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1. 发明授权

US08647741B2 Polypropylene fiber, method of producing the same and utilization of the same 有权
标题翻译：聚丙烯纤维，其生产方法和使用方法相同
公开(公告)号：US08647741B2
公开(公告)日：2014-02-11
申请号：US12532898
申请日：2008-03-24
申请人： Takashi Katayama , Yoshihiro Iwasaki , Masakazu Nishiyama
发明人： Takashi Katayama , Yoshihiro Iwasaki , Masakazu Nishiyama
IPC分类号： D02G3/00
CPC分类号： D01F6/06 , B29K2023/12 , B29K2223/12 , B29L2031/707 , C04B16/0633 , C04B28/02 , C08L23/10 , D02J1/22 , D04H1/4291 , D07B1/02 , D07B2201/2006 , D07B2201/2007 , D07B2201/2009 , D07B2205/201 , Y10T428/29 , Y10T428/2913 , Y10T428/2976 , Y10T442/10 , Y10T442/3854 , Y10T442/40 , Y10T442/674 , C08L2666/02 , D07B2801/10
摘要： The present invention aims to provide a polypropylene fiber (PP fiber) excellent in strength, heat resistance, and water-absorption properties, a method of producing the same, and a hydraulic composition, a rope, a sheet-shaped fiber structure, and a composite material with an organic polymer each using the PP fiber. The present invention provides: a PP fiber having a fiber having a fiber strength of 7 cN/dtex or more and having either or both of (i) DSC properties such that the endothermic peak shape by DSC is a single shape having a half width of 10° C. or lower and the melt enthalpy change (AH) is 125 J/ g and (ii) irregular properties such that the single fiber fineness is 0.i to 3 dtex and irregularities are formed on the surface.
摘要翻译：本发明的目的在于提供强度，耐热性和吸水性优异的聚丙烯纤维（PP纤维）及其制造方法，水硬性组合物，绳索，片状纤维结构体和复合材料与各自使用PP纤维的有机聚合物。本发明提供：具有纤维强度为7cN / dtex以上的纤维的PP纤维，并且具有（i）DSC性质中的任一种或两者，使得DSC的吸热峰形状为具有半数宽度的单一形状 10℃以下，熔体焓变（AH）为125J / g，（ii）单纤维纤度为0.3〜11分的不规则性，表面形成凹凸。

2. 发明申请

US20100173547A1 POLYPROPYLENE FIBER, METHOD OF PRODUCING THE SAME AND UTILIZATION OF THE SAME 有权
标题翻译：聚丙烯纤维，其制造方法及其利用
公开(公告)号：US20100173547A1
公开(公告)日：2010-07-08
申请号：US12532898
申请日：2008-03-24
申请人： Takashi Katayama , Yoshihiro Iwasaki , Masakazu Nishiyama
发明人： Takashi Katayama , Yoshihiro Iwasaki , Masakazu Nishiyama
IPC分类号： B32B27/12 , D02G3/02 , D02G3/22 , D01D5/12 , C08F110/06
CPC分类号： D01F6/06 , B29K2023/12 , B29K2223/12 , B29L2031/707 , C04B16/0633 , C04B28/02 , C08L23/10 , D02J1/22 , D04H1/4291 , D07B1/02 , D07B2201/2006 , D07B2201/2007 , D07B2201/2009 , D07B2205/201 , Y10T428/29 , Y10T428/2913 , Y10T428/2976 , Y10T442/10 , Y10T442/3854 , Y10T442/40 , Y10T442/674 , C08L2666/02 , D07B2801/10
摘要： The present invention aims to provide a polypropylene fiber (PP fiber) excellent in strength, heat resistance, and water-absorption properties, a method of producing the same, and a hydraulic composition, a rope, a sheet-shaped fiber structure, and a composite material with an organic polymer each using the PP fiber. The present invention provides: a PP fiber having a fiber strength of 7 cN/dtex or more and having either or both of (i) DSC properties such that the endothermic peak shape by DSC is a single shape having a half width of 10° C. or lower and the melt enthalpy change (AH) is 125 J/g and (ii) irregular properties such that the single fiber fineness is 0.1 to 3 dtex and irregularities are formed on the surface, the irregularities having an average interval of 6.5 to 20 μm and an average height of 0.35 to 1 μm as a result of alternate presence of a protruded portion having a large diameter and a non-protruded portion having a small diameter along its fiber axis; a method of producing the PP fiber by pre-drawing an undrawn PP fiber having an IPF of 94% or more at 120 to 150° C. at a drawing magnification of 3 to 10 times, and then post-drawing the resultant at 170 to 190° C. and a drawing magnification of 1.2 to 3.0 times under the conditions of a deformation rate of 1.5 to 15 times/min and a draw tension of 1.0 to 2.5 cN/dtex; and a hydraulic composition, a rope, a sheet-shaped fiber structure, and a composite material with an organic polymer each using the PP fiber.
摘要翻译：本发明的目的在于提供强度，耐热性和吸水性优异的聚丙烯纤维（PP纤维）及其制造方法，水硬性组合物，绳索，片状纤维结构体和复合材料与各自使用PP纤维的有机聚合物。本发明提供一种PP纤维，其纤维强度为7cN / dtex以上，并且具有（i）DSC性质中的任一种或两者，使得DSC的吸热峰形状为半宽度为10℃的单一形状或更低，熔体焓变（AH）为125J / g，（ii）单纤维纤度为0.1〜3dtex的不规则性，表面形成凹凸，平均间隔为6.5〜由于交替存在具有大直径的突起部分和沿其纤维轴线具有小直径的非突出部分的结果，平均高度为0.35至1μm，平均高度为0.35μm至1μm。通过将拉伸倍数为3〜10倍，在120〜150℃下预拉伸IPF为94％以上的未拉伸的PP纤维，然后在170℃下拉伸所得的PP纤维， 190℃，拉伸倍率为1.5〜15次/分钟，拉伸张力为1.0〜2.5cN / dtex的条件下的1.2〜3.0倍。和水硬性组合物，绳索，片状纤维结构体和具有各自使用PP纤维的有机聚合物的复合材料。

3. 发明申请

US20090184312A1 BENZOFLUORENE COMPOUND AND USE THEREOF 有权
标题翻译：苯并噻唑化合物及其用途
公开(公告)号：US20090184312A1
公开(公告)日：2009-07-23
申请号：US12296622
申请日：2007-04-12
申请人： Masakazu Nishiyama , Naoki Matsumoto , Takanori Miyazaki , Takeshi Kanbara
发明人： Masakazu Nishiyama , Naoki Matsumoto , Takanori Miyazaki , Takeshi Kanbara
IPC分类号： H01L51/00 , C07C211/00
CPC分类号： C07C211/61 , C07C2603/40 , C07C2603/94 , C07C2603/97 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , H01L51/0054 , H01L51/006 , H01L51/5012 , H01L51/5048 , H01L51/5088 , H05B33/14
摘要： A novel material having high hole-transporting ability and a high glass transition temperature and having long-lasting durability is obtained.A benzofluorene compound represented by formula (1) is used. (In the formula, M is a substituted or unsubstituted aryl group having 6-40 carbon atoms or a substituted or unsubstituted heteroaryl group having 5-40 carbon atoms; Ar1 to Ar4 each independently is a substituted or unsubstituted aryl group having 6-40 carbon atoms or a substituted or unsubstituted heteroaryl group having 5-40 carbon atoms, provided that at least one of Ar1 to Ar4 is a substituent represented by any of the following formulae (2) to (5); and p is an integer of 0-2.) (In the formulae, R1 to R4 each independently is a hydrogen atom, a halogen atom, a substituted or unsubstituted amino group, a linear, branched, or cyclic alkyl group, a linear, branched, or cyclic alkoxy group, a substituted or unsubstituted aryl group having 6-40 carbon atoms, or a substituted or unsubstituted aryloxy group having 6-40 carbon atoms, provided that R1 and R2 may be bonded to each other to form a ring.)
摘要翻译：获得具有高空穴传输能力和高玻璃化转变温度并具有持久耐久性的新型材料。使用由式（1）表示的苯并芴化合物。（式中，M为取代或未取代的碳原子数为6〜40的芳基或取代或未取代的碳原子数为5〜40的杂芳基，Ar 1〜Ar 4各自独立地为取代或未取代的碳原子数为6〜40的芳基原子或具有5-40个碳原子的取代或未取代的杂芳基，条件是Ar 1至Ar 4中的至少一个为由下式（2）至（5）中的任一个表示的取代基; p为0〜（式中，R 1〜R 4各自独立地为氢原子，卤素原子，取代或未取代的氨基，直链状，支链状或环状的烷基，直链状，支链状或环状的烷氧基，取代或未取代的具有6-40个碳原子的芳基或取代或未取代的具有6-40个碳原子的芳氧基，条件是R 1和R 2可以彼此键合形成环。

4. 发明申请

US20080194878A1 Amine Compound Having Fluorene Group as Framework, Process for Producing the Amine Compound, and Use of the Amine Compound 有权
标题翻译：具有芴基作为骨架的胺化合物，生产胺化合物的方法和胺化合物的用途
公开(公告)号：US20080194878A1
公开(公告)日：2008-08-14
申请号：US10585945
申请日：2005-01-14
申请人： Masakazu Nishiyama , Naoki Matsumoto , Hisao Eguchi
发明人： Masakazu Nishiyama , Naoki Matsumoto , Hisao Eguchi
IPC分类号： C07C211/44
CPC分类号： C07D285/14 , C07C211/61 , C07D209/56 , C07D333/08 , C07D409/04 , C09B1/00 , C09B57/00 , C09B57/008 , Y10S428/917
摘要： Novel amine compounds that can be utilized as hole transport materials, hole injection materials or the like of organic electroluminescence devices, electrophotographic receptors or the like, and their production processes are provided.The novel amine compound is represented by the following general formula (1).In the formula, R1 and R2 each independently represents hydrogen atom, a linear, branched or cyclic alkyl group or alkoxy group, an aryl group, an aryloxy group or a halogen atom; Ar1 and Ar2 each independently represents a substituted or unsubstituted aryl group or heteroaryl group, and may form a nitrogen-containing heterocyclic ring together with the nitrogen atom bonded thereto; and Ar3 each independently represents a substituted or unsubstituted phenyl group, naphthyl group, biphenylyl group, terphenylyl group, anthryl group, fluorenyl group or pyridyl group (except for amino-substituted groups); and M represents a single bond, an arylene group or a heteroarylene group.
摘要翻译：提供了可用作有机电致发光器件，电子照相感应器等的空穴传输材料，空穴注入材料等的新型胺化合物及其制备方法。该新型胺化合物由以下通式（1）表示。在该式中，R 1和R 2各自独立地表示氢原子，直链，支链或环状的烷基或烷氧基，芳基，芳氧基或卤素原子; Ar 1和Ar 2各自独立地表示取代或未取代的芳基或杂芳基，并可与其键合的氮原子一起形成含氮杂环; 和Ar 3各自独立地表示取代或未取代的苯基，萘基，联苯基，三联苯基，蒽基，芴基或吡啶基（氨基取代基除外）。 M表示单键，亚芳基或亚杂亚芳基。

5. 发明申请

US20070282111A1 Catalyst for producing arylamine and process for producing arylamine by means thereof 有权
标题翻译：用于制备芳基胺的催化剂及其制备方法
公开(公告)号：US20070282111A1
公开(公告)日：2007-12-06
申请号：US11806565
申请日：2007-06-01
申请人： Takanori Miyazaki , Masakazu Nishiyama , Naoki Matsumoto
发明人： Takanori Miyazaki , Masakazu Nishiyama , Naoki Matsumoto
IPC分类号： C07D233/56 , C07D231/12 , C07D209/04 , C07D209/82
CPC分类号： B01J31/24 , B01J2231/4283 , B01J2531/824 , C07C209/10 , C07C209/66 , C07C211/54
摘要： To provide a process for preparing an arylamine highly selectively and highly efficiently, which is also industrially superior without a fear of a side reaction when a strong base is employed. An aryl compound having an active group is reacted with an amine compound in the presence of a base by means of a catalyst for producing an arylamine which comprises a palladium compound having a tertiary phosphine group and a phase-transfer catalyst.
摘要翻译：提供一种高选择性和高效制备芳基胺的方法，当使用强碱时，它也在工业上优于无副反应的担心。具有活性基团的芳基化合物与胺化合物在碱的存在下通过用于制备包含具有叔膦基的钯化合物和相转移催化剂的芳基胺的催化剂进行反应。

6. 发明授权

US4886256A Vehicle suspension device with a coil spring embedded in an open cell foam 失效
标题翻译：具有螺旋弹簧的车辆悬挂装置嵌入开孔泡沫
公开(公告)号：US4886256A
公开(公告)日：1989-12-12
申请号：US761298
申请日：1985-07-29
申请人： Masakazu Nishiyama , Takeyoshi Shinbori , Hideo Yamamoto
发明人： Masakazu Nishiyama , Takeyoshi Shinbori , Hideo Yamamoto
IPC分类号： B60G11/52 , B60G15/07 , F16F3/12
CPC分类号： F16F3/12 , B60G11/52 , B60G15/07
摘要： A vehicle suspension device which suspends a vehicle body and a wheel, comprising a coil spring body having a predetermined number of coaxial turns, and a first cylinder and a second cylinder, each including a soft synthetic resin open-cell foam which is treated to be surging-proof and waterproof and which has a wall in which is embedded at least one turn located at each end of said coil spring body.
摘要翻译：一种悬挂车身和车轮的车辆悬挂装置，包括具有预定数量的同轴线圈的螺旋弹簧体，以及第一气缸和第二气缸，每个包括软合成树脂开孔泡沫，其被处理为防水和防水，并且其具有嵌入位于所述螺旋弹簧体的每个端部的至少一个转弯的壁。

7. 发明授权

US08097366B2 Alkaline battery separator comprising alkali-resistance synthetic fiber, fibrillated organic solvent-spun cellulose fiber and mercerized pulp, and alkaline primary battery 有权
标题翻译：碱性电池隔板，包括耐碱合成纤维，原纤化有机溶剂纺丝纤维素纤维和丝光纸浆，以及碱性一次电池
公开(公告)号：US08097366B2
公开(公告)日：2012-01-17
申请号：US11816714
申请日：2006-02-23
申请人： Toshimitsu Harada , Hisashi Nagi , Hiroyuki Kawai , Masakazu Nishiyama
发明人： Toshimitsu Harada , Hisashi Nagi , Hiroyuki Kawai , Masakazu Nishiyama
IPC分类号： H01M2/16
CPC分类号： H01M2/1633 , H01M2/1613 , H01M2/1626 , H01M6/06
摘要： An alkaline battery separator including 25 to 62% by mass of an alkali-resistance synthetic fiber, 5 to 25% by mass of a fibrillated organic solvent-spun cellulose fiber having a Canadian standard freeness value of 10 to 280 ml, and 33 to 50% by mass of a mercerized pulp having a Canadian standard freeness value of not less than 550 ml, wherein the fibrillated organic solvent-spun cellulose fiber intertwines with the mercerized pulp.
摘要翻译：碱性电池用隔膜，其含有25〜62质量％的耐碱合成纤维，5〜25质量％的加拿大标准游离度为10〜280ml的原纤化有机溶剂纺丝纤维素纤维，33〜50质量％质量％的具有加拿大标准游离度不低于550ml的丝光纸浆，其中原纤化有机溶剂纺丝纤维素纤维与丝光纸浆缠结。

8. 发明申请

US20090017385A1 ALKALINE BATTERY SEPARATOR AND ALKALINE PRIMARY BATTERY 有权
标题翻译：碱性电池分离器和碱性电池
公开(公告)号：US20090017385A1
公开(公告)日：2009-01-15
申请号：US11816714
申请日：2006-02-23
申请人： Toshimitsu Harada , Hisashi Nagi , Hiroyuki Kawai , Masakazu Nishiyama
发明人： Toshimitsu Harada , Hisashi Nagi , Hiroyuki Kawai , Masakazu Nishiyama
IPC分类号： H01M2/16
CPC分类号： H01M2/1633 , H01M2/1613 , H01M2/1626 , H01M6/06
摘要： An alkaline battery separator comprising an alkali-resistance synthetic fiber, a fibrillated organic solvent-spun cellulose fiber having a Canadian standard freeness value of 10 to 280 ml, and a mercerized pulp having a Canadian standard freeness value of not less than 550 ml is prepared. In the separator, the proportion of the alkali-resistance synthetic fiber, the proportion of the fibrillated organic solvent-spun cellulose fiber, and the proportion of the mercerized pulp relative to the total amount of the separator are respectively 25 to 62% by mass, 5 to 25% by mass, and 33 to 50% by mass, provided that the total amount of the separator is 100% by mass. The alkali-resistance synthetic fiber may comprise a polyvinyl alcohol-series fiber having an average fiber fineness of not more than 1 dtex. The alkaline battery separator may further comprise a polyvinyl alcohol-series binder in a proportion of 3 to 20% by mass relative to the total amount of the separator. The alkaline battery separator of the present invention may have a shrinkage by the area of not more than 3.5% after immersing in an aqueous solution of potassium hydroxide having a concentration of 40% by mass at 80° C. for 24 hours and a stiffness strength of not less than 2 N.
摘要翻译：制备碱性电池隔板，其包含耐碱合成纤维，加拿大标准游离度值为10〜280ml的原纤化有机溶剂纺丝纤维素纤维和加拿大标准游离度值不小于550ml的丝光纸浆。在隔板中，耐碱合成纤维的比例，原纤化有机溶剂纺丝纤维素纤维的比例和丝光纸浆的比例相对于隔膜的总量分别为25〜62质量％ 5〜25质量％，33〜50质量％，只要隔板的总量为100质量％即可。耐碱合成纤维可以包含平均纤维细度不超过1分特的聚乙烯醇系纤维。碱性电池隔板可以进一步包含相对于隔膜的总量为3〜20质量％的聚乙烯醇系粘合剂。本发明的碱性电池用隔膜在80℃下浸渍浓度为40质量％的氢氧化钾水溶液24小时后的收缩率为3.5％以下，其刚度强度不低于2 N.

9. 发明授权

US5380588A Polyvinyl alcohol-based synthetic fiber 失效
标题翻译：聚乙烯醇类合成纤维
公开(公告)号：US5380588A
公开(公告)日：1995-01-10
申请号：US902866
申请日：1992-06-23
申请人： Masakazu Nishiyama , Yasuhiro Harada , Akio Mizobe
发明人： Masakazu Nishiyama , Yasuhiro Harada , Akio Mizobe
IPC分类号： D06M11/55 , D06M13/123 , D06M13/127 , D02G3/00
CPC分类号： D06M13/123 , D06M11/55 , D06M13/127 , Y10T428/2913
摘要： Provided are polyvinyl alcohol-based synthetic fiber having excellent performances as a fiber for FRC that is prepared by autoclave curing and its very effective production processes. One of the processes comprises having a monoaldehyde or a dialdehyde or its acetalization product penetrate into the central region of a polyvinyl alcohol-based synthetic fiber at a first stage and then, at a second stage, effecting crosslinking reaction with a mixed solution containing a monoaldehyde and an acid. The other process comprises conducting acetalization with a bath containing 100 to 250 g/l of formaldehyde and 30 to 80 g/l of sulfuric acid at a temperature of 70.degree. to 100.degree. C. The processes can give a polyvinyl alcohol-based synthetic fiber having a strength of at least 11 g/d, a gel elasticity of at least 6.0.times.10.sup.-3 g/cm.multidot.d and a dissolution ratio of not more than 40% and being able to withstand an autoclave curing at 140.degree. C. which is necessary for securing the dimensional stability of the resulting cement products.
摘要翻译：本发明提供一种聚乙烯醇系合成纤维，其具有优异的性能，作为通过高压釜固化制备的FRC纤维及其非常有效的制备方法。其中一个方法包括在第一阶段使单醛或二醛或其缩醛产物渗入聚乙烯醇类合成纤维的中心区域，然后在第二阶段与含有单醛的混合溶液进行交联反应和酸。另一方法包括在70至100℃的温度下，用含有100至250g / l甲醛和30至80g / l硫酸的浴进行缩醛化。该方法可以得到基于聚乙烯醇的合成纤维具有至少11g / d的强度，至少6.0×10 -3 g / cm×d的凝胶弹性和不大于40％的溶解比，并且能够耐受140℃下的高压釜固化，这是必要的以确保所得水泥产品的尺寸稳定性。

10. 发明授权

US07803953B2 Catalyst for producing arylamine and process for producing arylamine by means thereof 有权
标题翻译：用于制备芳基胺的催化剂及其制备方法
公开(公告)号：US07803953B2
公开(公告)日：2010-09-28
申请号：US11806565
申请日：2007-06-01
申请人： Takanori Miyazaki , Masakazu Nishiyama , Naoki Matsumoto
发明人： Takanori Miyazaki , Masakazu Nishiyama , Naoki Matsumoto
IPC分类号： C07C209/10
CPC分类号： B01J31/24 , B01J2231/4283 , B01J2531/824 , C07C209/10 , C07C209/66 , C07C211/54
摘要： To provide a process for preparing an arylamine highly selectively and highly efficiently, which is also industrially superior without a fear of a side reaction when a strong base is employed. An aryl compound having an active group is reacted with an amine compound in the presence of a base by means of a catalyst for producing an arylamine which comprises a palladium compound having a tertiary phosphine group and a phase-transfer catalyst.
摘要翻译：提供一种高选择性和高效制备芳基胺的方法，当使用强碱时，它也在工业上优于无副反应的担心。具有活性基团的芳基化合物与胺化合物在碱的存在下通过用于制备包含具有叔膦基的钯化合物和相转移催化剂的芳基胺的催化剂进行反应。

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