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1. 发明授权

US06878663B2 Method for producing palladium complex compound 失效
标题翻译：钯配合物的制造方法
公开(公告)号：US06878663B2
公开(公告)日：2005-04-12
申请号：US10116057
申请日：2002-04-05
申请人： Takashi Kume , Satoru Narizuka , Makoto Koide , Koichi Mikami , Manabu Hatano , Masahiro Terada
发明人： Takashi Kume , Satoru Narizuka , Makoto Koide , Koichi Mikami , Manabu Hatano , Masahiro Terada
IPC分类号： C07F15/00 , C07F17/02
CPC分类号： C07F15/006 , C07F15/0066
摘要： An aromatic compound represented by the general formula Ar1X is reacted with a palladium compound and a phosphine derivative, in the presence of a first basic substance, thereby producing a palladium-complex compound represented by the general formula Ar1—PdL2X. This palladium-complex compound is reacted with a benzoic acid represented by the general formula Ar2—COOH, in the presence of a second basic substance, thereby producing another palladium-complex compound represented by the following general formula. The above palladium-complex compounds are useful as catalysts and can be produced easily by the above reactions. In the above general formulas, Ar1 is an aryl group; and X is a halogen that is fluorine, chlorine, bromine or iodine, trifluoromethanesulfonate group, an alkylsulfonate group having a carbon atom number of 1-4, or a substituted or unsubstituted arylsulfonate group; each L is independently a phosphine ligand; and Ar2 is an aryl group.
摘要翻译：在通式Ar 1 X表示的芳香族化合物与钯化合物和膦衍生物在第一碱性物质的存在下反应，由此制备由通式Ar 1〜 PdL2X。在第二碱性物质的存在下，使该钯络合物与通式为Ar 2 -COOH表示的苯甲酸反应，由此生成由以下通式表示的另一种钯络合物。复合化合物可用作催化剂，并且可以通过上述反应容易地制备。在上述通式中，Ar 1是芳基; X是氟，氯，溴或碘的卤素，三氟甲磺酸酯基，碳原子数为1-4的烷基磺酸酯基或取代或未取代的芳基磺酸酯基; 每个L独立地是膦配体; Ar 2为芳基。

2. 发明授权

US06706905B1 Method for producing palladium complex compound 失效
标题翻译：钯配合物的制造方法
公开(公告)号：US06706905B1
公开(公告)日：2004-03-16
申请号：US09458080
申请日：1999-12-10
申请人： Takashi Kume , Satoru Narizuka , Makoto Koide , Koichi Mikami , Manabu Hatano , Masahiro Terada , Michio Ishida , Yuzuru Morino
发明人： Takashi Kume , Satoru Narizuka , Makoto Koide , Koichi Mikami , Manabu Hatano , Masahiro Terada , Michio Ishida , Yuzuru Morino
IPC分类号： C07F1702
CPC分类号： C07F15/006 , C07F15/0066
摘要： An aromatic compound represented by the general formula Ar1X is reacted with a palladium compound and a phosphine derivative, in the presence of a first basic substance, thereby producing a palladium-complex compound represented by the general formula Ar1—PdL2X. This palladium-complex compound is reacted with a benzoic acid represented by the general formula Ar2—COOH, in the presence of a second basic substance, thereby producing another palladium-complex compound represented by the following general formula. The above palladium-complex compounds are useful as catalysts and can be produced easily by the above reactions. In the above general formulas, Ar1 is an aryl group; and X is a halogen that is fluorine, chlorine, bromine or iodine, trifluoromethanesulfonate group, an alkylsulfonate group having a carbon atom number of 1-4, or a substituted or unsubstituted arylsulfonate group; each L is independently a phosphine ligand; and Ar2 is an aryl group.
摘要翻译：在通式Ar 1 X表示的芳香族化合物与钯化合物和膦衍生物在第一碱性物质的存在下反应，由此制备由通式Ar 1〜 PdL2X。在第二碱性物质的存在下，使该钯络合物与通式为Ar 2 -COOH表示的苯甲酸反应，由此生成由以下通式表示的另一种钯络合物。复合化合物可用作催化剂，并且可以通过上述反应容易地制备。在上述通式中，Ar 1是芳基; X是氟，氯，溴或碘的卤素，三氟甲磺酸酯基，碳原子数为1-4的烷基磺酸酯基或取代或未取代的芳基磺酸酯基; 每个L独立地是膦配体; Ar 2为芳基。

3. 发明授权

US5155240A Process for producing optically active dihydropyran derivative 失效
标题翻译：光学活性二氢吡喃衍生物的制备方法
公开(公告)号：US5155240A
公开(公告)日：1992-10-13
申请号：US668656
申请日：1991-03-13
申请人： Koichi Mikami , Masahiro Terada , Takeshi Nakai , Noboru Sayo
发明人： Koichi Mikami , Masahiro Terada , Takeshi Nakai , Noboru Sayo
IPC分类号： C07D309/28
CPC分类号： C07D309/28
摘要： A process for producing an optically active dihydropyran derivative represented by formula (1): ##STR1## wherein R.sup.1, R.sup.2, R.sup.3, and R.sup.4 each represents a hydrogen atom, a lower alkyl group, a tri-lower alkylsilylmethyl group, a lower alkoxycarbonylamino group, or an --OR.sup.5 group, wherein R.sup.5 represents a lower alkyl group, a lower acyl group, a lower alkoxycarbonyl group, a di-lower alkylcarbamoyl group, or a tri-lower alkylsilyl group, or R.sup.1 and R.sup.2 are taken together to form a 5- to 7-membered cyclic hydrocarbon group or to form a condensed heterocyclic group with an oxygen atom, or R.sup.2 and R.sup.3 are taken together to form a 5- to 7-membered cyclic hydrocarbon group or to form a condensed heterocyclic group with an oxygen atom, provided that all of R.sup.1, R.sup.2, R.sup.3, and R.sup.4 do not represent hydrogen atoms at the same time; and R.sup.6 represents a lower alkyl group, which comprises reacting a diene compound represented by formula (2): ##STR2## wherein R.sup.1, R.sup.2, R.sup.3, and R.sup.4 have the same meanings as defined above, with a glyoxylic acid ester represented by formula (3): ##STR3## wherein R.sup.6 has the same meaning as defined above, in the presence of a binaphthol-titanium complex represented by formula (4): ##STR4## wherein X represents a chlorine atom or a bromine atom, is disclosed.
摘要翻译：一种制备式（1）表示的光学活性二氢吡喃衍生物的方法：其中R1，R2，R3和R4各自表示氢原子，低级烷基，三低级烷基甲硅烷基甲基，低级烷氧基羰基氨基或-OR5基团，其中R5表示低级烷基，低级酰基，低级烷氧基羰基，二低级烷基氨基甲酰基或三低级烷基甲硅烷基，或者R1和R2组合在一起形成5至7元环状烃基或与氧原子形成稠合杂环基，或将R 2和R 3一起形成5-至7-元环状烃基或形成稠合杂环基具有氧原子，条件是所有R1，R2，R3和R4不同时表示氢原子; 并且R 6表示低级烷基，其包括使式（2）表示的二烯化合物：其中R 1，R 2，R 3和R 4具有与上述相同的含义，与表示的二羟乙酸酯反应在式（4）表示的联萘酚钛化合物存在下，式（3）表示：其中R 6具有与上述相同的含义，其中X表示氯原子或溴原子。

4. 发明授权

US4965398A Process for producing optically active alpha-hydroxycarboxylates 失效
标题翻译：光学活性α-羟基羧酸盐的制备方法
公开(公告)号：US4965398A
公开(公告)日：1990-10-23
申请号：US386480
申请日：1989-07-28
申请人： Koichi Mikami , Masahiro Terada , Takeshi Nakai , Noboru Sayo , Hidenori Kumobayashi
发明人： Koichi Mikami , Masahiro Terada , Takeshi Nakai , Noboru Sayo , Hidenori Kumobayashi
IPC分类号： B01J31/22 , C07B61/00 , C07C67/347 , C07C69/732
CPC分类号： C07C69/732
摘要： A process for preparing an .alpha.-hydroxycarboxylate represented by formula (I): ##STR1## wherein R.sup.1 represents a hydrogen atom or a lower alkyl group; R.sup.2 represents a lower alkyl group, a phenyl group or a cycloalkyl group, or R.sup.1 and R.sup.2 are bonded to each other to form a five- to seven-membered cycloalkenyl or bicycloalkenyl ring which may be substituted with a lower alkyl group; and R.sup.3 represents a lower alkyl group,which comprises reacting an olefin compound represented by formula (II): ##STR2## wherein R.sup.1 ' represents a hydrogen atom or a lower alkyl group; and R.sup.2 ' represents a lower alkyl group, a phenyl group or a cycloalkyl group, or R.sup.1 ' and R.sup.2 ' are bonded to each other to form a five- to seven-membered cycloalkyl or bicycloalkyl ring which may be substituted with a lower alkyl group,with a glyoxylate represented by formula (III): ##STR3## wherein R.sup.3 is as defined above, in the presence of a binaphthol-titanium complex represented by formula (IV): ##STR4## wherein X represents a chlorine atom or bromine atom.

5. 发明授权

US5434289A Process for producing optically active .beta.-hydroxyketone 失效
标题翻译：光学活性β-羟基酮的制备方法
公开(公告)号：US5434289A
公开(公告)日：1995-07-18
申请号：US208379
申请日：1994-03-10
申请人： Koichi Mikami , Satoru Matsukawa , Masaki Shimizu , Masahiro Terada , Noboru Sayo
发明人： Koichi Mikami , Satoru Matsukawa , Masaki Shimizu , Masahiro Terada , Noboru Sayo
IPC分类号： B01J31/22 , C07B53/00 , C07B61/00 , C07C45/51 , C07C45/67 , C07C67/333 , C07C67/343 , C07C67/38 , C07C69/675 , C07C69/708 , C07C69/712 , C07C69/732 , C07C69/734 , C07C319/20 , C07C323/22 , C07C327/28 , C07C327/32 , C07C327/00 , C07C45/00 , C07C69/76
CPC分类号： C07C327/32 , C07C327/28 , C07C45/511 , C07C67/343
摘要： A process for producing an optically active .beta.-hydroxyketone represented by formula (I): ##STR1## by catalytic asymmetrical aldol reaction is disclosed, comprising reacting a silyl-enol ether represented by formula (II): ##STR2## with a substituted aldehyde represented by formula (III):R.sup.5 CHO (III)in the presence of a binaphthol-titanium complex represented by formula (IV): ##STR3## An optically active .beta.-hydroxyketone is efficiently produced with diastereo-specificity and enantio-specificity.
摘要翻译：公开了由式（I）表示的光学活性β-羟基酮：通过催化不对称醛醇缩合反应制备的光学活性β-羟基酮的方法，包括使由式（II）表示的甲硅烷基烯醇醚：）与由式（III）表示的取代的醛：R5CHO（III）在由式（IV）表示的联萘酚 - 钛络合物的存在下：以非对映特异性和对映体特异性有效地产生。

6. 发明授权

US08999463B2 Glare-proofing optical laminate 有权
标题翻译：防眩光学层压板
公开(公告)号：US08999463B2
公开(公告)日：2015-04-07
申请号：US11817818
申请日：2006-03-29
申请人： Koichi Mikami , Yukimitsu Iwata , Yoshihiro Nishimura , Takashi Kodama
发明人： Koichi Mikami , Yukimitsu Iwata , Yoshihiro Nishimura , Takashi Kodama
IPC分类号： C09K19/00 , G02B5/02 , G02B5/30
CPC分类号： G02B1/111 , G02B5/02 , G02B5/3033 , Y10T428/1036 , Y10T428/24372 , Y10T428/24537 , Y10T428/2457 , Y10T428/25 , Y10T428/26
摘要： An anti-dazzling laminate made of an optical laminate including a light transparent base material and an anti-dazzling layer having a concavoconvex shape provided on the material. The laminate simultaneously satisfies formulae: 0≦G100≦15 (I), 0.1≦Hs≦5.0 (II), 0.3≦Rz≦1.8 (III) wherein G100 represents a scintillation value which is a standard deviation of a variation in brightness distribution at a resolution of 100 ppi measured on the surface of the laminate; Hs represents the surface haze value of the laminate; and Rz represents the average roughness of the concavoconvex shape of the anti-dazzling layer.
摘要翻译：由光学层压制品制成的防光泽层压材料，该层压材料包括透明基材和具有凹凸形状的抗眩光层。层压板同时满足公式：0＆nlE; G100＆nlE; 15（I），0.1＆nlE; Hs＆nlE; 5.0（II），0.3＆nlE; Rz＆nlE; 1.8（III）其中G100表示闪烁值，其是亮度变化的标准偏差在层压板的表面上测量的分辨率为100ppi的分布; Hs表示层压板的表面雾度值; Rz表示防炫目层的凹凸形状的平均粗糙度。

7. 发明授权

US08741499B2 Solid oxide fuel cell 失效
标题翻译：固体氧化物燃料电池
公开(公告)号：US08741499B2
公开(公告)日：2014-06-03
申请号：US12926400
申请日：2010-11-16
申请人： Kuniaki Yoshikata , Koichi Mikami , Hirotoshi Sakamoto
发明人： Kuniaki Yoshikata , Koichi Mikami , Hirotoshi Sakamoto
IPC分类号： H01M8/24
CPC分类号： H01M8/1246 , H01M8/0247 , H01M8/0297 , H01M8/1213 , H01M8/1286 , H01M8/24 , H01M8/2425 , H01M8/2428 , Y02E60/525 , Y02P70/56
摘要： The solid oxide fuel cell of the present invention has a substrate (1); an electrolyte (3) that is disposed on one surface of the substrate (1); and at least one electrode element E having an anode (5) and a cathode (7) disposed on the same surface of the electrolyte (3) with a predetermined space therebetween.
摘要翻译：本发明的固体氧化物型燃料电池具有基板（1）。设置在所述基板（1）的一个表面上的电解质（3）; 以及至少一个具有阳极（5）和阴极（7）的电极元件E，其间以预定的间隔设置在电解质（3）的同一表面上。

8. 发明申请

US20130310580A1 Method For Producing Optically Active Fluorine-Containing Oxeten 有权
标题翻译：生产含活性氟的Oxeten的方法
公开(公告)号：US20130310580A1
公开(公告)日：2013-11-21
申请号：US13989662
申请日：2011-11-16
申请人： Koichi Mikami , Kohsuke Aikawa , Yuta Hioki
发明人： Koichi Mikami , Kohsuke Aikawa , Yuta Hioki
IPC分类号： C07D305/10
CPC分类号： C07D305/10 , C07D407/04 , C07D409/04
摘要： A method for producing an optically active fluorine-containing oxeten, the method being provided to include the steps of causing a fluorine-containing α-ketoester and an internal alkyne to react with each other in the presence of a transition metal complex that has an optically active ligand.
摘要翻译：一种制备光学活性的含氟氧杂环丁酮的方法，该方法包括以下步骤：使含氟α-酮酯和内炔在具有光学性活性配体。

9. 发明授权

US08493660B2 Optical layered body comprising a light-transmitting substrate and antiglare layer, polarizer and image display device 有权
标题翻译：光学层叠体，包括透光基板和防眩光层，偏振片和图像显示装置
公开(公告)号：US08493660B2
公开(公告)日：2013-07-23
申请号：US12377782
申请日：2007-08-16
申请人： Gen Furui , Yukimitsu Iwata , Takashi Kodama , Yoshihiro Nishimura , Koichi Mikami
发明人： Gen Furui , Yukimitsu Iwata , Takashi Kodama , Yoshihiro Nishimura , Koichi Mikami
IPC分类号： G02B1/10
CPC分类号： G02B1/11 , G02B5/0221 , G02B5/0278 , G02B5/30
摘要： An optical layered body including a light-transmitting substrate and an antiglare layer provided on the light-transmitting substrate. The antiglare layer has a surface roughness on the outermost surface. In the optical layered body, a mean spacing of tops of local peak of profile S is 0.045 mm or more and 0.10 mm or less determined by the procedure disclosed in the specification. The optical layered body can attain properties such as an antiglare property, scintillation prevention and black color reproducibility such as gloss blackness simultaneously.
摘要翻译：一种光学层叠体，包括设置在透光性基板上的透光性基板和防眩光层。防眩层在最外表面具有表面粗糙度。在光学层叠体中，轮廓S的局部峰的顶部的平均间距通过说明书中公开的程序确定为0.045mm以上且0.10mm以下。光学层叠体可以同时获得诸如防眩光性质，防闪烁性和黑色再现性等光泽度的性质。

10. 发明授权

US08278479B2 Method for producing optically active fluorine-containing carbonyl-ene product 有权
标题翻译：光学活性含氟羰基产物的制备方法
公开(公告)号：US08278479B2
公开(公告)日：2012-10-02
申请号：US12519959
申请日：2007-12-18
申请人： Koichi Mikami , Kohsuke Aikawa , Akihiro Ishii , Kaori Mogi , Takashi Ootsuka
发明人： Koichi Mikami , Kohsuke Aikawa , Akihiro Ishii , Kaori Mogi , Takashi Ootsuka
IPC分类号： C07C69/732
CPC分类号： C07C67/347 , C07B53/00 , C07B2200/07 , C07C67/343 , C07C69/732
摘要： An optically active, fluorine-containing carbonyl-ene product is produced by reacting a fluorine-containing α-ketoester with an alkene in the presence of a transition metal complex having an optically active ligand. There are Mode 1 of conducting this reaction in the absence of reaction solvent, Mode 2 of conducting this reaction in a solvent that is low in relative dielectric constant, and Mode 3 of conducting this reaction in a halogenated hydrocarbon-series solvent. In each of these three modes, it is possible to produce the optically active, fluorine-containing carbonyl-ene product with low cost.
摘要翻译：通过在具有光学活性配体的过渡金属络合物的存在下使含氟α-酮酯与烯烃反应来制备光学活性的含氟羰基产物。在没有反应溶剂的情况下进行该反应的方式1，在相对介电常数低的溶剂中进行该反应的方式2，以及在卤代烃系溶剂中进行该反应的方式3。在这三种模式中的每一种中，可以以低成本制造光学活性的含氟羰基产物。

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