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1. 发明申请

US20060167178A1 Process for producing aqueous resin dispersion 失效
标题翻译：水性树脂分散液的制造方法
公开(公告)号：US20060167178A1
公开(公告)日：2006-07-27
申请号：US10546070
申请日：2004-02-18
申请人： Takashi Kitamura , Keiichiro Saikawa , Kenichi Tomita , Takeshi Inoue , Kenya Suzuki , Hiromi Harakawa , Masami Sugishima
发明人： Takashi Kitamura , Keiichiro Saikawa , Kenichi Tomita , Takeshi Inoue , Kenya Suzuki , Hiromi Harakawa , Masami Sugishima
IPC分类号： C08F220/62 , C08F20/04
CPC分类号： C08F220/64
摘要： This invention provides a process for producing an aqueous resin dispersion in which the average particle diameter of the dispersed resin is not more than 500 nm, comprising finely dispersing a monomeric mixture (I) containing (A) fatty acid-modified polymerizable unsaturated monomer and (B) other polymerizable unsaturated monomer which is copolymerizable with the monomer (A) in an aqueous medium in such a manner that the dispersed particles have an average particle diameter not more than 500 nm, and polymerizing the resulting emulsified product. The invention also provides aqueous resin compositions which comprise the aqueous resin dispersions, and water-based paint compositions which comprise the aqueous resin compositions.
摘要翻译：本发明提供了分散树脂的平均粒径为500nm以下的水性树脂分散体的制造方法，其特征在于，将含有（A）脂肪酸改性聚合性不饱和单体和（A）的单体混合物（I） B）可在水性介质中与单体（A）共聚的其它可聚合不饱和单体，使得分散颗粒的平均粒径不超过500nm，并使得到的乳化产物聚合。本发明还提供包含水性树脂分散体的水性树脂组合物和包含水性树脂组合物的水性涂料组合物。

2. 发明授权

US07479524B2 Process for producing aqueous resin dispersions 失效
标题翻译：生产水性树脂分散体的方法
公开(公告)号：US07479524B2
公开(公告)日：2009-01-20
申请号：US10546070
申请日：2004-02-18
申请人： Takashi Kitamura , Keiichiro Saikawa , Kenichi Tomita , Takeshi Inoue , Kenya Suzuki , Hiromi Harakawa , Masami Sugishima
发明人： Takashi Kitamura , Keiichiro Saikawa , Kenichi Tomita , Takeshi Inoue , Kenya Suzuki , Hiromi Harakawa , Masami Sugishima
IPC分类号： C08L33/00
CPC分类号： C08F220/64
摘要： This invention provides a process for producing an aqueous resin dispersion in which the average particle diameter of the dispersed resin is not more than 500 nm, comprising finely dispersing a monomeric mixture (I) containing (A) fatty acid-modified polymerizable unsaturated monomer and (B) other polymerizable unsaturated monomer which is copolymerizable with the monomer (A) in an aqueous medium in such a manner that the dispersed particles have an average particle diameter not more than 500 nm, and polymerizing the resulting emulsified product. The invention also provides aqueous resin compositions which comprise the aqueous resin dispersions, and water-based paint compositions which comprise the aqueous resin compositions.
摘要翻译：本发明提供了分散树脂的平均粒径为500nm以下的水性树脂分散体的制造方法，其特征在于，将含有（A）脂肪酸改性聚合性不饱和单体和（A）的单体混合物（I） B）可在水性介质中与单体（A）共聚的其它可聚合不饱和单体，使得分散颗粒的平均粒径不超过500nm，并使得到的乳化产物聚合。本发明还提供包含水性树脂分散体的水性树脂组合物和包含水性树脂组合物的水性涂料组合物。

3. 发明授权

US6099968A Water-base metallic paint composition and method of forming overcoat 有权
标题翻译：水基金属漆组合物及其形成方法
公开(公告)号：US6099968A
公开(公告)日：2000-08-08
申请号：US341878
申请日：1999-07-19
申请人： Hiromi Harakawa , Kenya Suzuki
发明人： Hiromi Harakawa , Kenya Suzuki
IPC分类号： C09D133/06 , B32B27/36
CPC分类号： C09D133/062 , C09D133/066
摘要： The present invention provides an aqueous metallic coating composition comprising (A) 100 parts, based on solids, of a film-forming aqueous acrylic polymer obtained by neutralizing a copolymer having a number average molecular weight of 2,000 to 200,000, an acid value of 10 to 110 mg KOH/g and a hydroxyl value of 20 to 100 mg KOH/g, the copolymer being obtained by copolymerizing (a) 10 to 35 wt. % of styrene, (b) 5 to 25 wt. % of C.sub.6-18 alkyl (meth)acrylate, (c) 0.1 to 10 wt. % of phosphoric ester group-containing polymerizable unsaturated monomer represented by the general formula ##STR1## wherein X is a hydrogen atom or methyl, and m is an integer of 1 to 3, (d) 2 to 10 wt. % of carboxyl-containing polymerizable unsaturated monomer, (e) 5 to 20 wt. % of hydroxyl-containing polymerizable unsaturated monomer, and (f) 0 to 77.9 wt. % of other polymerizable unsaturated monomer, and (B) 2 to 100 parts by weight of a metallic flake pigment; and a method for forming a topcoat using the composition.
摘要翻译： PCT No.PCT / JP98 / 00183 Sec。 371日期1999年7月19日第 102（e）日期1999年7月19日PCT提交1998年1月20日PCT公布。公开号WO98 / 31756 日期1998年7月23日本发明提供一种水性金属涂料组合物，其包含（A）基于固体100份通过中和数均分子量为2,000至200,000的共聚物获得的成膜水性丙烯酸类聚合物，酸值为10〜110mgKOH / g，羟基值为20〜100mgKOH / g，共聚物通过（a）10〜35重量％％的苯乙烯，（b）5〜25wt。％的（甲基）丙烯酸C 6-18烷基酯，（c）0.1〜10重量％％的由以下通式表示的含磷酸酯基的可聚合不饱和单体其中X为氢原子或甲基，m为1〜3的整数，（d）为2〜10重量％％的含羧基的可聚合不饱和单体，（e）5〜20重量％％的含羟基的可聚不饱和单体，和（f）0〜77.9重量％％的其它可聚不饱和单体，（B）2〜100重量份的金属薄片颜料; 以及使用该组合物形成面漆的方法。

4. 发明授权

US5747572A Releasable aqueous coating composition and method of temporarily protecting finished coating film on automobile body by use of the same 失效
标题翻译：可拆卸的水性涂料组合物及其使用方法暂时保护汽车车身上的成品涂膜
公开(公告)号：US5747572A
公开(公告)日：1998-05-05
申请号：US750598
申请日：1996-12-19
申请人： Seiji Kashiwada , Shouji Takahashi , Hiroshi Inoue , Kenya Suzuki , Hiromi Harakawa , Fumiaki Nakao
发明人： Seiji Kashiwada , Shouji Takahashi , Hiroshi Inoue , Kenya Suzuki , Hiromi Harakawa , Fumiaki Nakao
IPC分类号： C09D5/20 , C09D133/06 , C08K5/54
CPC分类号： C09D5/20 , C09D133/062
摘要： The present invention relates to a releasable aqueous coating composition containing (A) a resin dispersion containing a carbonyl group-containing copolymer aqueous dispersion and a polyhydrazide compound in such a ratio that an amount of hydrazide group is in the range of 0.02 to 3.0 equivalents per one equivalent of carbonyl group in the emulsion particle, and (B) a release assistant; and a method of temporarily protecting a finished coating film of an automobile body, which method comprises coating said coating composition onto a surface of a finished cured coating film coated onto the automobile body.
摘要翻译： PCT No.PCT / JP96 / 01167 Sec。 371 1996年12月19日第 102（e）1996年12月19日PCT PCT 1996年4月26日PCT公布。公开号WO96 / 36671 日期：1996年11月21日本发明涉及一种可剥离水性涂料组合物，其含有（A）含有含羰基的共聚物水分散体和聚酰肼化合物的树脂分散体，其比例为酰肼基的量在乳剂颗粒中每一当量羰基为0.02至3.0当量，和（B）释放助剂; 以及临时保护汽车车体的成品涂膜的方法，该方法包括将涂布组合物涂布在涂覆在汽车车身上的完成的固化涂膜的表面上。

5. 发明授权

US5322865A Aqueous color paint compositions and coating method using same 失效
标题翻译：水性彩色油漆组合物及其涂布方法
公开(公告)号：US5322865A
公开(公告)日：1994-06-21
申请号：US10397
申请日：1993-01-28
申请人： Hiroshi Inoue , Hiromi Harakawa , Akira Kasari , Kenya Suzuki , Yoshinori Kato
发明人： Hiroshi Inoue , Hiromi Harakawa , Akira Kasari , Kenya Suzuki , Yoshinori Kato
IPC分类号： B05D7/14 , B05D7/00 , B05D7/24 , C08F283/01 , C08L67/00 , C08L67/06 , C09D133/06 , C09D167/06 , C08F2/22 , C08L33/08 , C08L33/10
CPC分类号： B05D7/532 , C09D133/066 , C09D167/06 , B05D2502/00 , C08L67/06
摘要： An aqueous color paint composition comprising(I) an aqueous dispersion of acrylic polymer fine particles,(II) a modified polyester resin aqueous dispersion obtained by neutralizing, with a basic substance, a modified polyester resin formed by polymerizing (A) a radical-polymerizable unsaturated group-containing polyester resin and (B) a mixture of an ethylenically unsaturated carboxylic acid and another copolymerizable unsaturated monomer and having an acid value of 8 to 200 and a hydroxyl value of 30 to 300, and dispersing the resulting resin in an aqueous dispersion medium,(III) a crosslinking agent, and(IV) a color pigment.The composition is, even if high-solid, good in coatability and excellent in smoothness of the coated film. It is therefore quite suitable as a high-solid base coat composition when coating an outside plate, etc. of automobiles, two-wheelers, electric appliances, etc. requiring beautiful appearance.
摘要翻译：一种含水彩色涂料组合物，其包含（I）丙烯酸类聚合物细颗粒的水性分散体，（II）通过用碱性物质中和（A）可自由基聚合的不饱和基团的聚酯树脂和（B）烯键式不饱和羧酸和另一种可共聚的不饱和单体的混合物，其酸值为8〜200，羟基值为30〜300，并将得到的树脂分散在水分散体介质，（III）交联剂，和（IV）着色颜料。组合物即使高固体，涂布性好，涂膜的平滑性也优异。因此，在涂装需要美观的汽车，二轮车，电器等的外板等时，作为高固体底涂层组合物是非常合适的。

6. 发明授权

US07838076B2 Thermosetting aqueous paint composition 有权
标题翻译：热固性水性漆组合物
公开(公告)号：US07838076B2
公开(公告)日：2010-11-23
申请号：US11662134
申请日：2005-09-07
申请人： Shuichi Nakahara , Hiromi Harakawa
发明人： Shuichi Nakahara , Hiromi Harakawa
IPC分类号： C08G63/02 , B05D3/00
CPC分类号： C09D5/02 , B05D3/0218 , B05D7/546 , B05D2202/00 , B05D2350/10 , B05D2451/00 , B05D2504/00 , B05D2508/00 , B05D2601/28 , C08G63/42 , C08G63/685 , C08G63/91 , C08K5/0025 , C08K5/29 , C08K5/34922 , C08L33/04 , C08L75/04 , C09D167/00 , C08L2666/02 , B05D2401/32 , B05D2420/01 , B05D2420/02
摘要： The present invention discloses a thermosetting aqueous paint, comprising an oligomer (A-1), having a specific acid value, hydroxyl value and number average molecular weight, and obtained by reacting a compound having at least one hydroxyl group and at least one carboxyl group in a molecule thereof, a monoepoxide compound having a long-chain hydrocarbon group, and as necessary, a polyvalent carboxylic acid and/or polyvalent carboxylic acid anhydride, and/or a polyester resin (A-2) obtained by further reacting a polyvalent carboxylic acid and/or a polyvalent carboxylic acid anhydride and/or a polyisocyanate compound with the oligomer, and a crosslinking agent (B); and also discloses a method for forming a paint film using this paint.
摘要翻译：本发明公开了一种热固性水性涂料，其包含具有特定酸值，羟基值和数均分子量的低聚物（A-1），并且通过使具有至少一个羟基的化合物和至少一个羧基在其分子中，具有长链烃基的单环氧化合物和必要的多元羧酸和/或多元羧酸酐，和/或通过使多元羧酸进一步反应得到的聚酯树脂（A-2）酸和/或多价羧酸酐和/或多异氰酸酯化合物和交联剂（B）; 并且还公开了使用这种涂料形成漆膜的方法。

7. 发明申请

US20070283852A1 Coating composition for cans 失效
标题翻译：罐头涂料组合物
公开(公告)号：US20070283852A1
公开(公告)日：2007-12-13
申请号：US11727176
申请日：2007-03-23
申请人： Masaaki Saika , Hideki Matsuda , Yuuichi Inada , Naoki Horike , Sumio Noda , Hideki Masuda , Keiichi Shimizu , Hiromi Harakawa
发明人： Masaaki Saika , Hideki Matsuda , Yuuichi Inada , Naoki Horike , Sumio Noda , Hideki Masuda , Keiichi Shimizu , Hiromi Harakawa
IPC分类号： C08F20/32
CPC分类号： C08G59/1461 , C08K3/30 , C08L33/064 , C08L63/00 , C09D5/024 , C09D7/43 , C09D7/65 , C09D7/67 , C09D7/68 , C09D151/08 , C09D163/00 , C08L2666/02 , C08L2666/04
摘要： The present invention provides a coating composition for cans comprising 100 parts by mass of a neutralized acrylic resin-modified epoxy resin (A), and from 1 to 50 parts by mass of anionic polymer crosslinked fine particles (B), (A) and (B) being dispersed in an aqueous medium, wherein the anionic polymer fine particles (B) are polymer fine particles comprising a polymer having an acid value of from 10 to 120 mg KOH/g and being produced by polymerizing radically polymerizable unsaturated monomers comprising from 2 to 30% by mass of a carboxyl group-containing radically polymerizable unsaturated monomer (b1), from 2 to 30% by mass of a polyvinyl compound (b2) and from 40 to 96% by mass of other radically polymerizable unsaturated monomer (b3) in the presence of water.
摘要翻译：本发明提供一种罐装用涂料组合物，其包含100质量份中和的丙烯酸树脂改性环氧树脂（A）和1至50质量份阴离子聚合物交联的细颗粒（B），（A）和（ B）分散在水性介质中，其中阴离子聚合物细颗粒（B）是包含酸值为10至120mg KOH / g的聚合物的聚合物细颗粒，并且通过聚合自由基聚合的不饱和单体制备，包含2 〜30质量％的含羧基的自由基聚合性不饱和单体（b1），2-30质量％的聚乙烯基化合物（b2）和40〜96质量％的其他自由基聚合性不饱和单体（b3）在水的存在下。

8. 发明申请

US20090111935A1 Aqueous urethane resin compositions 审中-公开
标题翻译：水性聚氨酯树脂组合物
公开(公告)号：US20090111935A1
公开(公告)日：2009-04-30
申请号：US12289457
申请日：2008-10-28
申请人： Takeshi Fujii , Hiromi Harakawa
发明人： Takeshi Fujii , Hiromi Harakawa
IPC分类号： C08G18/08
CPC分类号： C08G18/0823 , C08G18/10 , C08G18/6266 , C08G18/755 , C08G18/758 , C09D175/04 , C08G18/3228
摘要： This invention offers an aqueous urethane resin composition which contains a urethane resin obtained through reaction of acrylic polyol formed by copolymerization of carbonyl functional group-containing unsaturated monomer, hydrophilic group-containing unsaturated monomer and, where necessary, still other unsaturated monomer; with polyisocyanate compound and, where necessary, carboxyl group-containing diol; can form film of excellent physical properties such as spreadability and flexibility; and becomes ambient temperature-curable when combined with a crosslinking agent.
摘要翻译：本发明提供一种水性聚氨酯树脂组合物，其含有通过使含有羰基官能团的不饱和单体，含有亲水性基团的不饱和单体和必要时的其它不饱和单体的共聚形成的丙烯酸多元醇反应得到的聚氨酯树脂; 与多异氰酸酯化合物，必要时含有羧基的二醇; 可以形成具有优异物理性质的膜，如铺展性和柔韧性; 并且当与交联剂组合时变成环境温度可固化的。

9. 发明申请

US20080268269A1 Production method of pigment-dispersing resin 有权
标题翻译：颜料分散树脂的生产方法
公开(公告)号：US20080268269A1
公开(公告)日：2008-10-30
申请号：US12081977
申请日：2008-04-24
申请人： Masami Kobata , Noriyuki Yamada , Hiromi Harakawa
发明人： Masami Kobata , Noriyuki Yamada , Hiromi Harakawa
IPC分类号： B32B27/28 , C08G75/02 , C08L85/02 , B05D3/02
CPC分类号： C09D5/028 , C09D17/002 , C09D133/066 , C09D133/14 , Y10T428/31855
摘要： This invention provides a method for producing a pigment-dispersing resin which contains divalent group(s) represented by a general formula (I): (in which R1 stands for C1-10 alkylene group, m is an integer of 1-30, and the m recurring units, may be the same or different), phosphoric acid group(s) and/or sulfonic acid group(s), characterized by copolymerizing a polymerizable unsaturated monomeric mixture in a reaction solvent containing at least 30 mass %, based on the total mass of the reaction solvent, of an organic solvent having no hydroxyl group and having a solubility in 20° C. water of at least 100 mass %.
摘要翻译：本发明提供一种颜料分散树脂的制造方法，该颜料分散树脂含有由通式（I）表示的二价基团：（其中R 1代表C 1-10 - /亚烷基，m为1-30的整数，m个重复单元可以相同或不同），磷酸基和/或磺酸基，其特征在于使可聚合的不饱和单体混合物在含有至少30质量％的反应溶剂中，基于反应溶剂的总质量，在20℃的水中不具有羟基并且具有至少100质量％的溶解度的有机溶剂。

10. 发明授权

US5280054A Coating composition for use in hydrophilic treatment comprising an organic-inorganic composite reaction product 失效
标题翻译：用于亲水处理的涂料组合物，包括有机 - 无机复合反应产物
公开(公告)号：US5280054A
公开(公告)日：1994-01-18
申请号：US933180
申请日：1992-08-21
申请人： Shigeo Sakai , Naokazu Takeuchi , Tatsuyuki Kinoshita , Masateru Hayashi , Hiroshi Inoue , Hiromi Harakawa
发明人： Shigeo Sakai , Naokazu Takeuchi , Tatsuyuki Kinoshita , Masateru Hayashi , Hiroshi Inoue , Hiromi Harakawa
IPC分类号： B05D7/14 , C08F2/44 , C08J7/04 , C09D151/10 , C09D167/02 , F28F1/12 , F28F1/32 , C08K3/34 , C08L67/00
CPC分类号： C09D151/10 , C09D167/025
摘要： A coating composition for use in a hydrophilic treatment comprising (A) an organic-inorganic composite reaction product prepared by a process which comprises reacting 100 parts by weight, as the solid content, of (i) a water-dispersible silica with 0.1 to 10 parts by weight of (ii) a polymerizable vinylsilane monomer containing hydrolyzable alkoxysilane group to form an aqueous polymerizable vinyl group-containing silica dispersion and then reacting the aqueous polymerizable vinyl group-containing silica dispersion with (iii) a mixture of polymerizable unsaturated monomers other than the above (ii); (B) a curing agent and (C) a hydroxyl group-containing polyester resin, the ratio of the component (A) to the component (B) being in the range of 99 to 50:1 to 50 as the solid content weight ratio, and the amount of the component (C) being in the range of 5 to 60% by weight based on the solid content in the composition comprising the component (A), (B) and (C); a hydrophilic-treating method; and hydrophilically treated heat exchanger fins.
摘要翻译：一种用于亲水处理的涂料组合物，其包含（A）通过以下方法制备的有机 - 无机复合反应产物，该产物包括使100重量份的固体含量与（i）水分散性二氧化硅与0.1至10 （ii）含有可水解烷氧基硅烷基的可聚合乙烯基硅烷单体，形成含水可聚合乙烯基二氧化硅分散体，然后使含水可聚合乙烯基二氧化硅分散体与（iii）除可聚合的不饱和单体之外的可聚合不饱和单体的混合物上述（ii）; （B）固化剂和（C）含羟基的聚酯树脂，作为固体成分重量比，成分（A）与成分（B）的比例在99〜50:1〜50的范围内（A），（B）和（C）的组合物中的固体成分的含量为5〜60重量％的范围; 亲水处理方法; 和亲水处理的热交换器翅片。

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