质。

7. 发明授权

US07321071B2 Process for the production of water-soluble fluorine-containing vinyl ethers 有权
标题翻译：生产水溶性含氟乙烯基醚的方法
公开(公告)号：US07321071B2
公开(公告)日：2008-01-22
申请号：US10517667
申请日：2003-06-16
申请人： Kenji Ishii , Noriyuki Shinoki , Takuya Arase , Kazuyoshi Ichihara , Toshiya Mantani
发明人： Kenji Ishii , Noriyuki Shinoki , Takuya Arase , Kazuyoshi Ichihara , Toshiya Mantani
IPC分类号： C07C17/00 , C07C17/25
CPC分类号： C07C303/22 , C07C309/10
摘要： The present invention relates to a method for producing a water-soluble fluorine-containing vinyl ether which comprises subjecting a fluorine-containing 2-alkoxypropionic acid derivative represented by the following general formula (I): (wherein A represents —OM1 or —OM21/2, and M1 represents an alkali metal and M2 represents an alkaline earth metal; X represents a halogen atom; Y1 and Y2 are the same or different and each represents a fluorine atom, a chlorine atom, a perfluoroalkyl group or a fluorochloroalkyl group; n represents an integer of 0 to 3, and n of Y1s may be the same or different; m represents an integer of 1 to 5, and m of Y2s are the same or different; and Z represents a hydrophilic group) to thermal decomposition at a temperature of not lower than 50° C. but lower than 170° C. in the presence of a coordinating organic solvent to give a water-soluble fluorine-containing vinyl ether represented by the general formula (II): (wherein Y1, Y2, Z, n and m are as defined above), said coordinating organic solvent having a coordinating property with an ion of said M1 or an ion of said M2 said coordinating organic solvent being in an amount of 10 to 1,000 parts by mass per 100 parts by mass of the fluorine-containing 2-alkoxypropionic acid derivative.
摘要翻译：本发明涉及一种水溶性含氟乙烯醚的制造方法，其特征在于，将下述通式（I）表示的含氟2-烷氧基丙酸衍生物：（式中，A表示-OM1 或或-OM 2 1/2，M 1表示碱金属和M 2 表示碱土金属; X表示卤素原子; Y 1和Y 2相同或不同，表示氟原子，氯原子，全氟烷基或氟氯烷基; n表示0〜3的整数，Y 1的n可以相同或不同，m表示1〜5的整数，y表示0〜 2个相同或不同; Z表示亲水基团）在不低于50℃但低于170℃的温度下在配位有机溶剂的存在下进行热分解，得到水溶性含氟由通式（II）表示的乙烯基醚：其中Y 1，Y 2，Z，n和m如上所定义），所述配位有机溶剂具有与所述M 1的离子或所述M 2的所述配位有机溶剂的离子的配位性为每100质量份为10〜1000质量份的含氟2-烷氧基丙酸衍生物。

8. 发明申请

US20060194703A1 Liquid fluoropolymer composition, process for producing organosol, film, and fuel cell 审中-公开
标题翻译：液体含氟聚合物组合物，生产有机溶胶，薄膜和燃料电池的方法
公开(公告)号：US20060194703A1
公开(公告)日：2006-08-31
申请号：US10547770
申请日：2004-03-03
申请人： Masayoshi Tatemoto , Tadashi Ino , Takuya Arase , Atsushi Sakakura
发明人： Masayoshi Tatemoto , Tadashi Ino , Takuya Arase , Atsushi Sakakura
IPC分类号： C10M107/38
CPC分类号： C08F8/00 , C08J3/09 , C08J5/2237 , C08J2327/12 , C08K5/00 , C09D127/12 , H01M8/1023 , H01M8/1039 , H01M8/1058 , H01M8/1081 , Y02P70/56 , C08F14/18
摘要： The invention provides a fluoropolymer liquid composition comprising a fluoropolymer and a film-forming auxiliary, said fluoropolymer comprising acid/acid salt fluorovinyl ether units represented by the general formula (I): said film-forming auxiliary being an organic liquid which is compatible with water and has a boiling point higher than 100° C. but not higher than 300° C., said fluoropolymer liquid composition being a fluoropolymer dispersion composition comprising said film-forming auxiliary and a fluoropolymer fine particle comprising said fluoropolymer, said fluoropolymer fine particle containing, at the proportion of at least 25% by mass thereof, a spherical fluoropolymer fine particle, and said spherical fluoropolymer fine particle being substantially spherical.
摘要翻译：本发明提供含氟聚合物和成膜助剂的含氟聚合物液体组合物，所述含氟聚合物包含由通式（I）表示的酸/酸盐氟乙烯基醚单元：所述成膜助剂是与水相容的有机液体并且具有高于100℃但不高于300℃的沸点，所述含氟聚合物液体组合物是包含所述成膜助剂和包含所述含氟聚合物的含氟聚合物细颗粒的含氟聚合物分散体组合物，所述含氟聚合物细颗粒含有其比例为至少25质量％，球状含氟聚合物细颗粒，并且所述球形含氟聚合物细颗粒基本上为球形。

9. 发明申请

US20050228127A1 Fluoropolymer dispersion and process for producing fluoropolymer dispersion 审中-公开
标题翻译：含氟聚合物分散体和生产含氟聚合物分散体的方法
公开(公告)号：US20050228127A1
公开(公告)日：2005-10-13
申请号：US10518052
申请日：2003-06-16
申请人： Masayoshi Tatemoto , Takuya Arase , Tadashi Ino
发明人： Masayoshi Tatemoto , Takuya Arase , Tadashi Ino
IPC分类号： B01D67/00 , B01D69/10 , B01D69/12 , B01D69/14 , B01D71/32 , B01D71/82 , C08F6/00 , C08F6/14 , C08F6/16 , C08F8/00 , C08K3/00 , C08L27/12
CPC分类号： C08F2/10 , B01D67/0009 , B01D67/0011 , B01D69/10 , B01D69/12 , B01D69/141 , B01D71/32 , B01D71/82 , B01D2323/06 , B01D2323/46 , B01D2325/10 , B01D2325/14 , B01D2325/42 , C08F6/003 , C08F6/14 , C08F8/44 , C08F2800/10 , H01M8/1004 , H01M8/1025 , H01M8/1039 , H01M8/1072 , H01M2300/0082 , Y02E60/522 , Y02E60/523 , Y02P70/56 , C08L27/12 , C08F8/12 , C08F214/262
摘要： A fluoropolymer solid composition which contains a fine particle comprising a fluoropolymer, said fluoropolymer having an acid/acid salt group, said acid/acid salt group being a sulfonic acid group, —SO2NR17R18, a carboxyl group, —SO3NR1R2R3R4, —SO3M11/L, —COONR5R6R7R8 or —COOM21/L (in which R17 and R18 are the same or different and each represents a hydrogen atom, an alkali metal, an alkyl group or a sulfonyl-containing group, R1, R2, R3 and R4 are the same or different and each represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, R5, R6, R7 and R8 are the same or different and each represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, M1 and M2 are the same or different and each represents a metal whose valence is L, and said metal whose valence is L is a metal belonging to the group 1, 2, 4, 8, 11, 12 or 13 of the periodic table); said fine particle comprising the fluoropolymer containing, at the proportion of at least 25% by mass thereof, a spherical fluoropolymer fine particle, and said spherical fluoropolymer fine particle being substantially spherical.
摘要翻译：一种含氟聚合物固体组合物，其含有包含含氟聚合物的细颗粒，所述含氟聚合物具有酸/酸盐基团，所述酸/酸盐基团是磺酸基，-SO 2 NR 17 羧基，-SO 3，NR 1，R 2，R 2，R 2， 3/4，3/3，1 / L，-COONR＆lt; 3＆gt; 5 6 /其中R 17和R 18相同或不同，各自表示氢原子，碱金属，烷基或含磺酰基的基团 R 1，R 2，R 3和R 4相同或不同，并且各自表示氢原子或碳原子数1〜4的烷基，R 5，R 6，R 7，R 8， >相同或不同，各自表示氢原子或碳原子数1〜4的烷基，M 1和M 2 2价元素相同或不同，分别表示价数为L的金属，所述金属价为L的是金属属于第1,2,4,8,11,12或13族金属的周期表）; 所述含有氟聚合物的微粒子以至少25质量％的比例含有球状含氟聚合物细粒，所述球状含氟聚合物微粒基本上为球形。

10. 发明授权

US06740375B1 Fluorochemical adhesive material and laminate comprising the same 有权
标题翻译：含氟化合物粘合剂材料和包含其的层合物
公开(公告)号：US06740375B1
公开(公告)日：2004-05-25
申请号：US10070669
申请日：2002-05-08
申请人： Shigehito Sagisaka , Taketo Kato , Takeshi Inaba , Takuya Arase , Tetsuo Shimizu
发明人： Shigehito Sagisaka , Taketo Kato , Takeshi Inaba , Takuya Arase , Tetsuo Shimizu
IPC分类号： B32B2730
CPC分类号： B32B27/08 , B29C47/0021 , B29C47/06 , B29K2027/12 , B32B1/02 , B32B1/08 , B32B7/12 , B32B27/304 , B32B27/306 , B32B27/308 , B32B27/32 , B32B27/34 , B32B27/36 , B32B27/365 , B32B2329/04 , B32B2331/04 , B32B2367/00 , B32B2369/00 , C09J127/12 , C09J127/18 , Y10T428/1352 , Y10T428/31536 , Y10T428/3154 , Y10T428/31544
摘要： A fluorine-containing adhesive material comprising a fluorine-containing ethylenic polymer having a carbonate group and/or a carboxylic acid halide group at a chain end or a side chain of the polymer, wherein a total of a number of the carbonate groups and/or carboxylic acid halide groups is at less than 150 per 1×106 main chain carbon atoms, can directly impart the firm adherability to a substrate such as a metal, a glass or a resin while maintaining excellent properties such as chemical resistance, solvent resistance, weatherability and soil releasability possessed by a fluorine-containing polymer.
摘要翻译：一种含氟粘合剂材料，其包含在聚合物的链端或侧链上具有碳酸酯基和/或羧酸卤化物基团的含氟乙烯性聚合物，其中总共多个碳酸酯基和/或羧酸卤化物基团每1×10 6主链碳原子小于150，可以直接赋予基材如金属，玻璃或树脂牢固的粘合性，同时保持优异的性能如耐化学性，耐溶剂性，含氟聚合物具有的耐候性和土壤释放性。

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