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1. 发明授权

US06177030B1 Stimulable phosphor and radiation image conversion panel by use thereof 失效
标题翻译：可刺激的荧光体和辐射图像转换面板
公开(公告)号：US06177030B1
公开(公告)日：2001-01-23
申请号：US09294937
申请日：1999-04-19
申请人： Takehiko Shoji , Satoshi Honda , Manabu Watanabe , Masaaki Murayama , Yasushi Nakano , Haruhiko Masutomi , Hideaki Wakamatsu , Hiroyuki Nabeta , Kanae Kawabata
发明人： Takehiko Shoji , Satoshi Honda , Manabu Watanabe , Masaaki Murayama , Yasushi Nakano , Haruhiko Masutomi , Hideaki Wakamatsu , Hiroyuki Nabeta , Kanae Kawabata
IPC分类号： C09K1161
CPC分类号： C09K11/025 , C09K11/7705 , G21K4/00 , G21K2004/06 , G21K2004/10
摘要： A method for preparing a stimulable phosphor is disclosed, comprising forming a stimulable phosphor and coating the formed stimulable phosphor with a metal oxide and a silane coupling agent, or a metal oxide and a metal alkoxide. Another method is also disclosed, comprising forming a stimulable phosphor precursor, calcining the formed precursor in the presence of a metal oxide or metal alkoxide, and coating the calcined precursor with a silane coupling agent or metal alkoxide. Further disclosed is a preparation method of a radiation image conversion panel containing the stimulable phosphor.
摘要翻译：公开了一种制备可刺激的荧光体的方法，包括形成可刺激的荧光体并用金属氧化物和硅烷偶联剂或金属氧化物和金属醇盐涂覆形成的可刺激的荧光体。还公开了另一种方法，包括形成可刺激的荧光体前体，在金属氧化物或金属醇盐的存在下煅烧所形成的前体，并用硅烷偶联剂或金属醇盐涂覆煅烧的前体。进一步公开了包含可刺激荧光体的放射线图像转换面板的制备方法。

2. 发明授权

US06168730A Stimulable phosphor, preparation method thereof and radiation image conversion panel 失效
标题翻译：稳定荧光粉，其制备方法和辐射图像转换面板
公开(公告)号：US06168730A
公开(公告)日：2001-01-02
申请号：US09291459
申请日：1999-04-14
申请人： Hiroyuki Nabeta , Kanae Kawabata , Hideaki Wakamatsu , Haruhiko Masutomi
发明人： Hiroyuki Nabeta , Kanae Kawabata , Hideaki Wakamatsu , Haruhiko Masutomi
IPC分类号： C09K1161
CPC分类号： C09K11/7703 , C09K11/7705
摘要： A preparation method of an oxygen-introduced stimulable phosphor including a rare earth activated alkaline earth metal fluorohalide stimulable phosphor is disclosed, comprising the steps of heating a precursor of a stimulable phosphor in an atmosphere containing oxygen, and further heating the heated precursor in a weakly reducing atmosphere. Stimulable phosphors prepared by this method and a radiation image conversion panel by use thereof are also disclosed.
摘要翻译：公开了包含稀土活化的碱土金属氟卤化物可激发荧光体的引入氧的荧光体的制备方法，其包括在含氧的气氛中加热可刺激的荧光体的前体，并进一步加热弱的前体减少气氛。还公开了通过该方法制备的稳定的荧光体和其使用的辐射图像转换面板。

3. 发明授权

US06638447B2 Preparation method of rare earth activated alkaline earth metal fluorohalide stimulable phosphor and radiographic image conversion panel 失效
公开(公告)号：US06638447B2
公开(公告)日：2003-10-28
申请号：US09838856
申请日：2001-04-20
申请人： Hideaki Wakamatsu , Hiroto Itoh , Hiroyuki Nabeta , Kanae Kawabata
发明人： Hideaki Wakamatsu , Hiroto Itoh , Hiroyuki Nabeta , Kanae Kawabata
IPC分类号： C09K1161
CPC分类号： C01F17/0012 , C01F17/0031 , C01P2002/52 , C01P2004/61 , C09K11/7705
摘要： A preparation method of an oxygen-introduced rare earth activated alkaline earth metal fluorohalide stimulable phosphor is disclosed, comprising (a) preparing a reactant solution having a barium concentration of not less than 3.3 mol/l in a reaction vessel, (b) forming a precursor of the stimulable phosphor, and (c) removing a solvent from a mother liquor.

4. 发明申请

US20090121140A1 HALIDE-CONTAINING STIMULABLE PHOSPHOR PRECURSOR, HALIDE-CONTAINING STIMULABLE PHOSPHOR, RADIATION IMAGE CONVERSION PANEL AND PRODUCTION METHOD THEREOF 审中-公开
标题翻译：含卤素的可刺激的磷酸盐前体，含卤素的可刺激的磷，辐射图像转换面板及其生产方法
公开(公告)号：US20090121140A1
公开(公告)日：2009-05-14
申请号：US11994545
申请日：2006-07-13
申请人： Akihiro Maezawa , Satoshi Honda , Hideaki Wakamatsu , Hiroyuki Nabeta
发明人： Akihiro Maezawa , Satoshi Honda , Hideaki Wakamatsu , Hiroyuki Nabeta
IPC分类号： C09K11/61 , G01F23/00 , C09K11/00 , C09K11/08 , G21K4/00
CPC分类号： G21K4/00 , C01F11/20 , C01P2002/52 , C01P2004/30 , C01P2004/38 , C01P2004/39 , C01P2004/41 , C01P2004/52 , C01P2004/54 , C01P2004/61 , C01P2006/60 , C09K11/7733
摘要： This invention relates to a halide-containing stimulable phosphor having improved moisture resistance and luminance, and a process for producing the same. The halide-containing stimulable phosphor is characterized in that, among elements constituting the outermost surface and inside of the phosphor, there is a difference in composition ratio of a halogen element between the outermost surface and the inside of the phosphor. A radiation image conversion panel, which has been improved, for example, in moisture resistance, luminance and image quality by using the phosphor, and a process for producing the same are also provided.
摘要翻译：本发明涉及具有改善的耐湿性和亮度的含卤素的可激发的荧光体及其制造方法。含卤素的可激发性荧光体的特征在于，在构成荧光体的最外表面和内部的元素中，荧光体的最外表面和内部之间的卤素元素的组成比存在差异。还提供了通过使用荧光体而改进了例如耐湿性，亮度和图像质量的辐射图像转换面板及其制造方法。

5. 发明申请

US20060175577A1 Preparation method of rare earth activated alkaline earth metal fluorohalide stimulable phosphor precursor, rare earth activated alkaline earth metal fluorohalide stimulable phosphor and radiographic image conversion panel 失效
标题翻译：稀土活化碱土金属氟卤化物可激发荧光体前体，稀土活化碱土金属氟卤化物可激发荧光粉和射线照相图像转换面板的制备方法
公开(公告)号：US20060175577A1
公开(公告)日：2006-08-10
申请号：US11342543
申请日：2006-01-31
申请人： Hideaki Wakamatsu , Hiroyuki Nabeta
发明人： Hideaki Wakamatsu , Hiroyuki Nabeta
IPC分类号： C09K11/61
CPC分类号： C09K11/7733
摘要： A preparation method of a precursor of a rare earth activated alkaline earth metal fluorohalide stimulable phosphor is disclosed, comprising (A) adding an aqueous solution of an inorganic fluoride into a mother liquor containing a barium halide to form a reaction mixture containing a precipitate of a precursor of the stimulable phosphor, and (B) removing a solvent from the reaction mixture to obtain a concentrated reaction mixture, wherein the steps (A) and (B) are concurrently performed over periods of a and b, respectively, and meeting the following requirement: 0.25
摘要翻译：公开了一种稀土活化的碱土金属氟卤化物可激发荧光体的前体的制备方法，其包括（A）将无机氟化物的水溶液加入到含有卤化钡的母液中以形成含有（B）从反应混合物中除去溶剂，得到浓缩的反应混合物，其中步骤（A）和（B）分别同时进行a和b的时间段，并满足以下步骤要求：<？in-line-formula description =“In-line Formulas”end =“lead”？> 0.25 还公开了可刺激荧光体的制备方法和使用可激发荧光体的放射线图像转换面板。

6. 发明授权

US07422705B2 Preparation method of rare earth activated alkaline earth metal fluorohalide stimulable phosphor precursor, rare earth activated alkaline earth metal fluorohalide stimulable phosphor and radiographic image conversion panel 失效
标题翻译：稀土活化碱土金属氟卤化物可激发荧光体前体，稀土活化碱土金属氟卤化物可激发荧光粉和射线照相图像转换面板的制备方法
公开(公告)号：US07422705B2
公开(公告)日：2008-09-09
申请号：US11342543
申请日：2006-01-31
申请人： Hideaki Wakamatsu , Hiroyuki Nabeta
发明人： Hideaki Wakamatsu , Hiroyuki Nabeta
IPC分类号： C09K11/61 , C09K11/55
CPC分类号： C09K11/7733
摘要： A preparation method of a precursor of a rare earth activated alkaline earth metal fluorohalide stimulable phosphor is disclosed, comprising (A) adding an aqueous solution of an inorganic fluoride into a mother liquor containing a barium halide to form a reaction mixture containing a precipitate of a precursor of the stimulable phosphor, and (B) removing a solvent from the reaction mixture to obtain a concentrated reaction mixture, wherein the steps (A) and (B) are concurrently performed over periods of a and b, respectively, and meeting the following requirement: 0.25
摘要翻译：公开了一种稀土活化的碱土金属氟卤化物可激发荧光体的前体的制备方法，其包括（A）将无机氟化物的水溶液加入到含有卤化钡的母液中以形成含有（B）从反应混合物中除去溶剂，得到浓缩的反应混合物，其中步骤（A）和（B）分别同时进行a和b的时间段，并满足以下步骤要求：<？in-line-formula description =“In-line formula”end =“lead”？> 0.25 还公开了可刺激荧光体的制备方法和使用可激发荧光体的辐射图像转换面板。

7. 发明申请

US20060108565A1 Manufacturing process of rare earth activated alkaline earth metal fluorohalide stimulable phosphor 审中-公开
标题翻译：稀土活化碱土金属氟卤素可激发荧光粉的制造工艺
公开(公告)号：US20060108565A1
公开(公告)日：2006-05-25
申请号：US11281038
申请日：2005-11-17
申请人： Hideaki Wakamatsu , Hiroyuki Nabeta
发明人： Hideaki Wakamatsu , Hiroyuki Nabeta
IPC分类号： C09K11/61
CPC分类号： C09K11/7733
摘要： Provided is a manufacturing process of a rare earth activated alkaline earth metal fluorohalide stimulable phosphor exhibiting improved productivity accompanied with an X-ray resistance property against repeating use upon X-ray exposure. Also disclosed is a liquid phase manufacturing process of a rare earth activated alkaline earth metal fluorohalide stimulable phosphor represented in following Formula (1) possessing the steps of adding an aqueous solution containing inorganic fluoride into a reaction mother liquor in which barium halide is dissolved at a reaction temperature of 85-100° C., to form a crystalline precipitate of a precursor of a rare earth activated alkaline earth metal fluorohalide stimulable phosphor, and removing a solvent from the reaction mother liquor, wherein a precursor of a stimulable phosphor is prepared via the foregoing steps conducted in parallel. Ba(1-x)M2(x)FBr(y)I(1-y):aM1, bLn, cO Formula (I)
摘要翻译：提供了一种稀土活化的碱土金属氟卤化物可刺激荧光体的制造方法，其具有在X射线曝光时反复使用的X射线电阻性能的提高的生产率。还公开了下述式（1）所示的稀土类活化碱土金属氟卤化物可刺激性荧光体的液相制造方法，具有以下步骤：将含有无机氟化物的水溶液加入到其中溶解有卤化钡的反应母液中反应温度为85-100℃，以形成稀土活化的碱土金属氟卤化物可刺激磷光体的前体的结晶沉淀物，并从反应母液中除去溶剂，其中可刺激磷光体的前体通过上述步骤并行进行。（1-x）<2>（x）在线公式描述=“在线公式”end =“lead” （1）y（1-y）：aM 1，bLn，c 0式（I）<α line-formula description =“In-line Formulas”end =“tail”？>

8. 发明申请

US20100155738A1 Light Emitting Diode and Method for Manufacturing Same 审中-公开
标题翻译：发光二极管及其制造方法相同
公开(公告)号：US20100155738A1
公开(公告)日：2010-06-24
申请号：US11884398
申请日：2006-02-06
申请人： Hiroyuki Nabeta , Hideaki Wakamatsu
发明人： Hiroyuki Nabeta , Hideaki Wakamatsu
IPC分类号： H01L33/00
CPC分类号： H01L33/42 , H01L33/32
摘要： This invention provides a light emitting diode in which a thick transparent conductive electrode is formed on an emitting side of GaN based semiconductor light emitting element, and a light emitting efficiency of the GaN semiconductor light emitting element is improved. Further, it provides a manufacturing method of the light emitting diode by which a thick transparent electrode film of the light emitting diode is effectively formed. A light emitting diode which emits light in a blue or an ultraviolet region comprising a substrate and a light emitting layer thereon comprising at least an n-type GaN based semiconductor layer, a p-type GaN based semiconductor layer, and a GaN based semiconductor sandwiched between them, wherein a transparent conductive film having a thickness of 1-100 μm is provided on the light emitting layer.
摘要翻译：本发明提供了一种发光二极管，其中在GaN基半导体发光元件的发射侧形成厚的透明导电电极，并提高了GaN半导体发光元件的发光效率。此外，它提供了一种发光二极管的制造方法，通过该方法可以有效地形成发光二极管的厚的透明电极膜。发射蓝色或紫外线区域的发光二极管，其包括基板及其上的发光层，所述发光二极管至少包括n型GaN基半导体层，p型GaN基半导体层和夹在中间的GaN基半导体层在它们之间，其中在发光层上设置有厚度为1-100μm的透明导电膜。

9. 发明授权

US07592192B2 White light emitting diode (white LED) and method of manufacturing white LED 失效
标题翻译：白光发光二极管（白光LED）及制造白光LED的方法
公开(公告)号：US07592192B2
公开(公告)日：2009-09-22
申请号：US10590589
申请日：2005-02-24
申请人： Hiroyuki Nabeta , Hideaki Wakamatsu
发明人： Hiroyuki Nabeta , Hideaki Wakamatsu
IPC分类号： H01L21/20
CPC分类号： H01L33/501 , C09K11/7774 , H01L2933/0041 , Y02B20/181
摘要： Disclosed is a white light emitting diode possessing a phosphor layer to convert blue light into yellow light, provided on a blue light emitting diode, wherein the phosphor layer possesses an inorganic compound containing a phosphor, and particularly a white light emitting diode, wherein this inorganic compound is a phosphor. Also disclosed is a method of manufacturing a white light emitting diode, possessing a step of forming the foregoing phosphor layer made of an inorganic compound containing a phosphor via an aerosol deposition method. A white light emitting diode exhibiting high reliability and longer operating life, which is prepared via use of a blue LED element, can be provided by what is described above.
摘要翻译：公开了一种白色发光二极管，其具有将蓝色光转换成黄色光的荧光体层，设置在蓝色发光二极管上，其中荧光体层具有含有荧光体的无机化合物，特别是白色发光二极管，其中该无机化合物是磷光体。还公开了一种制造白色发光二极管的方法，具有通过气溶胶沉积法形成由含有荧光体的无机化合物制成的上述荧光体层的步骤。通过使用蓝色LED元件制备的显示高可靠性和较长使用寿命的白色发光二极管可以通过上述方式提供。

10. 发明申请

US20070176194A1 White light emitting diode and method of manufcturing the same 有权
标题翻译：白光发光二极管及其制作方法
公开(公告)号：US20070176194A1
公开(公告)日：2007-08-02
申请号：US11570952
申请日：2005-06-10
申请人： Hideaki Wakamatsu , Hiroyuki Nabeta
发明人： Hideaki Wakamatsu , Hiroyuki Nabeta
IPC分类号： H01L33/00
CPC分类号： H01L33/501 , H01L2933/0041
摘要： Employing a LED which emits light via excitation with UV light, particularly the foregoing high-power LED, disclosed are a white LED exhibiting high reliability and longer operating life, and a method of manufacturing the white LED. Also disclosed are a white light emitting diode possessing a phosphor layer which emits light via excitation with UV light, wherein the phosphor layer consists of phosphor, or possesses phosphor and transparent inorganic oxide, and a method of manufacturing the white light emitting diode, possessing the step of making phosphor particles to collide with a light emitting diode at high speed to deposit the phosphor layer, employing an aerosol deposition process.
摘要翻译：采用通过紫外光激发发光的LED，特别是上述大功率LED，公开了一种白色LED，其具有高可靠性和较长的使用寿命，以及一种制造白光LED的方法。还公开了一种白光发光二极管，其具有通过紫外光激发而发光的荧光体层，其中荧光体层由磷光体构成或具有荧光体和透明无机氧化物，以及制造白色发光二极管的方法，使用气溶胶沉积工艺使荧光体颗粒与发光二极管高速碰撞以沉积磷光体层的步骤。

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