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1. 发明授权

US5834404A Substituted bicycloheptanedione derivative and herbicide 失效
标题翻译：取代的双环庚二酮衍生物和除草剂
公开(公告)号：US5834404A
公开(公告)日：1998-11-10
申请号：US836285
申请日：1997-07-15
申请人： Takahiro Sagae , Masao Yamaguchi , Hiroyuki Adachi , Kazuyuki Tomida , Akihiro Takahashi , Takashi Kawana
发明人： Takahiro Sagae , Masao Yamaguchi , Hiroyuki Adachi , Kazuyuki Tomida , Akihiro Takahashi , Takashi Kawana
IPC分类号： A01N35/06 , A01N41/10 , C07C45/51 , C07C45/68 , C07C45/71 , C07C49/753 , C07C49/83 , C07C49/835 , C07C49/84 , C07C205/45 , C07C317/24 , C07C323/22 , C07D213/71 , A01N31/04 , A01N43/36 , C07C49/115 , C07D211/70
CPC分类号： C07D213/71 , A01N35/06 , A01N41/10 , C07C205/45 , C07C317/24 , C07C323/22 , C07C45/513 , C07C45/68 , C07C45/71 , C07C49/753 , C07C49/83 , C07C49/835 , C07C49/84 , C07C2102/20
摘要： The present invention is directed to substituted bicycloheptanedion e derivatives represented by a general formula �I!; ##STR1## wherein R represents C.sub.1 -C.sub.4 alkyl, R.sup.1 represents hydrogen, C.sub.1 -C.sub.10 alkyl, C.sub.2 -C.sub.4 alkenyl, C.sub.2 -C.sub.4 alkynyl, aralkyl, C.sub.2 -C.sub.4 haloalkynyl, C.sub.1 -C.sub.4 alkoxy C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 haloalkyl, C.sub.2 -C.sub.4 haloalkenyl, etc. and R.sup.2 represents optionally substituted phenyl or optionally substituted pyridyl, the salts thereof and herbicides comprising the same as the active ingredient.
摘要翻译： PCT No.PCT / JP95 / 02259 Sec。 371日期1997年7月15日 102（e）日期1997年7月15日PCT 1995年11月7日PCT PCT。公开号WO96 / 14285 日期：1996年5月17日本发明涉及由通式[I]表示的取代的双环庚烷二酮衍生物e衍生物。其中R表示C 1 -C 4烷基，R 1表示氢，C 1 -C 10烷基，C 2 -C 4烯基，C 2 -C 4炔基，芳烷基，C 2 -C 4卤代炔基，C 1 -C 4烷氧基C 1 -C 4烷基，C 1 -C 4卤代烷基，C 2 -C 4卤代烯基等，R 2表示任选取代的苯基或任选取代的吡啶基，其盐和除草剂与活性成分相同。

2. 发明授权

US6100421A Heterocycle-substituted benzene derivatives and herbicides 失效
标题翻译：杂环取代的苯衍生物和除草剂
公开(公告)号：US6100421A
公开(公告)日：2000-08-08
申请号：US359444
申请日：1999-07-22
申请人： Hiroyuki Adachi , Masao Yamaguchi , Takahiro Sagae , Masami Koguchi , Kazuyuki Tomita , Takashi Kawana , Akihiro Takahashi
发明人： Hiroyuki Adachi , Masao Yamaguchi , Takahiro Sagae , Masami Koguchi , Kazuyuki Tomita , Takashi Kawana , Akihiro Takahashi
IPC分类号： C07C317/44 , C07C321/00
CPC分类号： C07C317/44
摘要： The present invention is directed to a benzoic acid derivative methyl 3-formyl-4-methanesulfonyl-2-methylbenzoate. The compound is useful as a starting material for herbicide manufacture.
摘要翻译：本发明涉及苯甲酸衍生物3-甲酰基-4-甲磺酰基-2-甲基苯甲酸甲酯。该化合物可用作除草剂制备的起始原料。

3. 发明授权

US5948917A 3-(isoxazol-5-yl)-substituted benzoic acid derivative and method for production thereof 失效
标题翻译： 3-（异恶唑-5-基） - 取代苯甲酸衍生物及其制备方法
公开(公告)号：US5948917A
公开(公告)日：1999-09-07
申请号：US875548
申请日：1997-09-24
申请人： Hiroyuki Adachi , Masao Yamaguchi , Osamu Miyahara , Takahiro Sagae
发明人： Hiroyuki Adachi , Masao Yamaguchi , Osamu Miyahara , Takahiro Sagae
IPC分类号： A01N43/56 , A01N43/653 , A01N43/713 , A01N43/74 , A01N43/80 , A01N43/82 , C07D261/08 , C07D401/10 , C07D413/10
CPC分类号： C07D401/10 , A01N43/56 , A01N43/653 , A01N43/713 , A01N43/74 , A01N43/80 , A01N43/82 , C07D261/08 , C07D413/10
摘要： This invention concerns a benzoic acid represented by the formula �I! ##STR1## or a benzoic acid derivative and a method for the production of a compound represented by the formula �I!. The compound represented by the formula �I! is an intermediate for the production of a herbicidally active pyrazole compound represented by the formula �B! ##STR2##
摘要翻译： PCT No.PCT / JP97 / 00341 Sec。 371 1997年10月2日第 102（e）日期1997年10月2日PCT 1997年2月10日提交PCT公布。出版物WO97 / 35850 日期1997年10月2日本发明涉及由式[I]表示的苯甲酸或苯甲酸衍生物及其制备式[I]表示的化合物的方法。由式[I]表示的化合物是用于制备由式[B]表示的除草活性吡唑化合物的中间体，

4. 发明授权

US06359143B1 Heterocycle-bearing thio phenol compounds, intermediates for the preparation of the same and processes for the preparation of both 失效
标题翻译：含杂环硫代苯酚化合物，其制备中间体及其制备方法
公开(公告)号：US06359143B1
公开(公告)日：2002-03-19
申请号：US09719021
申请日：2000-12-05
申请人： Hiroyuki Adachi , Takahiro Sagae , Toshio Aihara
发明人： Hiroyuki Adachi , Takahiro Sagae , Toshio Aihara
IPC分类号： C07D23112
CPC分类号： C07D261/08
摘要： Novel thio phenol compounds bearing heterocyclic groups as the substituent, useful as intermediates for the preparation of agricultural chemicals, particularly herbicides; intermediates for the preparation of the same; and processes for the preparation of both as represented by reaction formula (I), herein R1 is C1-C4 alkyl; R2 is hydrogen or C1-C4 alkyl; R3 is hydrogen cyano, amido, C1-C4 alkylcarbonyl or C1-C4 alkoxycarbonyl; R4 is C1-C4 alkyl; and Q is isoxazolyl or the like.
摘要翻译：含有杂环基团的新型硫代苯酚化合物作为取代基，可用作制备农药，特别是除草剂的中间体; 中间体制备相同; 和由反应式（I）表示的两者的制备方法，其中R 1是C 1 -C 4烷基; R2是氢或C1-C4烷基; R3是氢氰基，酰胺基，C1-C4烷基羰基或C1-C4烷氧基羰基; R4是C1-C4烷基; Q是异恶唑基等。

5. 发明申请

US20100210876A1 MICROREACTOR AND LIQUID PHASE CHEMICAL REACTION METHOD USING MICROREACTOR 有权
标题翻译：微生物和液相化学反应方法
公开(公告)号：US20100210876A1
公开(公告)日：2010-08-19
申请号：US12734066
申请日：2008-10-10
申请人： Ilhyong Ryu , Masaaki Sato , Takahiro Sagae , Kenichi Hayashi
发明人： Ilhyong Ryu , Masaaki Sato , Takahiro Sagae , Kenichi Hayashi
IPC分类号： C07C201/00 , B01J8/02 , C07C17/00
CPC分类号： C07C17/275 , B01J19/0093 , B01J21/04 , B01J23/44 , B01J35/023 , B01J35/026 , B01J2219/00835 , B01J2219/00891 , C07C67/343 , C07C205/16 , C07C22/04 , C07C69/618
摘要： This invention provides a microreactor comprising a microchamber provided with a raw material introduction port and a product discharge port; wherein solid catalysts are aligned in a line in the longitudinal direction of the microchamber to fill the microchamber.
摘要翻译：本发明提供了一种微反应器，其包括设置有原料引入口和产品排出口的微型室; 其中固体催化剂在微室的纵向方向上一行排列以填充微室。

6. 发明授权

US08609034B2 Microreactor and liquid phase chemical reaction method using microreactor 有权
标题翻译：微反应器和液相化学反应法采用微反应器
公开(公告)号：US08609034B2
公开(公告)日：2013-12-17
申请号：US12734066
申请日：2008-10-10
申请人： Ilhyong Ryu , Masaaki Sato , Takahiro Sagae , Kenichi Hayashi
发明人： Ilhyong Ryu , Masaaki Sato , Takahiro Sagae , Kenichi Hayashi
IPC分类号： B01J8/00
CPC分类号： C07C17/275 , B01J19/0093 , B01J21/04 , B01J23/44 , B01J35/023 , B01J35/026 , B01J2219/00835 , B01J2219/00891 , C07C67/343 , C07C205/16 , C07C22/04 , C07C69/618
摘要： This invention provides a microreactor comprising a microchamber provided with a raw material introduction port and a product discharge port; wherein solid catalysts are aligned in a line in the longitudinal direction of the microchamber to fill the microchamber.
摘要翻译：本发明提供了一种微反应器，其包括设置有原料引入口和产品排出口的微型室; 其中固体催化剂在微室的纵向方向上一行排列以填充微室。

7. 发明申请

US20060287527A1 Process for producing acrylic acid derivative 审中-公开
标题翻译：制备丙烯酸衍生物的方法
公开(公告)号：US20060287527A1
公开(公告)日：2006-12-21
申请号：US11446448
申请日：2006-06-01
申请人： Yasuyuki Miyazawa , Takahiro Sagae , Yutaka Ishii , Hiroyuki Yazaki , Makoto Funabora , Satoru Yamazaki
发明人： Yasuyuki Miyazawa , Takahiro Sagae , Yutaka Ishii , Hiroyuki Yazaki , Makoto Funabora , Satoru Yamazaki
IPC分类号： C07D239/34
CPC分类号： C07D239/56 , C07C67/31 , C07C67/343 , C07D239/34 , C07D239/52 , C07C69/734 , C07C69/732
摘要： Processes for producing a compound represented by the formula (1), which includes an acrylic acid derivative and is useful as an agricultural chemical or medicine. One of the processes comprises the step of formulating a compound (3) and converting the OH of the resultant compound (2) into OR″. The first step comprises reacting a formic or orthoformic ester in the presence of a Lewis acid and a base. The second step comprises reacting the compound with R″OH or with R″OH and CH(OR″)3 under acidic conditions or using a phase-transfer catalyst in a two-phase system and regulating the base and the concentration thereof to stereoselectively synthesize the target compound. In another, process, the compound is efficiently produced without isolating the compound. The compound can also be produced without the compound (2).
摘要翻译：制备由式（1）表示的化合物的方法，其包括丙烯酸衍生物并且可用作农业化学品或药物。其中一个方法包括配制化合物（3）并将所得化合物（2）的OH转化为OR“的步骤。第一步包括在路易斯酸和碱的存在下使甲酸或正癸酸酯反应。第二步包括在酸性条件下或在两相体系中使用相转移催化剂使化合物与R''OH或与R''OH和CH（OR“）3'反应，调节碱和其浓度以立体选择性合成目标化合物。在另一个方法中，化合物在不分离化合物的情况下有效生产。化合物也可以不用化合物（2）制备。

8. 发明授权

US07358356B2 Processes for preparation of organic compounds 失效
标题翻译：有机化合物的制备方法
公开(公告)号：US07358356B2
公开(公告)日：2008-04-15
申请号：US10529392
申请日：2003-10-02
申请人： Mitsuru Takase , Takahiro Sagae , Hiroyuki Yazaki , Shigeo Mori , Daisuke Asanuma
发明人： Mitsuru Takase , Takahiro Sagae , Hiroyuki Yazaki , Shigeo Mori , Daisuke Asanuma
IPC分类号： C07D499/18
CPC分类号： C07D499/893 , C07D499/88
摘要： The present invention provides a method for preparing an organic compound, which comprises a dehydration step of distilling off water from a polar organic solvent solution containing the organic compound and water to bring the concentration of water below a given level, wherein the dehydration step comprises distilling off water together with the polar organic solvent while adding a polar organic solvent to the solution, or comprises repeating several cycles of adding a polar organic solvent to the solution and then distilling off water together with the polar organic solvent. The present invention further provides the preparation of an organic compound, which enables efficient isolation of the target product in high isolated yield from a polar organic solvent solution containing the organic compound, water and, if necessary, a compound which produces, upon coming into contact with water or the like, a substance accelerating the decomposition of the organic compound.
摘要翻译：本发明提供了一种制备有机化合物的方法，该方法包括从含有有机化合物和水的极性有机溶剂溶液中蒸馏出水以使水的浓度低于给定水平的脱水步骤，其中脱水步骤包括蒸馏将极性有机溶剂与极性有机溶剂一起加入到溶液中，或者包括重复多次向溶液中加入极性有机溶剂，然后与极性有机溶剂一起蒸馏出水。本发明还提供有机化合物的制备，其能够以高分离产率从含有有机化合物的极性有机溶剂溶液，水和必要时的化合物在接触时产生高分离产物。用水等加速有机化合物分解的物质。

9. 发明授权

US07041820B2 Process for producing (dioxolenon-4-yl)methyl ester derivative 失效
标题翻译：（二氧噻吩-4-基）甲酯衍生物的制备方法
公开(公告)号：US07041820B2
公开(公告)日：2006-05-09
申请号：US10473297
申请日：2002-03-29
申请人： Toshiyuki Watai , Mitsuru Takase , Takahiro Sagae , Shigeo Mori , Noriaki Kawahara
发明人： Toshiyuki Watai , Mitsuru Takase , Takahiro Sagae , Shigeo Mori , Noriaki Kawahara
IPC分类号： C07D499/08
CPC分类号： C07D499/88 , C07D317/40 , C07D499/00
摘要： There is provided a method by which various compounds (1) having a carboxyl group in the molecule have the carboxyl group converted to a (dioxolenon-4-yl)methyl ester at low cost, in a simple way and at high yield.The process for producing compounds of formula (3) according to the reaction scheme shown below comprises reacting carboxylic acids of formula (1) with 4-chloromethyldioxolenone compounds of formula (2) in a solvent in the presence of both a phase transfer catalyst and a metal iodide: [where Q represents an organic group, M represents a hydrogen atom, an alkali metal, an alkaline earth metal or a transition metal, R1 and R2 represent a hydrogen atom, an optionally substituted (C1-6 alkyl group or phenyl group)].
摘要翻译：提供了以简单的方式和高产率，分子中具有羧基的各种化合物（1）以低成本将羧基转化为（二氧戊环-4-基）甲酯的方法。根据下述反应路线制备式（3）化合物的方法包括使式（1）的羧酸与式（2）的4-氯甲基二氧戊烯酮化合物在溶剂中在相转移催化剂和金属碘化物：[其中Q表示有机基团，M表示氢原子，碱金属，碱土金属或过渡金属，R 1和R 2表示氢原子，任选取代的（C 1-6烷基或苯基）]。

10. 发明申请

US20060058521A1 Processes for preparation of organic compounds 失效
标题翻译：有机化合物的制备方法
公开(公告)号：US20060058521A1
公开(公告)日：2006-03-16
申请号：US10529392
申请日：2003-10-02
申请人： Mitsuru Takase , Takahiro Sagae , Hiroyuki Yazaki , Shigeo Mori , Daisuke Asanuma
发明人： Mitsuru Takase , Takahiro Sagae , Hiroyuki Yazaki , Shigeo Mori , Daisuke Asanuma
IPC分类号： C07D205/02
CPC分类号： C07D499/893 , C07D499/88
摘要： The present invention provides a method for preparing an organic compound, which comprises a dehydration step of distilling off water from a polar organic solvent solution containing the organic compound and water to bring the concentration of water below a given level, wherein the dehydration step comprises distilling off water together with the polar organic solvent while adding a polar organic solvent to the solution, or comprises repeating several cycles of adding a polar organic solvent to the solution and then distilling off water together with the polar organic solvent. The present invention further provides the preparation of an organic compound, which enables efficient isolation of the target product in high isolated yield from a polar organic solvent solution containing the organic compound, water and, if necessary, a compound which produces, upon coming into contact with water or the like, a substance accelerating the decomposition of the organic compound.
摘要翻译：本发明提供了一种制备有机化合物的方法，该方法包括从含有有机化合物和水的极性有机溶剂溶液中蒸馏出水以使水的浓度低于给定水平的脱水步骤，其中脱水步骤包括蒸馏将极性有机溶剂与极性有机溶剂一起加入到溶液中，或者包括重复多次向溶液中加入极性有机溶剂，然后与极性有机溶剂一起蒸馏出水。本发明还提供有机化合物的制备，其能够以高分离产率从含有有机化合物的极性有机溶剂溶液，水和必要时的化合物在接触时产生高分离产物。用水等加速有机化合物分解的物质。

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