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1. 发明授权

US5371116A Vulcanizable organopolysiloxane composition 失效
标题翻译：可硫化的有机聚硅氧烷组合物
公开(公告)号：US5371116A
公开(公告)日：1994-12-06
申请号：US90374
申请日：1993-07-13
申请人： Takafumi Sakamoto , Masatoshi Arai , Kei Miyoshi
发明人： Takafumi Sakamoto , Masatoshi Arai , Kei Miyoshi
IPC分类号： C08K3/16 , C08F2/46 , C08K5/057 , C08K5/098 , C08K5/54 , C08K5/5419 , C08K5/5425 , C08K5/57 , C08L83/04 , C08L83/06
CPC分类号： C08K5/5425 , C08K5/5419 , C08K5/57 , C08L83/04 , C08G77/16
摘要： Vulcanizable organopolysiloxane compositions comprise a hydroxy-terminated organopolysiloxane, an acrylic or methacryllc functional alkoxy silane, a divalent tin compound, an alkoxy-.alpha.-silyl ester, a photopolymerization initiator, and a curing catalyst whereby the composition is cured by UV irradiation and/or by the action of moisture in air. The composition has good shelf stability and can yield rubber elastomers having good physical properties.
摘要翻译：可硫化的有机聚硅氧烷组合物包含羟基封端的有机聚硅氧烷，丙烯酸或甲基丙烯酸官能的烷氧基硅烷，二价锡化合物，烷氧基-α-甲硅烷基酯，光聚合引发剂和固化催化剂，由此组合物通过UV照射和/或通过空气中的水分作用。该组合物具有良好的贮存稳定性并且可以产生具有良好物理性能的橡胶弹性体。

2. 发明授权

US5286892A 2-trimethoxysilylpropionate 失效
标题翻译： 2-三甲氧基甲硅烷基丙酸酯
公开(公告)号：US5286892A
公开(公告)日：1994-02-15
申请号：US985868
申请日：1992-12-04
申请人： Masatoshi Arai , Takafumi Sakamoto , Yoshifumi Inoue , Kei Miyoshi
发明人： Masatoshi Arai , Takafumi Sakamoto , Yoshifumi Inoue , Kei Miyoshi
IPC分类号： C07F7/04 , C07F7/18 , C09K3/00 , C07F7/08
CPC分类号： C07F7/045 , C07F7/1836
摘要： The present novel organosilicon compound is a 2-trimethoxysilylpropionate represented by the following formula ##STR1## wherein R represents a monovalent hydrocarbon group having 6 to 12 carbon atoms. This ester reacts efficiently with alcohols and silanols and is useful, for example, as a terminal alkoxysilylating agent for organopolysiloxanes such as industrially useful .alpha.,.omega.-dihydroxypolydimethylsiloxane, or as a surface treatment for silicas, or as a storage stabilizer that serves as a scavenger of an alcohol for alcohol elimination type RTV. Further, since the present organosilicon compound is a three-functional alkoxysilane having three methoxy groups in the molecule, it is useful as a curing agent for alcohol elimination type RTV.
摘要翻译：本发明的新型有机硅化合物是由下式（*化学结构*）表示的2-三甲氧基甲硅烷基丙酸酯，其中R表示碳原子数为6〜12的一价烃基。该酯与醇和硅烷醇有效反应，并且可用作例如工业上有用的（α），（ω） - 二羟基聚二甲基硅氧烷的有机聚硅氧烷的末端烷氧基硅烷化剂，或作为二氧化硅的表面处理或作为储存稳定剂作为酒精消除型RTV的酒精清除剂。此外，由于本发明的有机硅化合物是分子中具有三个甲氧基的三官能烷氧基硅烷，因此可用作醇消除型RTV的固化剂。

3. 发明授权

US5508459A 2-methyldialkoxysilyl propionic acid ester 失效
标题翻译： 2-甲基二烷氧基甲硅烷基丙酸酯
公开(公告)号：US5508459A
公开(公告)日：1996-04-16
申请号：US404574
申请日：1995-03-15
申请人： Masatoshi Arai , Takafumi Sakamoto , Kei Miyoshi
发明人： Masatoshi Arai , Takafumi Sakamoto , Kei Miyoshi
IPC分类号： C07F7/18 , C07F7/08
CPC分类号： C07F7/184
摘要： 2-Methyldialkoxysilyl propionic acid esters defined by general chemical formula (1): ##STR1## wherein R is an alkyl group with at most four carbon atoms, and R.sup.1 is a monovalent, substituted or unsubstituted, hydrocarbon group with 1 to 12 carbon atoms, are novel compounds with good reactivity. These compounds are extremely useful as alkoxylation agents for the terminal groups of organopolysiloxanes, surface treatment agents for silica, stabilizers during storage and curing agents.
摘要翻译：由通式（1）定义的2-甲基二烷氧基甲硅烷基丙酸酯：其中R是具有至多四个碳原子的烷基，R 1是具有1至12个碳原子的单价，取代或未取代的烃基碳原子是具有良好反应性的新型化合物。这些化合物作为有机聚硅氧烷的末端基团的烷氧基化剂，二氧化硅的表面处理剂，储存期间的稳定剂和固化剂是非常有用的。

4. 发明授权

US5482992A Room temperature quick curable organopolysiloxane composition excellent in water resistance 失效
标题翻译：室温快速固化有机聚硅氧烷组合物耐水性优良
公开(公告)号：US5482992A
公开(公告)日：1996-01-09
申请号：US328515
申请日：1994-10-25
申请人： Tsuneo Kimura , Kei Miyoshi , Masatoshi Arai
发明人： Tsuneo Kimura , Kei Miyoshi , Masatoshi Arai
IPC分类号： C08K5/04 , C08G65/336 , C08K5/07 , C08K5/17 , C08L71/02 , C08L83/04 , C08L83/06 , C08J3/00 , C08K3/20 , C08L83/00 , C08G77/00
CPC分类号： C08G65/336 , C08K5/07
摘要： A room temperature curable rubber composition of a condensation curing type that comprises as a base polymer a diorganopolysiloxane or a polyoxyalkylene in which both ends of the molecular chain are blocked with a hydrolyzable silyl group, and a .beta.-dicarbonyl compound and an amino group containing organic compound that are blended with the base polymer. Since the room temperature curable rubber composition is cured with water in the air and at the same time the dehydration condensation of the .beta.-carbonyl group and the amino group produces water in the composition, the quick curability and deep curability are improved remarkably. In addition, since this dehydration condensation reaction is an irreversible reaction, the product produced by the condensation dehydration is hydrolyzed to prevent the amino group containing compound from being regenerated, and as a result the hydrophilic nature of the cured product is prevented from increasing not to damage the water resistance.
摘要翻译：一种缩合固化型室温可固化橡胶组合物，其包含作为基础聚合物的二有机聚硅氧烷或分子链两端用可水解甲硅烷基封端的聚氧化烯，以及β-二羰基化合物和含氨基的有机物与基础聚合物共混的化合物。由于室温固化橡胶组合物在空气中用水固化，同时β-羰基和氨基的脱水缩合在组合物中产生水，因此快速固化性和深度固化性显着提高。此外，由于该脱水缩合反应是不可逆反应，所以通过缩合脱水生成的产物被水解以防止含氨基化合物再生，结果，防止了固化产物的亲水性增加，不会增加损坏防水性。

5. 发明授权

US5514741A Room temperature curable organopolysiloxane composition 失效
标题翻译：室温可固化的有机聚硅氧烷组合物
公开(公告)号：US5514741A
公开(公告)日：1996-05-07
申请号：US337440
申请日：1994-11-08
申请人： Masatoshi Arai , Kei Miyoshi , Shinichi Sato
发明人： Masatoshi Arai , Kei Miyoshi , Shinichi Sato
IPC分类号： C08K3/20 , C08K3/22 , C08K5/54 , C08K5/5419 , C08L83/04 , C08L83/06 , C08K3/10
CPC分类号： C08K5/5406 , C08L83/04 , C08G77/16 , C08G77/24
摘要： A condensation curing type room temperature curable organopolysiloxane composition, comprising (A) a diorganopolysiloxane the both ends of the molecular chain of which are terminated with a hydroxyl group, (B) an organosilicon compound containing at least three hydrolyzable groups bonded to a silicon atom in the molecule or its partial hydrolysis-condensation product, (C) an alkoxysilane having a fluorine-containing organic group, and (D) aluminum hydroxide. This composition can form a cured product excellent in soil resistance and can keep favorably the tracking resistance for a long period of time. Particularly, the composition is quite useful as a protective coating material for high voltage power supply parts used outdoors.
摘要翻译：一种缩合固化型室温可固化的有机聚硅氧烷组合物，其包含（A）分子链的两端用羟基封端的二有机聚硅氧烷，（B）含有至少三个与硅原子键合的可水解基团的有机硅化合物该分子或其部分水解缩合产物，（C）具有含氟有机基团的烷氧基硅烷和（D）氢氧化铝。该组合物可以形成耐土壤性优异的固化物，并且可以长时间保持耐追踪性。特别地，该组合物作为用于室外的高压电源部件的保护涂层材料是非常有用的。

6. 发明授权

US5216037A Room temperature vulcanizable, foamable polysiloxane composition 失效
标题翻译：室温硫化，可发泡聚硅氧烷组合物
公开(公告)号：US5216037A
公开(公告)日：1993-06-01
申请号：US903308
申请日：1992-06-24
申请人： Kei Miyoshi , Masatoshi Arai
发明人： Kei Miyoshi , Masatoshi Arai
IPC分类号： C08J9/02 , C08L83/04 , C08L83/05 , C08L83/06
CPC分类号： C08J9/02 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/70 , C08J2383/04
摘要： A room temperature vulcanizable, foamable polysiloxane composition is described, which comprises:(A) a specific type of .alpha., .omega.-dihydroxyorganopolysiloxane which has a surface tension of not lower than 22 dynes/cm at 25.degree. C.;(B) a specific type of organopolyhydroxypolysiloxane;(C) a polyorganohydrogensiloxane which has at least two units of the following general formula in one moleculeR.sup.5.sub.a H.sub.b SiO.sub.(4-(a+b))/2 wherein R.sup.5 represents a monovalent hydrocarbon group except for aliphatic unsaturated hydrocarbon group, a is an integer of 0 to 2, and b is an integer of from 0 to 3 provided that the total of a+b is an integer of from 1 to 3;(D) an unsubstituted or substituted alcohol having from 1 to 12 carbon atoms; and(E) a platinum catalyst.The composition has a high degree of foaming and the foamed product obtained from the composition has good foaming stability and good tensile strength.
摘要翻译：描述了室温可硫化的可发泡聚硅氧烷组合物，其包括：（A）在25℃具有不低于22达因/厘米的表面张力的特定类型的α，ω-二羟基有机聚硅氧烷。（B）特定类型的有机多羟基聚硅氧烷; （C）在一个分子中具有至少两个以下通式的单元的聚有机氢硅氧烷：R5aHbSiO（4-（a + b））/ 2其中R5表示除脂肪族不饱和烃基以外的一价烃基，a为 0〜2，b为0〜3的整数，条件是a + b为1〜3的整数。（D）具有1至12个碳原子的未取代或取代的醇; 和（E）铂催化剂。该组合物具有高度的发泡性，并且由该组合物获得的发泡产品具有良好的起泡稳定性和良好的拉伸强度。

7. 发明授权

US5196477A Silcone compositions comprising organic compounds having the capabilities of coordination with metals 失效
标题翻译：包含具有与金属配位能力的有机化合物的丝素组合物
公开(公告)号：US5196477A
公开(公告)日：1993-03-23
申请号：US556496
申请日：1990-07-24
申请人： Masatoshi Arai , Yoshifumi Inoue , Kei Miyoshi
发明人： Masatoshi Arai , Yoshifumi Inoue , Kei Miyoshi
IPC分类号： C08K5/00 , C08K5/54 , C08K5/5419 , H01B3/46
CPC分类号： H01B3/46 , C08K5/0008 , C08K5/54 , C08K5/5419
摘要： Silicone compositions comprising an organopolysiloxane composition and an organic compound capable of coordination with metals are described. Since the organic compound is preferentially adsorbed on a metal surface, the composition is particularly suitable for use in electric or electronic parts to prevent contact failure. A more specific embodiment comprises a diorganopolysiloxane of the average unit formula, R.sub.a SiO.sub.(4-a)/2, wherein each R independently represents an unsubstituted or substituted monovalent hydrocarbon group, and a is a value of from 1.90 to 2.05, a filler, an alkoxysilane or its hydrolyzate, a silylation catalyst made of an organic silicon compound having at least one specific type of group, an organic tin compound, another organosilicon compound capable of reaction with an alcohol in order to stabilize the composition, and an organic compound capable of coordination with metals.
摘要翻译：描述了包含有机聚硅氧烷组合物和能与金属配位的有机化合物的硅酮组合物。由于有机化合物优先吸附在金属表面上，因此该组合物特别适用于电气或电子部件以防止接触不良。更具体的实施方案包括平均单元式的二有机聚硅氧烷，RaSiO（4-a）/ 2，其中每个R独立地表示未取代或取代的一价烃基，a为1.90至2.05的值，填料，烷氧基硅烷或其水解物，由具有至少一种特定类型基团的有机硅化合物制成的甲硅烷基化催化剂，有机锡化合物，能够与醇反应的另一种有机硅化合物以稳定组合物，以及能够与金属配合。

8. 发明申请

US20120029229A1 METHOD FOR PRODUCING HIGH PURITY TERMINAL OLEFIN COMPOUND 有权
标题翻译：生产高纯度终端烯烃化合物的方法
公开(公告)号：US20120029229A1
公开(公告)日：2012-02-02
申请号：US13262372
申请日：2010-01-08
申请人： Kei Miyoshi , Goro Asanuma
发明人： Kei Miyoshi , Goro Asanuma
IPC分类号： C07C7/04 , C07C253/34 , C07C67/54 , C07C45/82
CPC分类号： C07C45/85 , C07C7/005 , C07C7/04 , C07C45/82 , C07C67/60 , C07C253/34 , C07C11/02 , C07C47/21 , C07C69/533 , C07C255/07
摘要： An industrially advantageous method for producing a high purity terminal olefin is disclosed, comprising the steps of (a) contacting a mixture comprising a terminal olefin represented by formula (1): and one or more corresponding internal olefins as impurities, with a brominating agent in the presence of water or an alcohol, to convert the internal olefin(s) to compound(s) having a higher boiling point than the terminal olefin; and (b) purifying the terminal olefin by distillation from the reaction mixture.
摘要翻译：公开了一种用于生产高纯度末端烯烃的工业上有利的方法，其包括以下步骤：（a）将包含由式（1）表示的末端烯烃与一种或多种相应的内部烯烃作为杂质的混合物与溴化剂存在水或醇，将内烯烃转化成沸点高于末端烯烃的化合物; 和（b）通过蒸馏从反应混合物中纯化末端烯烃。

9. 发明授权

US07838117B2 Silicone-sealed LED 有权
标题翻译：硅胶密封LED
公开(公告)号：US07838117B2
公开(公告)日：2010-11-23
申请号：US11334471
申请日：2006-01-19
申请人： Kei Miyoshi , Eiichi Tabei
发明人： Kei Miyoshi , Eiichi Tabei
IPC分类号： B32B27/00 , H01L21/56 , C08L83/00 , C08G77/04
CPC分类号： H01L33/56 , C08G77/12 , C08G77/16 , C08G77/18 , C08G77/20 , C08L83/04 , Y10T428/31663 , C08L83/00
摘要： Provided is a silicone-sealed LED including: a LED chip, a cured silicone rubber layer which coats the LED chip, and a cured silicone resin layer which coats and seals the periphery of the cured silicone rubber layer. Also provided are a process for producing the silicone-sealed LED and a process for sealing a LED. In the silicone-sealed LED, a silicone rubber layer disposed between a silicone resin layer that represents the sealing body and a LED chip functions as a buffer layer, meaning cracks are not easily generated in the silicone resin layer that represents the sealing body, while full use is made of the excellent heat resistance, weather resistance, and color fastness of the silicone rubber and the silicone resin.
摘要翻译：本发明提供一种硅密封LED，其包括：LED芯片，涂覆LED芯片的固化硅橡胶层和涂覆固化的硅橡胶层的周边的固化的有机硅树脂层。还提供了用于制造硅树脂密封LED的工艺和用于密封LED的工艺。在硅酮密封型LED中，设置在表示密封体的有机硅树脂层和LED芯片之间的硅橡胶层用作缓冲层，意味着在代表密封体的有机硅树脂层中不容易产生裂纹，同时充分利用硅橡胶和硅树脂的优异的耐热性，耐候性和色牢度。

10. 发明授权

US07705104B2 Addition curable silicon resin composition for light emitting diode 有权
标题翻译：用于发光二极管的加成可固化硅树脂组合物
公开(公告)号：US07705104B2
公开(公告)日：2010-04-27
申请号：US11461895
申请日：2006-08-02
申请人： Naoki Yamakawa , Kei Miyoshi
发明人： Naoki Yamakawa , Kei Miyoshi
IPC分类号： C08G77/12
CPC分类号： C08G77/44 , C08G77/12 , C08G77/14 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/70 , C08G77/80 , C08L83/04 , C08L2205/02 , C08L2205/035 , C08L83/00
摘要： An addition curable silicone resin composition for a light emitting diode is provided The composition includes an organopolysiloxane that includes a straight-chain segment represented by a formula: —(R12SiO)n— wherein, R1 is an unsaturated aliphatic bonding-free monovalent hydrocarbon group, and n is an integer of 1 or greater, and a resin-like segment consisting of R23SiO1/2 units wherein, R2 is a monovalent hydrocarbon group, an alkoxy group, or a hydroxyl group, SiO2 units, and/or R2SiO3/2 units wherein, R2 is as defined above, in which at least two of all the R2 groups are alkenyl groups. The composition exhibits strong resistance to thermal shock, and is resistant to cracking even under severe temperature cycling.
摘要翻译：提供了一种用于发光二极管的可加成固化的有机硅树脂组合物。该组合物包括有机聚硅氧烷，其包括由下式表示的直链链段： - （R 12 SiO）n - ，其中，R 1是不饱和的无脂族键结的一价烃基，和n为1以上的整数，以及由R 23 SiO 1/2单元构成的树脂状链段，其中，R 2为一价烃基，烷氧基或羟基，SiO 2单元和/或R 2 SiO 3/2单元其中R2如上所定义，其中所有R2基团中的至少两个是烯基。该组合物显示出对热冲击的强耐受性，并且即使在剧烈的温度循环下也能耐裂纹。

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