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1. 发明授权

US07045321B2 POLYHYDROXYALKANOATE CONTAINING UNIT WITH PHENYLSULFANYL STRUCTURE IN THE SIDE CHAIN, PROCESS FOR ITS PRODUCTION, CHARGE CONTROL AGENT, TONER BINDER AND TONER WHICH CONTAIN NOVEL POLYHYDROXYALKANOATE, AND IMAGE-FORMING METHOD AND IMAGE-FORMING APPARATUS WHICH MAKE USE OF THE TONER 失效
标题翻译：含有侧链中的酚醛结构的聚羟基烷酸酯单体，其生产方法，充电控制剂，含有新型聚羟基烷基酯的调色剂和调色剂，以及使用该调色剂的图像形成方法和成像装置
公开(公告)号：US07045321B2
公开(公告)日：2006-05-16
申请号：US10084172
申请日：2002-02-28
申请人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
发明人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
IPC分类号： C12P11/00 , C12P13/00 , C08G63/02
CPC分类号： G03G9/08755 , C08G63/6882 , C12P7/625 , C12P11/00 , G03G9/08791 , G03G9/09733 , G03G9/09775
摘要： A polyhydroxyalkanoate characterized by having in the molecule a unit represented by Chemical Formula (1): wherein n may assume any one integral value within the range of from 1 to 8. Also disclosed are a process for producing the polyhydroxyalkanoate by the use of a microorganism having the ability to produce the polyhydroxyalkanoate and accumulate it in the bacterial body; a charge control agent, a toner binder and a toner which contain this polyhydroxyalkanoate; and an image-forming method and an image-forming apparatus which make use of the toner.
摘要翻译：公开了在分子中具有由化学式（1）表示的单元的聚羟基链烷酸酯。其中R选自氢原子，卤原子，CN，NO 2，COOR'，SO 2 R“，CH 3，C 2 H 5，C 3 H 7，C（CH 3）2 H和C（CH 3）3; 其中R'是H，Na，K，CH3或C2H5，R“是OH，ONa，OK，卤素原子，OCH3或OC2H5; x是任意选自1至8的整数; 条件是排除了具有氢原子作为R的聚羟基链烷酸酯，并且所有单元中的x均为2或4.还公开了通过使用具有生产聚羟基链烷酸酯的能力的微生物来生产聚羟基链烷酸酯并累积它在细菌体内

2. 发明授权

US06911521B2 Polyhydroxyalkanoate that comprises unit having substituted or unsubstituted (phenylmethyl) sulfanyl structure in side chain thereof and process for producing the same 失效
标题翻译：包含在侧链具有取代或未取代（苯基甲基）硫烷基结构的单元的聚羟基链烷酸酯及其制备方法
公开(公告)号：US06911521B2
公开(公告)日：2005-06-28
申请号：US10157142
申请日：2002-05-30
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
IPC分类号： C08G63/06 , C08G63/02 , C08G63/688 , C08G63/78 , C12P7/62 , C12P11/00
CPC分类号： C12P11/00 , C08G63/6882 , C12P7/625
摘要： A polyhydroxyalkanoate that comprises a unit represented by the following chemical formula (1): wherein R1 is a substituent of an aromatic ring selected from the group consisting of H, CH3, C2H5, CH3CH2CH2, (CH3)2CH, (CH3)3C, a halogen atom, CN, NO2, COOR′, and SO2R″, wherein R′ is selected from the group consisting of H, Na, K, CH3, and C2H5, and R″ is selected from the group consisting of OH, a halogen atom, ONa, OK, OCH3, and OC2H5; and x represents an integer of 1 to 8 being the same or different each other in the polyhydroxyalkanoate. A method for producing the polyhydroxyalkanoate is also provided.
摘要翻译：一种聚羟基链烷酸酯，其包含由以下化学式（1）表示的单元：其中R1是选自H，CH 3，C 2， CH 3，CH 3，CH 2，CH 2，CH 3，CH 3，CH 3，CH 3，）CH 2（CH 3）3 C，卤素原子，CN，NO 2，COOR' ，和SO 2 R“，其中R'选自H，Na，K，CH 3，和C 2 H 5，并且R“选自OH，卤素原子，ONa，OK，OCH 3和OC 2， 5 H 5; x表示在聚羟基链烷酸酯中相同或不同的1〜8的整数。还提供了生产聚羟基链烷酸酯的方法。

3. 发明授权

US06808907B2 Method and apparatus for producing polyhydroxyalkanoate 失效
标题翻译：聚羟基链烷酸酯的制备方法和装置
公开(公告)号：US06808907B2
公开(公告)日：2004-10-26
申请号：US10105332
申请日：2002-03-26
申请人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Takashi Kenmoku
发明人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Takashi Kenmoku
IPC分类号： C12P762
CPC分类号： C12P7/625 , C12M47/06
摘要： The present invention provides a method for producing highly purified polyhydroxyalkanoate (PHA) with high yield, by removing cell components other than PHA from cells containing PHA. Moreover, the present invention provides a method for simply removing or reducing chlorine remained in the collected PHA particles, when a treatment with an oxidizing agent containing hypochlorite is performed in the production of PHA as described above. One of the above-described methods comprises a step of treating cells containing polyhydroxyalkanoate with an oxidizing agent containing at least hypochlorite, a step of separating the treated cells into a water-soluble fraction and a water-insoluble fraction, and a step of reducing chlorine remained in the water-insoluble fraction. The step of reducing chlorine may be a step of washing the water-insoluble fraction with a hot water, thiosulfate solution or polar solvent solution containing at least an organic polar solvent in which polyhydroxyalkanoate is insoluble.
摘要翻译：本发明提供了通过从含有PHA的细胞中除去PHA以外的细胞成分而以高产率生产高纯度聚羟基链烷酸酯（PHA）的方法。此外，本发明提供了如上所述在生产PHA中进行含有次氯酸盐的氧化剂的处理时，简单地除去或还原所收集的PHA颗粒中残留的氯的方法。上述方法之一包括用至少含有次氯酸盐的氧化剂处理含有聚羟基链烷酸酯的细胞的步骤，将经处理的细胞分离成水溶性级分和水不溶性级分的步骤以及还原氯保留在水不溶性部分中。还原氯的步骤可以是用至少含有聚羟基链烷酸酯不溶的有机极性溶剂的热水，硫代硫酸盐溶液或极性溶剂溶液洗涤水不溶性部分的步骤。

4. 发明授权

US07408017B2 Polyhydroxyalkanoate containing unit with phenylsulfanyl structure in the side chain, process for its production, charge control agent, toner binder and toner which contain novel polyhydroxyalkanoate, and image forming method and image-forming apparatus which make use of the toner 失效
标题翻译：在侧链中具有苯基硫烷基结构的聚羟基链烷酸酯单元，其制备方法，电荷控制剂，调色剂粘合剂和含有新型聚羟基链烷酸酯的调色剂，以及使用调色剂的成像方法和图像形成装置
公开(公告)号：US07408017B2
公开(公告)日：2008-08-05
申请号：US11155599
申请日：2005-06-20
申请人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
发明人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
IPC分类号： C08G63/688
CPC分类号： G03G9/08755 , C08G63/6882 , C12P7/625 , C12P11/00 , G03G9/08791 , G03G9/09733 , G03G9/09775
摘要： A polyhydroxyalkanoate is disclosed which has in the molecule a unit represented by Chemical Formula (1). wherein R is arbitrarily selected from a hydrogen atom, a halogen atom, CN, NO2, COOR′, SO2R″, CH3, C2H5, C3H7, C(CH3)2H and C(CH3)3; where R′ is H, Na, K, CH3 or C2H5, and R″ is OH, ONa, OK, a halogen atom, OCH3 or OC2H5; and x is an integer arbitrarily selected from 1 to 8; with the proviso that a polyhydroxyalkanoate is excluded which has a hydrogen atom as R and x in all the units is 2 or 4. Also disclosed is a process for producing the polyhydroxyalkanoate by the use of a microorganism having the ability to produce the polyhydroxyalkanoate and accumulate it in the bacterial body.
摘要翻译：公开了在分子中具有由化学式（1）表示的单元的聚羟基链烷酸酯。其中R可以任选地选自氢原子，卤原子，CN，NO 2，COOR'，SO 2 R“，CH 3 C 2 H 3，C 3 H 3，C（CH 3）3 H 3，C 3 H 3， 2）H和C（CH 3 3）3。其中R'是H，Na，K，CH 3或C 2 H 5，并且R“是OH，ONa，OK，卤素原子，OCH 3或OC 2 H 5; x是任意选自1至8的整数; 条件是排除了具有氢原子作为R的聚羟基链烷酸酯，并且所有单元中的x均为2或4.还公开了通过使用具有生产聚羟基链烷酸酯的能力的微生物来生产聚羟基链烷酸酯并累积它在细菌体内。

5. 发明申请

US20050250191A1 Novel polyhydroxyalkanoate containing unit with phenylsulfanyl structure in the side chain, process for its production, charge control agent, toner binder and toner which contain novel polyhydroxyalkanoate, and image forming method and image-forming apparatus which make use of the toner 失效
标题翻译：在侧链中具有苯基硫烷基结构的新型聚羟基链烷酸酯单元，其制备方法，电荷控制剂，调色剂粘合剂和含有新型聚羟基链烷酸酯的调色剂，以及使用调色剂的成像方法和图像形成装置
公开(公告)号：US20050250191A1
公开(公告)日：2005-11-10
申请号：US11155599
申请日：2005-06-20
申请人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
发明人： Takeshi Imamura , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Tomohiro Suzuki , Tsutomu Honma , Takashi Kenmoku , Tatsuki Fukui
IPC分类号： C08G63/688 , C12P7/62 , C12P11/00 , G03G9/087 , G03G9/097 , C08G63/68
CPC分类号： G03G9/08755 , C08G63/6882 , C12P7/625 , C12P11/00 , G03G9/08791 , G03G9/09733 , G03G9/09775
摘要： A polyhydroxyalkanoate is disclosed which has in the molecule a unit represented by Chemical Formula (1). wherein R is arbitrarily selected from a hydrogen atom, a halogen atom, CN, NO2, COOR′, SO2R″, CH3, C2H5, C3H7, C(CH3)2H and C(CH3)3; where R′ is H, Na, K, CH3 or C2H5, and R″ is OH, ONa, OK, a halogen atom, OCH3 or OC2H5; and x is an integer arbitrarily selected from 1 to 8; with the proviso that a polyhydroxyalkanoate is excluded which has a hydrogen atom as R and x in all the units is 2 or 4. Also disclosed is a process for producing the polyhydroxyalkanoate by the use of a microorganism having the ability to produce the polyhydroxyalkanoate and accumulate it in the bacterial body.
摘要翻译：公开了在分子中具有由化学式（1）表示的单元的聚羟基链烷酸酯。其中R可以任选地选自氢原子，卤原子，CN，NO 2，COOR'，SO 2 R“，CH 3 C 2 H 3，C 3 H 3，C（CH 3）3 H 3，C 3 H 3， 2）H和C（CH 3 3）3。其中R'是H，Na，K，CH 3或C 2 H 5，并且R“是OH，ONa，OK，卤原子，OCH 3或OC 2 H 5; x是任意选自1至8的整数; 条件是排除了具有氢原子作为R的聚羟基链烷酸酯，并且所有单元中的x均为2或4.还公开了通过使用具有生产聚羟基链烷酸酯的能力的微生物来生产聚羟基链烷酸酯并累积它在细菌体内。

6. 发明申请

US20050054063A1 Method and apparatus for producing polyhydroxyalkanoate 审中-公开
标题翻译：聚羟基链烷酸酯的制备方法和装置
公开(公告)号：US20050054063A1
公开(公告)日：2005-03-10
申请号：US10940029
申请日：2004-09-14
申请人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Takashi Kenmoku
发明人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Takashi Kenmoku
IPC分类号： C08G63/90 , C12M1/00 , C12P7/62 , C12P7/26
CPC分类号： C12P7/625 , C12M47/06
摘要： The present invention provides a method for producing highly purified polyhydroxyalkanoate (PHA) with high yield, by removing cell components other than PHA from cells containing PHA. Moreover, the present invention provides a method for simply removing or reducing chlorine remained in the collected PHA particles, when a treatment with an oxidizing agent containing hypochlorite is performed in the production of PHA as described above. One of the above-described methods comprises a step of treating cells containing polyhydroxyalkanoate with an oxidizing agent containing at least hypochlorite, a step of separating the treated cells into a water-soluble fraction and a water-insoluble fraction, and a step of reducing chlorine remained in the water-insoluble fraction. The step of reducing chlorine may be a step of washing the water-insoluble fraction with a hot water, thiosulfate solution or polar solvent solution containing at least an organic polar solvent in which polyhydroxyalkanoate is insoluble.
摘要翻译：本发明提供了通过从含有PHA的细胞中除去PHA以外的细胞成分而以高产率生产高纯度聚羟基链烷酸酯（PHA）的方法。此外，本发明提供了如上所述在生产PHA中进行含有次氯酸盐的氧化剂的处理时，简单地除去或还原所收集的PHA颗粒中残留的氯的方法。上述方法之一包括用至少含有次氯酸盐的氧化剂处理含有聚羟基链烷酸酯的细胞的步骤，将经处理的细胞分离成水溶性级分和水不溶性级分的步骤以及还原氯保留在水不溶性部分中。还原氯的步骤可以是用至少含有聚羟基链烷酸酯不溶的有机极性溶剂的热水，硫代硫酸盐溶液或极性溶剂溶液洗涤水不溶性部分的步骤。

7. 发明授权

US06861496B2 Polyhydroxyalkonoate and method of producing same, and ω-(2-thienylsulfanyl) alkanoic acid and method of producing same 失效
标题翻译：聚羟基链烷酸酯及其制造方法，ω-（2-噻吩基硫烷基）链烷酸及其制造方法
公开(公告)号：US06861496B2
公开(公告)日：2005-03-01
申请号：US10641090
申请日：2003-08-15
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
IPC分类号： C08G63/60 , C07D333/34 , C08G63/68 , C08G63/688 , C12P7/62 , C12P11/00 , C12R1/38 , C08G63/02
CPC分类号： C12P7/625 , C07D333/34 , C08G63/6882 , C12P11/00 , Y10S435/874 , Y10S435/877
摘要： PHA containing a novel 3-hydroxy-thioalkanoic acid unit having a highly reactive thienyl group in a side chain thereof, and a method of producing the same are provided. Specifically, 5-(2-thienylsulfanyl) valeric acid represented by Chemical Formula [4] below and 6-(2-thienylsulfanyl) hexanoic acid represented by Chemical Formula [5] below are provided. Further, a method of producing PHA, comprising the step of collecting PHA from cells of a microorganism cultured in a medium containing the valeric acid or hexanoic acid, and a novel PHA represented by Chemical Formula [1] below are provided. (n denotes an integer of 1 to 9)
摘要翻译：提供了含有其侧链中具有高反应性噻吩基的新型3-羟基 - 硫代链烷酸单元的PHA及其制备方法。具体地，提供由下述化学式[4]表示的5-（2-噻吩基硫烷基）戊酸和由下述化学式[5]表示的6-（2-噻吩基硫烷基）己酸。此外，提供了一种制备PHA的方法，其包括从含有戊酸或己酸的培养基中培养的微生物的细胞和由下述化学式[1]表示的新型PHA收集PHA的步骤（n表示 1〜9的整数）

8. 发明授权

US06803444B2 Polyhydroxyalkanoate polyester having vinyl phenyl structure in the side chain and its production method 失效
标题翻译：侧链中具有乙烯基苯基结构的聚羟基链烷酸酯聚酯及其制备方法
公开(公告)号：US06803444B2
公开(公告)日：2004-10-12
申请号：US10084167
申请日：2002-02-28
申请人： Tomohiro Suzuki , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tsutomu Honma , Takashi Kenmoku
发明人： Tomohiro Suzuki , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tsutomu Honma , Takashi Kenmoku
IPC分类号： C08G6306
CPC分类号： C12P7/625 , C08G63/06 , Y10S435/874 , Y10S435/877
摘要： Polyhydroxyalkanoate type polyester that comprises one unit % or more of 3-hydroxy-&ohgr;-(4-vinylphenyl)alkanoic acid units. A microbial production method is also provided.
摘要翻译：包含一个单元％以上的3-羟基-ω-（4-乙烯基苯基）链烷酸单元的聚羟基链烷酸酯型聚酯。还提供微生物生产方法。

9. 发明授权

US06686439B2 Polyhydroxyalkanoate and method of producing same, and &ohgr;-(2-thienylsulfanyl) alkanoic acid and method of producing same 失效
标题翻译：聚羟基链烷酸酯及其制造方法，ω-（2-噻吩基硫烷基）链烷酸及其制造方法
公开(公告)号：US06686439B2
公开(公告)日：2004-02-03
申请号：US10084168
申请日：2002-02-28
申请人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
发明人： Takashi Kenmoku , Etsuko Sugawa , Tetsuya Yano , Tsuyoshi Nomoto , Takeshi Imamura , Tomohiro Suzuki , Tsutomu Honma
IPC分类号： C08G6302
CPC分类号： C12P7/625 , C07D333/34 , C08G63/6882 , C12P11/00 , Y10S435/874 , Y10S435/877
摘要： PHA containing a novel 3-hydroxy-thioalkanoic acid unit having a highly reactive thienyl group in a side chain thereof, and a method of producing the same are provided. Specifically, 5-(2-thienyl-sulfanyl)valeric acid represented by Chemical Formula [4] below and 6-(2-thienylsulfanyl)hexanoic acid represented by Chemical Formula [5] below are provided. Further, a method of producing PHA, comprising the step of collecting PHA from cells of a microorganism cultured in a medium containing the valeric acid or hexanoic acid, and a novel PHA represented by Chemical Formula [1] below are provided. (n denotes an integer of 1 to 9)
摘要翻译：提供了含有其侧链中具有高反应性噻吩基的新型3-羟基 - 硫代链烷酸单元的PHA及其制备方法。具体地，提供由下述化学式[4]表示的5-（2-噻吩基 - 硫烷基）戊酸和由下述化学式[5]表示的6-（2-噻吩基硫烷基）己酸。此外，提供了一种制备PHA的方法，其包括从含有戊酸或己酸的培养基中培养的微生物的细胞和由下述化学式[1]表示的新型PHA收集PHA的步骤（n表示 1〜9的整数）

10. 发明授权

US07078200B2 Method for manufacturing a polyhydroxyalkanoate 失效
标题翻译：聚羟基链烷酸酯的制造方法
公开(公告)号：US07078200B2
公开(公告)日：2006-07-18
申请号：US10603996
申请日：2003-06-26
申请人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Takeshi Imamura , Takashi Kenmoku
发明人： Tsutomu Honma , Etsuko Sugawa , Tetsuya Yano , Takeshi Imamura , Takashi Kenmoku
IPC分类号： C12P7/62 , C08G63/06 , C08G63/78
CPC分类号： C12P7/625 , C08G63/06 , C08G63/6822 , C08G63/6852
摘要： A method for producing a polyhydroxyalkanoate using a microorganism capable of substantially reducing unintended monomer units and obtaining the polyhydroxyalkanoate in a high yield. A microorganism capable of synthesizing a novel polyhydroxyalkanoate having 3-hydroxy-substituted benzoylalkanoic acid as a monomer unit, using a substituted benzoylalkanoic acid as a material, is cultured in a medium containing a substituted benzoylalkanoic acid. Then, the polyhydroxyalkanoate produced in the cultured bacteria is extracted and recovered.
摘要翻译：使用能够显着降低非预期的单体单元并以高产率获得聚羟基链烷酸酯的微生物制备聚羟基链烷酸酯的方法。在含有取代的苯甲酰基链烷酸的培养基中培养能够以取代的苯甲酰基链烷酸为原料合成具有3-羟基取代的苯甲酰基链烷酸作为单体单元的新型聚羟基链烷酸酯的微生物。然后，提取并回收在培养细菌中产生的聚羟基链烷酸酯。

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