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1. 发明授权

US5786096A Surface-treated substrate and process for its production 失效
标题翻译：表面处理基材及其生产工艺
公开(公告)号：US5786096A
公开(公告)日：1998-07-28
申请号：US746482
申请日：1996-11-12
申请人： Takashige Yoneda , Fumiaki Gunji , Takeshi Morimoto
发明人： Takashige Yoneda , Fumiaki Gunji , Takeshi Morimoto
IPC分类号： B05D1/18 , C03C17/34 , B05D3/02 , B32B9/04
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , C03C17/3405 , Y10T428/31612 , Y10T428/31663
摘要： A surface-treated substrate which is a substrate having at least two treated surface layers, wherein the first layer constituting the outermost layer among the treated surface layers is a layer formed by treatment with a surface treating agent containing compound B of the formula (B) as an essential component, and the second layer constituting an underlayer in contact with the outermost layer is a layer formed by treatment with a surface treating agent containing compound A of the formula (A) and Si(NCO).sub.4 as essential components: (R.sup.1).sub.a (R.sup.2).sub.b Si(Z).sub.4-a-b (A) (R.sup.3).sub.c (R.sup.4).sub.d Si(NCO).sub.4-c-d (B) wherein R.sup.1 is an organic group, R.sup.2 is a hydrogen atom or an organic group, a is 1, 2 or 3, b is 0, 1 or 2, provided that 1.ltoreq.a+b.ltoreq.3, and Z is an isocyanate group or a hydrolyzable group; and R.sup.3 is an organic group, R.sup.4 is a hydrogen atom or an organic group, c is 1, 2 or 3, and d is 0, 1 or 2, provided that 1.ltoreq.c+d.ltoreq.3.
摘要翻译：作为具有至少两个经处理的表面层的基板的表面处理基板，其中，处理表面层中构成最外层的第一层是通过用含有式（B）的化合物B的表面处理剂处理形成的层，构成与最外层接触的底层的第二层是通过用含有式（A）的化合物A和Si（NCO）4作为必要成分的表面处理剂处理形成的层：（R1 ）a（R2）bSi（Z）4-ab（A）（R3）c（R4）dSi（NCO）4-cd（B）其中R1是有机基团，R2是氢原子或有机基团，是1,2或3，b是0,1或2，条件是1≤a+b≤3，Z是异氰酸酯基或可水解基团; R3为有机基团，R4为氢原子或有机基团，c为1,2或3，d为0,1或2，条件是1≤c+d≤3。

2. 发明授权

US5576109A Surface treating agent and surface-treated substrate 失效
标题翻译：表面处理剂和表面处理基材
公开(公告)号：US5576109A
公开(公告)日：1996-11-19
申请号：US425037
申请日：1995-04-18
申请人： Takashige Yoneda , Takeshi Morimoto , Fumiaki Gunji , Kenji Ishizeki , Yukiko Ono
发明人： Takashige Yoneda , Takeshi Morimoto , Fumiaki Gunji , Kenji Ishizeki , Yukiko Ono
IPC分类号： B05D7/00 , C03C17/30 , C07F7/08 , C08G18/77 , C09D4/00 , B32B25/20
CPC分类号： B05D7/54 , C03C17/30 , C07F7/0863 , C08G18/778 , C09D4/00 , Y10T428/31663
摘要： A surface treating agent containing a silicone compound of the formula (A):(R.sup.1).sub.a (R.sup.2).sub.b (Z.sup.1).sub.3-a-b SiO--[Si(R.sup.3).sub.c (R.sup.4).sub.d (Z.sup.2).sub.2-c-d O].sub.n --Si(R.sup.5).sub.e (R.sup.6).sub.f (Z.sup.3).sub.3-e-f (A)wherein each of R.sup.1 to R.sup.6 which are independent of one another, is a hydrogen atom or an organic group, provided that at least one of R.sup.1 to R.sup.6 is an organic group;each of Z.sup.1 to Z.sup.3 which are independent of one another, is an isocyanate group or a hydrolyzable group;each of a to f which are independent of one another, is an integer of 0, 1 or 2, provided l.ltoreq.a+b.ltoreq.3, 0.ltoreq.c+d.ltoreq.2, l.ltoreq.e+f.ltoreq.3 and 2.ltoreq.a+b+c+d+e+f.ltoreq.7; andn is an integer of 0 or at least 1.
摘要翻译：含有式（A）的硅氧烷化合物的表面处理剂:( R1）a（R2）b（Z1）3-a-bSiO- [Si（R3）c（R4）d（Z2）2-c-dO ] n-Si（R 5）e（R 6）f（Z 3）3-ef（A）其中彼此独立的R 1至R 6中的每一个为氢原子或有机基团，条件是R 1至R 6中的至少一个 R6是有机基团; 彼此独立的Z 1至Z 3各自为异氰酸酯基或可水解基; 每个a至f彼此独立，为0,1或2的整数，条件是：a = a + b 3 = 0，c + d 2 / = e + f

3. 发明授权

US5976702A Composition for surface treatment 失效
标题翻译：表面处理用组合物
公开(公告)号：US5976702A
公开(公告)日：1999-11-02
申请号：US637109
申请日：1996-04-24
申请人： Takashige Yoneda , Fumiaki Gunji , Takeshi Morimoto
发明人： Takashige Yoneda , Fumiaki Gunji , Takeshi Morimoto
IPC分类号： C08G18/08 , C08G18/71 , C08G18/77 , B32B17/06 , B05D3/02 , C03C17/30 , C09K3/18
CPC分类号： C08G18/778 , C08G18/0852 , C08G18/718 , Y10T428/31612 , Y10T428/31663 , Y10T428/31667
摘要： A composition for surface treatment, which comprises a compound of the following formula (A) and an organic solvent (B) comprising an organic compound having a fluorine atom:(R.sup.1).sub.a (R.sup.2).sub.b (R.sup.3).sub.c Si(NCO).sub.4-a-b-c (A)wherein R.sup.1 is a monovalent organic group having a carbon number of from 1 to 30;R.sup.2 and R.sup.3 are respectively a hydrogen atom or a monovalent organic group having a carbon number of from 1 to 30, which may be the same or different;a is an integer of from 1 to 3; andb and c are independently 0 or 1 and 1.ltoreq.a+b+c.ltoreq.3.
摘要翻译：用于表面处理的组合物，其包含下式（A）的化合物和包含具有氟原子的有机化合物的有机溶剂（B）：（R1）a（R2）b（R3）cSi（NCO）4- abc（A）其中R1是碳数为1至30的一价有机基团; R2和R3分别为氢原子或碳原子数为1〜30的一价有机基团，其可以相同或不同; a为1〜3的整数; b和c独立地为0或1，且1≤b+ c + 3。

4. 发明授权

US5871843A Laminate and process for its production 失效
标题翻译：层压板及其生产工艺
公开(公告)号：US5871843A
公开(公告)日：1999-02-16
申请号：US824290
申请日：1997-03-26
申请人： Takashige Yoneda , Makoto Fukawa , Takeshi Morimoto , Kazuo Sato , Fumiaki Gunji , Hiromichi Nishimura , Satoshi Takeda , Yasuo Hayashi , Hiroyuki Fujita
发明人： Takashige Yoneda , Makoto Fukawa , Takeshi Morimoto , Kazuo Sato , Fumiaki Gunji , Hiromichi Nishimura , Satoshi Takeda , Yasuo Hayashi , Hiroyuki Fujita
IPC分类号： C03C17/00 , C03C17/25 , G02B1/11 , G02B1/10 , C03C17/02
CPC分类号： C03C17/25 , C03C17/007 , C03C17/009 , G02B1/113 , C03C2217/213 , C03C2217/42 , C03C2217/77 , C03C2218/113 , Y10T428/249978 , Y10T428/266
摘要： A laminate comprising a substrate and at least one layer formed on the substrate, in which the outermost layer as a surface layer has a plurality of micropores therein and, at its surface, a flat portion and fine craters, said flat portion having a surface roughness R.sub.a of at most 3 nm and an area ratio of at least 20%.
摘要翻译：一种层压体，包括基材和至少一层形成在基材上的层，其中作为表面层的最外层在其中具有多个微孔，在其表面具有平坦部分和细小凹坑，所述平坦部分具有表面粗糙度 Ra为3nm以下，面积率为20％以上。

5. 发明授权

US5605958A Composition for surface treatment 失效
标题翻译：表面处理用组合物
公开(公告)号：US5605958A
公开(公告)日：1997-02-25
申请号：US530911
申请日：1995-09-20
申请人： Takashige Yoneda , Fumiaki Gunji , Takeshi Morimoto , Yukiko Ono
发明人： Takashige Yoneda , Fumiaki Gunji , Takeshi Morimoto , Yukiko Ono
IPC分类号： C04B41/83 , C03C17/30 , C07F7/10 , C09D4/00 , C09D5/00 , C09D201/00 , C09K3/00 , C09K3/18 , C08K5/06
CPC分类号： C09D201/00 , C09D4/00 , C09D5/00 , Y10T428/31663
摘要： A composition for surface treatment, which comprises the following components (I), (II) and (III) as essential components:(I) at least one compound capable of forming a coating film with a contact angle of at least 70.degree. against water;(II) a solvent capable of dissolving the component (I); and(III) a solvent having an evaporation rate lower than the component (II).
摘要翻译：用于表面处理的组合物，其包含以下成分（I），（II）和（III）作为必要成分：（I）至少一种能够形成与水接触角至少为70°的涂膜的化合物 ; （II）能够溶解组分（I）的溶剂; 和（III）具有低于组分（II）的蒸发速率的溶剂。

6. 发明授权

US06599634B2 Fluorine-containing organic silicon compound, water repellent composition containing it, and surface-treated substrate and process for its production 失效
标题翻译：含氟有机硅化合物，含有它的防水组合物和表面处理基材及其制备方法
公开(公告)号：US06599634B2
公开(公告)日：2003-07-29
申请号：US09973891
申请日：2001-10-11
申请人： Takashige Yoneda , Tadashi Hamano , Fumiaki Gunji
发明人： Takashige Yoneda , Tadashi Hamano , Fumiaki Gunji
IPC分类号： B32B904
CPC分类号： C09D183/08 , C07F7/04 , C08G77/24 , C08L83/08 , C09D4/00 , Y10T428/31612 , Y10T428/31663 , C08G77/00
摘要： A fluorine-containing organic silicon compound of the following formula (1): wherein Rf is a fluorine-containing C1-20 monovalent organic group, X1 is an alkylene group, n is an integer of from 0 to 100, R is a C1-5 monovalent hydrocarbon group, X is a hydrolyzable group, and p is 0, 1 or 2.
摘要翻译：下式（1）的含氟有机硅化合物：其中，Rf为氟代C 1-20一价有机基团，X 1为亚烷基，n为0〜100的整数，R为C1- 5个一价烃基，X是可水解基团，p是0,1或2。

7. 发明授权

US06733892B1 Surface treatment composition, method of surface treatment, substrate and article 失效
标题翻译：表面处理组合物，表面处理方法，基材和制品
公开(公告)号：US06733892B1
公开(公告)日：2004-05-11
申请号：US09508080
申请日：2000-04-19
申请人： Takashige Yoneda , Fumiaki Gunji
发明人： Takashige Yoneda , Fumiaki Gunji
IPC分类号： B32B904
CPC分类号： C09K3/18 , C09D183/08 , Y10T428/31612 , Y10T428/31663
摘要： The object of the present invention is to provide a surface treatment composition having excellent storage stability and waterdrop rolling property. The present invention provides a surface treatment composition containing a partial hydrolysate of a fluorine-containing reactive silane such as C8F17CH2CH2Si(OCH3)3 having a molecular weight of M measured by GPC, wherein the proportion of molecules with molecular weights of from 300 to at most 2M in the partial hydrolysate is less than 70%, and the proportion of molecules with molecular weights of from 6M to 100000 in the partial hydrolysate is less than 10%. The present invention also provides a method of surface treatment of glass with the surface treatment composition. The present invention also provides a substrate treated with the surface treatment composition. The present invention also provides an article incorporating the substrate such as a transport equipment.
摘要翻译：本发明的目的是提供一种表面处理组合物，其具有优异的储存稳定性和水滴性能。本发明提供了含有含氟反应性硅烷的部分水解产物如C8F17CH2CH2Si（OCH3）3的表面处理组合物，其具有通过GPC测量的M的分子量，其中在部分水解产物中分子量为300至至多2M的分子的比例小于70％，部分水解产物中分子量为6M至100000的分子的比例本发明还提供了一种用表面处理组合物对玻璃进行表面处理的方法。本发明还提供了用表面处理组合物处理的基材。本发明还提供了一种将基材如运输设备。

8. 发明授权

US5482768A Surface-treated substrate and process for its production 失效
标题翻译：表面处理基材及其生产工艺
公开(公告)号：US5482768A
公开(公告)日：1996-01-09
申请号：US242675
申请日：1994-05-13
申请人： Takeshi Kawasato , Kazuya Hiratsuka , Takashige Yoneda , Tsuneo Wakabayashi , Fumiaki Gunji
发明人： Takeshi Kawasato , Kazuya Hiratsuka , Takashige Yoneda , Tsuneo Wakabayashi , Fumiaki Gunji
IPC分类号： B05D5/08 , B05D7/00 , C03C17/34 , B32B17/06 , C09K3/18
CPC分类号： B05D7/54 , B05D5/083 , C03C17/3405 , C03C2217/42 , C03C2217/47 , C03C2217/475 , Y10T428/254 , Y10T428/31612 , Y10T428/31663
摘要： A surface-treated substrate consisting essentially of a substrate having at least two treated surface layers wherein the first layer constituting the outermost layer among the treated surface layers is a layer formed by treating with a treating agent containing a compound (I) capable of forming a surface having a contact angle of at least 70.degree. against water, and the second layer constituting an underlayer in contact with the outermost layer is a thin film layer of a heat resistant polymer formed by treating with a treating agent containing a compound (II) capable of forming a thin film of a heat resistant polymer and fine particles of a polymer, to form a thin film and heating the thin film to thermally decompose the fine particles of a polymer.
摘要翻译：表面处理基材，其基本上由具有至少两个经处理的表面层的基材组成，其中构成处理过的表面层中的最外层的第一层是通过用含有能够形成表面与水接触角至少为70°，构成与最外层接触的底层的第二层是通过用含有化合物（II）的处理剂进行处理而形成的耐热聚合物的薄膜层形成耐热聚合物的薄膜和聚合物的细颗粒，以形成薄膜并加热薄膜以使聚合物的细颗粒热分解。

9. 发明授权

US06500553B1 Substrate having treated surface layers and process for producing it 失效
标题翻译：具有处理表面层的基体及其制造方法
公开(公告)号：US06500553B1
公开(公告)日：2002-12-31
申请号：US09712214
申请日：2000-11-15
申请人： Takashige Yoneda , Tadashi Hamano , Fumiaki Gunji
发明人： Takashige Yoneda , Tadashi Hamano , Fumiaki Gunji
IPC分类号： B32B904
CPC分类号： C03C17/3405 , C03C17/42 , Y10T428/31612 , Y10T428/31663
摘要： A substrate having at least two treated surface layers, wherein the first layer constituting the outermost layer among the treated surface layers is a layer formed by covering with a composition containing a reactive silane compound (I) which forms a surface having a rolling angle of at most 30° to water, and the second layer constituting an underlayer in contact with the first layer is a layer formed by covering with a composition (II) containing a fluorine-containing reactive silane compound (II) which forms a surface having a contact angle of at least 100° to water.
摘要翻译：具有至少两个经处理的表面层的基底，其中构成处理过的表面层中的最外层的第一层是通过用包含反应性硅烷化合物（I）的组合物覆盖而形成的层，所述反应性硅烷化合物（I）形成具有与水最多30°，构成与第一层接触的底层的第二层是通过用含有含氟反应性硅烷化合物（II）的组合物（II）覆盖形成的层，其形成具有接触角的表面与水至少100°。

10. 发明授权

US06479157B1 Substrate having treated surface layers and process for producing it 失效
标题翻译：具有处理表面层的基体及其制造方法
公开(公告)号：US06479157B1
公开(公告)日：2002-11-12
申请号：US09712251
申请日：2000-11-15
申请人： Takashige Yoneda , Tadashi Hamano , Fumiaki Gunji
发明人： Takashige Yoneda , Tadashi Hamano , Fumiaki Gunji
IPC分类号： B32B1710
CPC分类号： C03C17/42 , C03C17/3405 , Y10T428/31612 , Y10T428/31663
摘要： A substrate having at least two treated surface layers, wherein the first layer constituting the outermost layer among the treated surface layers is a layer formed by covering with a composition (I) containing a predetermined organic silicon compound, and the second layer constituting an underlayer in contact with the first layer is a layer formed by covering with a composition (II) containing a fluorine-containing reactive silane compound (II) which forms a surface having a contact angle of at least 100° to water.
摘要翻译：具有至少两个经处理的表面层的基板，其中构成处理过的表面层中的最外层的第一层是通过用含有预定的有机硅化合物的组合物（I）覆盖而形成的层，并且构成下层的第二层与第一层接触是通过用含有含氟反应性硅烷化合物（II）的组合物（II）覆盖形成的层，其形成与水的接触角至少为100°的表面。

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