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1. 发明申请

US20090215918A1 PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM 失效
标题翻译：生产柔性聚氨酯泡沫的方法
公开(公告)号：US20090215918A1
公开(公告)日：2009-08-27
申请号：US12429762
申请日：2009-04-24
申请人： Takayuki SASAKI , Daisuke Kaku , Takashi Ito , Naohiro Kumagai
发明人： Takayuki SASAKI , Daisuke Kaku , Takashi Ito , Naohiro Kumagai
IPC分类号： C08G18/08
CPC分类号： C08G18/283 , C08G18/4812 , C08G2101/0008 , C08G2101/0058 , C08G2101/0083
摘要： To provide a flexible polyurethane foam which is excellent in low resiliency and durability without using a plasticizer and which shows little change in hardness against a change in temperature and at the same time, has high air flow.A process for producing a flexible polyurethane foam, which comprises reacting a polyol mixture comprising the following polyol (A), the following polyol (B) and the following monool (D) with a polyisocyanate compound in the presence of a blowing agent and a foam stabilizer, at an isocyanate index of at least 90, wherein: Polyol (A) is a polyether polyol having an average of from 2 to 3 hydroxyl groups, a hydroxyl value of from 10 to 60 mgKOH/g and an oxyethylene group content of from 0 to 30 mass %, obtained by ring-opening polymerization of an alkylene oxide to an initiator using a phosphazene compound, a Lewis acid compound or an alkali metal compound catalyst; Polyol (B) is a polyether polyol having an average of from 2 to 3 hydroxyl groups and a hydroxyl value of from 70 to 250 mgKOH/g; and Monool (D) is a polyether monool having a hydroxyl value of from 10 to 200 mgKOH/g.
摘要翻译：为了提供在不使用增塑剂的情况下具有优异的低弹性和耐久性的柔性聚氨酯泡沫，并且硬度相对于温度变化几乎没有变化，并且同时具有高气流。一种软质聚氨酯泡沫塑料的制造方法，其特征在于，在发泡剂和泡沫体的存在下，使含有下述多元醇（A）的多元醇混合物，下述多元醇（B）和下述一元醇（D）与多异氰酸酯化合物反应稳定剂，异氰酸酯指数至少为90，其中：多元醇（A）是平均具有2至3个羟基的聚醚多元醇，羟值为10至60mgKOH / g，氧化乙烯基含量为 0〜30质量％，使用磷腈化合物，路易斯酸化合物或碱金属化合物催化剂通过烯化氧与引发剂的开环聚合得到的; 多元醇（B）是平均2〜3个羟基，羟值为70〜250mgKOH / g的聚醚多元醇; 单醇（D）是羟值为10〜200mgKOH / g的聚醚一元醇。

2. 发明申请

US20080081847A1 FLEXIBLE POLYURETHANE FOAM, PROCESS FOR ITS PRODUCTION, AND SEAT FOR AUTOMOBILE USING THE FLEXIBLE POLYURETHANE FOAM 有权
标题翻译：柔性聚氨酯泡沫，其生产工艺及使用柔性聚氨酯泡沫的汽车座椅
公开(公告)号：US20080081847A1
公开(公告)日：2008-04-03
申请号：US11944730
申请日：2007-11-26
申请人： Takayuki SASAKI , Takashi Ito , Yoshinori Toyota , Naohiro Kumagai
发明人： Takayuki SASAKI , Takashi Ito , Yoshinori Toyota , Naohiro Kumagai
IPC分类号： C08G18/06
CPC分类号： C08G18/61 , C08G18/3203 , C08G18/3275 , C08G18/4072 , C08G18/4866 , C08G18/632 , C08G18/7607 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08G2350/00
摘要： To provide a flexible polyurethane foam having good vibration characteristics and suitable particularly for a seat for an automobile. A flexible polyurethane foam obtained by reacting a high molecular weight polyoxyalkylene polyol or a polymer-dispersed polyol containing fine polymer particles in the high molecular weight polyoxyalkylene polyol, with a polyisocyanate compound, in the presence of a catalyst, a blowing agent and a foam stabilizer, characterized in that an amino-modified silicone (F) having a silicon atom and a nitrogen atom in its molecule is used in an amount of from 0.00001 to 1 part by mass per 100 parts by mass of all active hydrogen compounds.
摘要翻译：提供具有良好振动特性的柔性聚氨酯泡沫，特别适用于汽车座椅。通过使高分子量聚氧化烯多元醇或含有高分子量聚氧化烯多元醇中的聚合物微粒的聚合物分散多元醇与多异氰酸酯化合物在催化剂，发泡剂和泡沫稳定剂的存在下反应而获得的软质聚氨酯泡沫体其特征在于，相对于100质量份的所有活性氢化合物，其分子中具有硅原子和氮原子的氨基改性硅酮（F）的使用量为0.00001〜1质量份。

3. 发明申请

US20090270520A1 PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM 审中-公开
标题翻译：生产柔性聚氨酯泡沫的方法
公开(公告)号：US20090270520A1
公开(公告)日：2009-10-29
申请号：US12486790
申请日：2009-06-18
申请人： Takayuki SASAKI , Naohiro KUMAGAI
发明人： Takayuki SASAKI , Naohiro KUMAGAI
IPC分类号： C08J9/00
CPC分类号： C08G18/4288 , C08G2101/0008 , C08G2350/00 , C08J9/12 , C08J2205/06 , C08J2375/04
摘要： To produce a flexible polyurethane foam molded product having good air flow and cushioning characteristic and having cell roughening at the skin portion suppressed by using a raw material derived from a natural fat/oil.A release agent (X) containing a first polysiloxane compound (S1) having a number average molecular weight of at least 1,200 and at most 40,000, in which an organic group having an alkylene oxide chain is bonded to some of silicon atoms constituting the polysiloxane chain, is adhered to the inner surface of a mold, and in the mold, a reactive mixture (Y) containing a polyol (A) containing a polyol (A1) derived from a vegetable fat/oil, a polyisocyanate compound (B) and a silicone foam stabilizer (S) which is a second polysiloxane compound (S2) having a number average molecular weight of at least 150 and less than 1,200 is subjected to mold-foaming.
摘要翻译：为了制造具有良好的气流和缓冲特性的柔性聚氨酯泡沫塑料模制产品，并且通过使用衍生自天然油脂的原料抑制皮肤部分的细胞粗糙化。含有数均分子量为1,200以上至40,000的第一聚硅氧烷化合物（S1）的脱模剂（X），其中具有烯化氧链的有机基团与构成聚硅氧烷链的一些硅原子键合粘合到模具的内表面，在模具中，含有含有来源于植物油脂的多元醇（A1）的多元醇（A），多异氰酸酯化合物（B）和作为数均分子量为150以上且小于1,200的第二聚硅氧烷化合物（S2）的硅氧烷泡沫稳定剂（S）经受模塑发泡。

4. 发明申请

US20120252916A1 PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM AND SEAT 审中-公开
标题翻译：生产柔性聚氨酯泡沫和座椅的方法
公开(公告)号：US20120252916A1
公开(公告)日：2012-10-04
申请号：US13438460
申请日：2012-04-03
申请人： Takayuki SASAKI , Naohiro Kumagai , Chitoshi Suzuki , Masahito Furumi
发明人： Takayuki SASAKI , Naohiro Kumagai , Chitoshi Suzuki , Masahito Furumi
IPC分类号： C08G71/04 , C08J9/00
CPC分类号： C08G18/4866 , C08G18/4825 , C08G18/4833 , C08G65/2663 , C08G2101/0008
摘要： A process for producing a flexible polyurethane foam excellent in mechanical strength, and exhibiting reduced shrinkage. The foam is produced using a polyol (A) containing from 40 to 100 mass % of a polyoxyalkylene polyol (A1). The polyoxyalkylene polyol (A1) is produced through an initial step of adding, to a reaction liquid containing an initiator and a double metal cyanide complex catalyst, 5 to 20 mass % of an alkylene oxide, based on the content of the initiator. After the initial step, an alkylene oxide is newly supplied to carry out polymerization. In the initial step, the temperature of the reaction system when addition of the alkylene oxide is started is from 120 to 165° C., and the maximum temperature of the reaction system after the alkylene oxide has been added in the initial step is higher by 15 to 50° C. than the temperature when addition of the alkylene oxide was started.
摘要翻译：一种制造机械强度优异且缩小收缩率低的柔性聚氨酯泡沫的方法。使用含有40〜100质量％聚氧化烯多元醇（A1）的多元醇（A）制造泡沫体。基于引发剂的含量，通过向包含引发剂和双金属氰化物配合物催化剂的反应液中添加5〜20质量％的烯化氧的初始工序来制造聚氧化烯多元醇（A1）。在初始步骤之后，新提供烯化氧以进行聚合。在初始步骤中，开始加入烯化氧时反应体系的温度为120〜165℃，初始阶段加入环氧烷后的反应体系的最高温度高于比加入环氧烷的温度高15〜50℃。

5. 发明申请

US20090239964A1 PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM 审中-公开
标题翻译：生产柔性聚氨酯泡沫的方法
公开(公告)号：US20090239964A1
公开(公告)日：2009-09-24
申请号：US12412416
申请日：2009-03-27
申请人： Takayuki SASAKI , Naohiro Kumagai , Yasuyuki Sasao , Shigeru Ikai , Chitoshi Suzuki
发明人： Takayuki SASAKI , Naohiro Kumagai , Yasuyuki Sasao , Shigeru Ikai , Chitoshi Suzuki
IPC分类号： C08G18/32
CPC分类号： C08G18/4866 , C08G18/4804 , C08G18/7607 , C08G65/2615 , C08G65/2648 , C08G65/2663 , C08G2101/0008 , C08G2101/0058 , C08G2101/0083 , C08G2350/00
摘要： To provide a process for producing a flexible polyurethane foam, which can suitably form a flexible polyurethane foam having a good cushioning characteristic by using a raw material derived from a natural fat/oil.The process comprises a step of reacting a polyoxyalkylene polyol (A) containing the first polyoxyalkylene polyol (A1) obtained by ring-opening polymerization of an alkylene oxide (c) with an initiator (b) in the presence of a polymerization catalyst (a), with a polyisocyanate compound (B) in the presence of a catalyst (C) and a blowing agent (D). The polymerization catalyst (a) is at least one member selected from the group consisting of a coordination anionic polymerization catalyst and a cationic polymerization catalyst, and the initiator (b) is a polyol derived from a natural fat/oil, which is obtained by providing a natural fat/oil with hydroxyl groups through a chemical reaction, and has a hydroxyl value of from 20 to 250 mgKOH/g and a ratio of the mass average molecular weight to the number average molecular weight calculated as polystyrene, (Mw/Mn), of at least 1.2.
摘要翻译：提供一种生产软质聚氨酯泡沫的方法，其可以通过使用衍生自天然油脂的原料适当地形成具有良好缓冲特性的柔性聚氨酯泡沫。该方法包括在聚合催化剂（a）的存在下使包含通过环氧烷烃（c）的开环聚合获得的第一聚氧化烯多元醇（A1）与引发剂（b）的聚氧化烯多元醇（A），在催化剂（C）和发泡剂（D）的存在下与多异氰酸酯化合物（B）反应。聚合催化剂（a）是选自由配位阴离子聚合催化剂和阳离子聚合催化剂组成的组中的至少一种，引发剂（b）是衍生自天然油脂的多元醇，其通过提供通过化学反应具有羟基的天然脂肪/油，羟基值为20〜250mgKOH / g，以平均分子量为基准的聚苯乙烯换算的重均分子量（Mw / Mn），至少1.2。

6. 发明申请

US20120178840A1 POLYMER-DISPERSED POLYOL AND PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM 审中-公开
标题翻译：聚合物分散聚合物和生产柔性聚氨酯泡沫的方法
公开(公告)号：US20120178840A1
公开(公告)日：2012-07-12
申请号：US13430172
申请日：2012-03-26
申请人： Takayuki SASAKI , Naohiro KUMAGAI , Chitoshi SUZUKI , Yasuyuki SASAO , Jun KURATI
发明人： Takayuki SASAKI , Naohiro KUMAGAI , Chitoshi SUZUKI , Yasuyuki SASAO , Jun KURATI
IPC分类号： C08L75/04 , C08J9/04 , C08K5/053
CPC分类号： C08F289/00 , C08F2/44 , C08G18/36 , C08G18/4072 , C08G18/4866 , C08G18/631 , C08G2101/0008 , C08G2101/0083
摘要： To provide a polymer-dispersed polyol made by using materials derived from a natural fat/oil, which has a low viscosity, without lowering the biomass degree and without impairing the performance of a flexible polyurethane foam to be obtained. Further, to provide a process for producing a flexible polyurethane foam using the polymer-dispersed polyol. A polymer-dispersed polyol, comprising polymer particles dispersed in a matrix containing a polyol (a1) derived from a natural fat/oil and an epoxidized natural fat/oil (x). And, a process for producing a flexible polyurethane foam, which comprises reacting a polyol containing the above polymer-dispersed polyol and a polyisocyanate compound in the presence of a catalyst and a blowing agent.
摘要翻译：提供通过使用具有低粘度的衍生自天然脂肪/油的原料制造的聚合物分散多元醇，而不降低生物质量并且不损害所获得的柔性聚氨酯泡沫的性能。此外，提供使用聚合物分散多元醇制造软质聚氨酯泡沫的方法。一种聚合物分散的多元醇，其包含分散在含有天然脂肪/油衍生的多元醇（a1）和环氧化天然油脂（x）的基质中的聚合物颗粒。另外，生产软质聚氨酯泡沫体的方法包括在催化剂和发泡剂的存在下，使含有上述聚合物分散多元醇的多元醇与多异氰酸酯化合物反应。

7. 发明申请

US20100179240A1 PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM, PROCESS FOR PRODUCING HOT PRESS MOLDED PRODUCT, AND HOT PRESS MOLDED PRODUCT 失效
标题翻译：用于生产柔性聚氨酯泡沫的方法，用于生产热压成型产品的方法和热压成型产品
公开(公告)号：US20100179240A1
公开(公告)日：2010-07-15
申请号：US12732778
申请日：2010-03-26
申请人： Takayuki SASAKI , Daisuke Kaku
发明人： Takayuki SASAKI , Daisuke Kaku
IPC分类号： C08J9/00
CPC分类号： C08G18/4866 , C08G18/244 , C08G18/283 , C08G18/4808 , C08G65/2609 , C08G65/2648 , C08G65/2663 , C08G65/30 , C08G2101/0008 , C08G2101/0083 , C08L71/02 , C08L2666/22
摘要： To provide a process for producing a flexible polyurethane foam which is excellent in low resiliency, air flow and hot moldability, and a process for producing a hot press molded product by using such a flexible polyurethane foam. Further, the present invention provides a hot press molded product which has a low resiliency and air flow.A process for producing a flexible polyurethane foam, which comprises reacting a specific polyol with a specific polyisocyanate in the presence of a urethane-forming catalyst, a blowing agent and a foam stabilizer, at an isocyanate index of less than 90. Further, a process for hot press molding the flexible polyurethane foam obtained by such a process, and such a hot press molded product.
摘要翻译：提供一种生产柔软的聚氨酯泡沫的方法，其具有优异的低弹性，气流和热可模塑性，以及通过使用这种柔性聚氨酯泡沫制造热压成型产品的方法。此外，本发明提供一种具有低回弹性和空气流动性的热压成型制品。一种生产柔性聚氨酯泡沫的方法，其包括在异氰酸酯指数小于90的情况下，在氨基甲酸酯形成催化剂，发泡剂和泡沫稳定剂的存在下，使特定的多元醇与特定的多异氰酸酯反应。此外，用于热压成型通过这种方法得到的软质聚氨酯泡沫塑料，以及这种热压成型品。

8. 发明申请

US20100168262A1 PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM 失效
标题翻译：生产柔性聚氨酯泡沫的方法
公开(公告)号：US20100168262A1
公开(公告)日：2010-07-01
申请号：US12719930
申请日：2010-03-09
申请人： Takayuki SASAKI , Daisuke KAKU
发明人： Takayuki SASAKI , Daisuke KAKU
IPC分类号： C08J9/06
CPC分类号： C08G18/283 , C08G18/4072 , C08G18/4804 , C08G18/4866 , C08G18/632 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083 , C08G2350/00 , C08J2205/06
摘要： To provide a process for producing a flexible polyurethane foam, which comprises reacting a polyol compound and a polyisocyanate compound in an open system substantially without using a silicone foam stabilizer.A process for producing a flexible polyurethane foam, which comprises reacting a polyol composition (I) containing at least a polyol compound and containing at least one of a polyol compound (A) and a monool compound (X) obtained by ring-opening polymerization of an alkylene oxide with an initiator by using a double metal cyanide complex catalyst, and a polyisocyanate composition (II) in the presence of a urethane-forming catalyst made of a metal catalyst and an amine catalyst, and a blowing agent, in an open system substantially without using a silicone foam stabilizer.
摘要翻译：提供一种生产柔性聚氨酯泡沫的方法，其包括基本上不使用硅氧烷泡沫稳定剂在开放体系中使多元醇化合物和多异氰酸酯化合物反应。 1.一种软质聚氨酯泡沫塑料的制造方法，其特征在于，使至少含有多元醇化合物的多元醇组合物（I）与通过开环聚合得到的多元醇化合物（A）和一元醇化合物（X）中的至少一种反应，在金属催化剂和胺催化剂制成的氨基甲酸酯形成催化剂和发泡剂的存在下，通过使用双金属氰化物配合物催化剂的环氧烷与引发剂和多异氰酸酯组合物（II）基本上不使用硅氧烷泡沫稳定剂。

9. 发明申请

US20100096768A1 POLYMER-DISPERSED POLYOL AND PROCESS FOR PRODUCING FLEXIBLE POLYURETHANE FOAM 失效
标题翻译：聚合物分散聚合物和生产柔性聚氨酯泡沫的方法
公开(公告)号：US20100096768A1
公开(公告)日：2010-04-22
申请号：US12644043
申请日：2009-12-22
申请人： Takayuki SASAKI , Yasuyuki Sasao , Naohiro Kumagai , Chitoshi Suzuki , Shigeru Ikai
发明人： Takayuki SASAKI , Yasuyuki Sasao , Naohiro Kumagai , Chitoshi Suzuki , Shigeru Ikai
IPC分类号： C08J9/06 , C08K5/06 , C08K5/05 , C08J9/00
CPC分类号： C08G18/3206 , C08F2/20 , C08F2/44 , C08F283/06 , C08G18/4072 , C08G18/4841 , C08G18/4891 , C08G18/632 , C08G18/638 , C08G2101/0008 , C08G2101/0058 , C08G2101/0083 , C08J2205/06
摘要： To provide a process for producing a flexible polyurethane foam having a higher biomass degree than a conventional flexible polyurethane foam and excellent in foam physical properties and its appearance.A polymer-dispersed polyol obtained by polymerizing a vinyl monomer in the presence of the following polyol (a1) derived from a natural fat/oil and/or the following polyoxyalkylene polyol (a2) is used: Polyol (a1) derived from a natural fat/oil: a polyol derived from a natural fat/oil, which is obtained by providing a natural fat/oil with hydroxy groups by chemical reaction, and which has a hydroxy value of from 20 to 250 mgKOH/g and a molecular weight distribution of at least 1.2; Polyoxyalkylene polyol (a2): a polyoxyalkylene polyol which is produced by ring-opening polymerization of an alkylene oxide (c) with the polyol (a1) derived from a natural fat/oil in the presence of at least one polymerization catalyst (b) selected from the group consisting of a coordination anionic polymerization catalyst and a cationic polymerization catalyst.
摘要翻译：提供一种具有比常规柔性聚氨酯泡沫塑料具有更高生物质量并且具有优异的泡沫物理性能及其外观的柔性聚氨酯泡沫体的方法。使用通过在天然油脂和/或下列聚氧化烯多元醇（a2）得到的下列多元醇（a1）存在下使乙烯基单体聚合得到的聚合物分散多元醇：来自天然脂肪的多元醇（a1） /油：衍生自天然油脂的多元醇，其通过化学反应提供具有羟基的天然脂肪/油而得到，羟基值为20〜250mgKOH / g，分子量分布为至少1.2; 聚氧化烯多元醇（a2）：在至少一种聚合催化剂（b）的存在下，通过环氧烷（c）与由天然油脂衍生的多元醇（a1）的开环聚合制备的聚氧化烯多元醇由配位阴离子聚合催化剂和阳离子聚合催化剂组成。

10. 发明申请

US20080114088A1 LOW RESILIENCE FLEXIBLE POLYURETHANE FOAM AND PROCESS FOR ITS PRODUCTION 失效
标题翻译：低弹性柔性聚氨酯泡沫及其生产工艺
公开(公告)号：US20080114088A1
公开(公告)日：2008-05-15
申请号：US11876237
申请日：2007-10-22
申请人： Takayuki SASAKI , Takashi Ito
发明人： Takayuki SASAKI , Takashi Ito
IPC分类号： C08J9/04 , C08G18/08 , C08G18/48
CPC分类号： C08G18/283 , C08G18/4812 , C08G18/4866 , C08G2101/0008 , C08G2101/0058 , C08G2101/0083 , C08G2350/00
摘要： To provide a flexible polyurethane foam which is excellent in low resiliency and durability without using a plasticizer and which shows little change in hardness against a change in temperature and at the same time, has high air permeability. A process for producing a flexible polyurethane foam, which comprises reacting a polyol mixture comprising polyol (A), polyol (B) and monool (D) with a polyisocyanate compound in the presence of a blowing agent etc. at an isocyanate index of at least 90. Polyol (A) is a polyether polyol having an average of 2-3 hydroxyl groups and a hydroxyl value of from 10 to 90 mgKOH/g, obtained by ring-opening addition polymerization of an alkylene oxide to an initiator using a double metal cyanide complex catalyst; Polyol (B) is a polyether polyol having an average of 2-3 hydroxyl groups and a hydroxyl value of from 15 to 250 mgKOH/g, other than the polyol (A); and Monool (D) is a polyether monool having a hydroxyl value of from 10 to 200 mgKOH/g.
摘要翻译：为了提供一种柔软的聚氨酯泡沫塑料，其具有优异的低回弹性和耐久性，而不使用增塑剂，并且硬度相对于温度变化几乎没有变化，并且同时具有高的透气性。一种柔性聚氨酯泡沫塑料的制造方法，其特征在于，在发泡剂等的存在下，使多元醇（A），多元醇（B）和一元醇（D）的多元醇混合物与异氰酸酯指数的异氰酸酯指数至少多元醇（A）是具有平均2-3个羟基，羟基值为10至90mgKOH / g的聚醚多元醇，其通过使用双金属通过环氧烷与引发剂的开环加成聚合获得氰化物配合物催化剂; 多元醇（B）是多元醇（A）以外的平均2-3个羟基，羟值为15〜250mgKOH / g的聚醚多元醇。单醇（D）是羟值为10〜200mgKOH / g的聚醚一元醇。

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