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1. 发明授权

US07253315B2 Process for preparing fluorocarboxylic acids 有权
标题翻译：制备氟代羧酸的方法
公开(公告)号：US07253315B2
公开(公告)日：2007-08-07
申请号：US11088370
申请日：2005-03-24
申请人： Ta-Wei Fu , Steven H. Swearingen , Takuya Ichida , Shigeyuki Yoshii
发明人： Ta-Wei Fu , Steven H. Swearingen , Takuya Ichida , Shigeyuki Yoshii
IPC分类号： C07C53/15 , C07C51/58
CPC分类号： C07C51/04 , C07C51/48 , C07C59/135 , C07C53/21
摘要： A fluorocarboxylic acid preparation process which includes hydrolyzing fluorocarboxylic acid fluoride in the presence of an aqueous sulfuric acid solution to form a reaction product containing a fluorocarboxylic acid and hydrogen fluoride (present as hydrofluoric acid); and removing at least some of the hydrogen fluoride from the reaction product by washing the reaction production with aqueous sulfuric acid solution. The hydrolyzing and washing are carried out at a temperature at which the fluorocarboxylic acid is a liquid.
摘要翻译：一种氟代羧酸制备方法，其包括在硫酸水溶液存在下水解氟代羧酸，形成含有氟代羧酸和氟化氢（以氢氟酸形式存在）的反应产物; 并通过用硫酸水溶液洗涤反应生成，从反应产物中除去至少一些氟化氢。水解和洗涤在氟代羧酸是液体的温度下进行。

2. 发明授权

US07126016B2 Process for preparing fluorocarboxylic acids 有权
标题翻译：制备氟代羧酸的方法
公开(公告)号：US07126016B2
公开(公告)日：2006-10-24
申请号：US11088465
申请日：2005-03-24
申请人： Ta-Wei Fu , Steven H. Swearingen , Takuya Ichida , Shuji Itatani
发明人： Ta-Wei Fu , Steven H. Swearingen , Takuya Ichida , Shuji Itatani
IPC分类号： C07C51/00
CPC分类号： C07C51/48 , C07C51/02 , C07C59/135 , C07C53/21
摘要： A fluorocarboxylic acid preparation process continuously carries out acidification reaction treatment and washing treatment, and includes subjecting a fluorocarboxylate-containing aqueous solution to acidification reaction treatment in the presence of sulfuric acid so as to form a sulfate-containing fluorocarboxylic acid phase; and subjecting the fluorocarboxylic acid phase to washing treatment using an aqueous sulfuric acid solution.
摘要翻译：氟代羧酸制备方法连续进行酸化反应处理和洗涤处理，包括在含硫酸盐存在下使含氟羧酸酯的水溶液进行酸化反应处理以形成含硫酸盐的氟代羧酸相; 并使用硫酸水溶液对氟代羧酸相进行洗涤处理。

3. 发明申请

US20050165254A1 Process for preparing fluorocarboxylic acids 有权
标题翻译：制备氟代羧酸的方法
公开(公告)号：US20050165254A1
公开(公告)日：2005-07-28
申请号：US11088370
申请日：2005-03-24
申请人： Ta-Wei Fu , Steven Swearingen , Takuya Ichida , Shigeyuki Yoshii
发明人： Ta-Wei Fu , Steven Swearingen , Takuya Ichida , Shigeyuki Yoshii
IPC分类号： C07C51/04 , C07C51/48 , C07C59/135
CPC分类号： C07C51/04 , C07C51/48 , C07C59/135 , C07C53/21
摘要： A fluorocarboxylic acid preparation process which includes hydrolyzing fluorocarboxylic acid fluoride in the presence of an aqueous sulfuric acid solution to form a reaction product containing a fluorocarboxylic acid and hydrogen fluoride (present as hydrofluoric acid); and removing at least some of the hydrogen fluoride from the reaction product by washing the reaction production with aqueous sulfuric acid solution. The hydrolyzing and washing are carried out at a temperature at which the fluorocarboxylic acid is a liquid.
摘要翻译：一种氟代羧酸制备方法，其包括在硫酸水溶液存在下水解氟代羧酸，形成含有氟代羧酸和氟化氢（以氢氟酸形式存在）的反应产物; 并通过用硫酸水溶液洗涤反应生成，从反应产物中除去至少一些氟化氢。水解和洗涤在氟代羧酸是液体的温度下进行。

4. 发明申请

US20050171381A1 Process for preparing fluorocarboxylic acids 有权
标题翻译：制备氟代羧酸的方法
公开(公告)号：US20050171381A1
公开(公告)日：2005-08-04
申请号：US11088465
申请日：2005-03-24
申请人： Ta-Wei Fu , Steven Swearingen , Takuya Ichida , Shuji Itatani
发明人： Ta-Wei Fu , Steven Swearingen , Takuya Ichida , Shuji Itatani
IPC分类号： C07C51/02 , C07C51/48 , C07C59/135
CPC分类号： C07C51/48 , C07C51/02 , C07C59/135 , C07C53/21
摘要： A fluorocarboxylic acid preparation process continuously carries out acidification reaction treatment and washing treatment, and includes subjecting a fluorocarboxylate-containing aqueous solution to acidification reaction treatment in the presence of sulfuric acid so as to form a sulfate-containing fluorocarboxylic acid phase; and subjecting the fluorocarboxylic acid phase to washing treatment using an aqueous sulfuric acid solution.
摘要翻译：氟代羧酸制备方法连续进行酸化反应处理和洗涤处理，包括在含硫酸盐存在下使含氟羧酸酯的水溶液进行酸化反应处理以形成含硫酸盐的氟代羧酸相; 并使用硫酸水溶液对氟代羧酸相进行洗涤处理。

5. 发明授权

US4999099A Process for making mesophase pitch 失效
标题翻译：制备中间相沥青的方法
公开(公告)号：US4999099A
公开(公告)日：1991-03-12
申请号：US824387
申请日：1986-01-30
申请人： Ta-Wei Fu , Manfred Katz
发明人： Ta-Wei Fu , Manfred Katz
IPC分类号： C10C3/00 , C10C3/04
CPC分类号： C10C3/002 , C10C3/04
摘要： An improved process for producing an anisotropic pitch product suitable for carbon fiber manufacture. A carbonaceous feedstock is heated at elevated temperature while passing a reactive sparging gas through the feedstock. The sparging gas is an oxidative gas such as a gaseous mixture containing a major proportion of inert gas and from about 0.1 to 2% by volume of oxygen. The process produces an anisotropic pitch having from 50 to 100% by volume mesophase which is suitable for producing good quality carbon fibers.
摘要翻译：一种用于生产适用于碳纤维制造的各向异性沥青产品的改进方法。将碳质原料在升高的温度下加热，同时使反应性喷射气体通过原料。喷射气体是氧化性气体，例如含有大部分惰性气体和约0.1-2％（体积）氧气的气体混合物。该方法产生具有50至100体积％中间相的各向异性沥青，适用于生产优质碳纤维。

6. 发明授权

US4758329A Premium coking process 失效
标题翻译：优质焦化工艺
公开(公告)号：US4758329A
公开(公告)日：1988-07-19
申请号：US20404
申请日：1987-03-02
申请人： Bruce A. Newman , Ta-Wei Fu
发明人： Bruce A. Newman , Ta-Wei Fu
IPC分类号： C10B57/04 , C10B55/00 , C10B57/12 , C10G9/14
CPC分类号： C10B57/12 , C10B55/00
摘要： In a delayed premium coking process utilizing as feedstock an aromatic mineral oil having a high aromatic content and a low molecular weight, coke CTE is reduced and coke particle size is increased by sparging with a gas during the coking cycle.

7. 发明授权

US5569797A Method of removing olefinic impurities from hydrochlorofluorocarbons 失效
标题翻译：从氢氯氟烃中除去烯烃杂质的方法
公开(公告)号：US5569797A
公开(公告)日：1996-10-29
申请号：US817628
申请日：1992-01-07
申请人： Ta-Wei Fu , Velliyur N. M. Rao
发明人： Ta-Wei Fu , Velliyur N. M. Rao
IPC分类号： B01J23/40 , C07B61/00 , C07C17/20 , C07C17/38 , C07C17/395 , C07C19/10
CPC分类号： C07C17/395 , C07C17/38
摘要： A process for preparing a hydrochlorofluorocarbon essentially free of olefinic impurities by selectively hydrogenating the olefinic impurities. The process may be controlled such that at least a portion of the hydrochlorofluorocarbon is converted into a fluorohydrocarbon.
摘要翻译：通过选择性氢化烯属杂质制备基本上不含烯属杂质的氢氯氟烃的方法。可以控制该方法，使得至少一部分氢氯氟烃转化为氟代烃。

8. 发明授权

US4892642A Process for the production of mesophase 失效
标题翻译：中间相生产工艺
公开(公告)号：US4892642A
公开(公告)日：1990-01-09
申请号：US298536
申请日：1989-01-17
申请人： Hugh E. Romine , Ta-Wei Fu
发明人： Hugh E. Romine , Ta-Wei Fu
IPC分类号： C10C3/00 , C10C3/04 , C10C3/08 , C10C3/10 , D01F9/145
CPC分类号： C10C3/08 , C10C3/002 , C10C3/04
摘要： An improved process for producing an anisotropic pitch product suitable for carbon fiber manufacture. A carbonaceous feedstock substantially free of mesophase pitch is heated at elevated temperature while passing an oxidatively reactive sparging gas such as air through the feedstock. The oxidatively treated feedstock, which contains isotropic pitch, is solvent fractionated to recover a solid pitch which on fusion becomes an anisotropic pitch product having from 50 to 100 percent by volume mesophase. In one aspect of the invention the carbonaceous feedstock is oxidatively treated in a melt phase at a lower temperature and the resulting isotropic pitch is then heated at a higher temperature in a melt phase in the presence or absence of a non-oxidative sparging gas prior to solvent fractionation.
摘要翻译：一种用于生产适用于碳纤维制造的各向异性沥青产品的改进方法。基本上不含中间相沥青的碳质原料在升高的温度下加热，同时使氧化反应性的鼓泡气体如空气通过原料。包含各向同性沥青的经氧化处理的原料被溶剂分馏以回收固体沥青，其在熔化时成为具有50至100体积％中间相的各向异性沥青产物。在本发明的一个方面，碳质原料在较低温度下在熔融相中进行氧化处理，然后在存在或不存在非氧化性鼓泡气体的情况下，在熔融相中将所得各向同性沥青加热，溶剂分馏。

9. 发明授权

US4959139A Binder pitch and method of preparation 失效
标题翻译：粘合剂沥青及其制备方法
公开(公告)号：US4959139A
公开(公告)日：1990-09-25
申请号：US295425
申请日：1989-01-09
申请人： Dave L. Blakeburn, II , Ta-Wei Fu , Keith M. Roussel
发明人： Dave L. Blakeburn, II , Ta-Wei Fu , Keith M. Roussel
IPC分类号： C04B35/52 , C10C3/00 , C10C3/02
CPC分类号： C10C3/00
摘要： Binder pitch is prepared by combining a petroleum aromatic mineral oil thermal tar and super finely subdivided calcined premium coke particles. The petroleum aromatic mineral oil thermal tar is obtained by hydrotreating, thermally cracking and vacuum distilling an aromatic mineral oil. Additionally, the aromatic mineral oil thermal tar may be subjected to heat soaking.

10. 发明授权

US4892641A Process for the production of mesophase pitch 失效
标题翻译：生产中间相沥青的方法
公开(公告)号：US4892641A
公开(公告)日：1990-01-09
申请号：US308600
申请日：1989-02-08
申请人： Ta-Wei Fu , Manfred Katz
发明人： Ta-Wei Fu , Manfred Katz
IPC分类号： C10C3/00 , C10C3/04
CPC分类号： C10C3/002 , C10C3/04
摘要： An improved process for producing an anisotropic pitch product suitable for carbon fiber manufacture. A carbonaceous feedstock substantially free of mesophase pitch is heated at elevated temperature while passing an oxidatively reactive sparging gas such as air through the feedstock. The oxidatively treated feedstock, which remains substantially free of mesophase pitch, is then heated at a higher temperature in the presence of a non-oxidative sparging gas to produce an anisotropic pitch having from 50 to 100% by volume mesophase which is suitable for producing good quality carbon fibers.

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