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1. 发明公开

EP1947131A4 OPTICAL DEVICE AND ACHROMATIC LENS 审中-公开
标题翻译：光学装置和消色差透镜
公开(公告)号：EP1947131A4
公开(公告)日：2010-10-27
申请号：EP06823393
申请日：2006-11-08
申请人： TEIJIN CHEMICALS LTD
发明人： HATANAKA KUNIO , IMANAKA YOSHIHIKO , MONRI MASANORI
IPC分类号： C08G64/10 , C08K3/32 , C08K5/10 , C08K5/53 , C08L69/00 , G02B1/04
CPC分类号： G02B1/04 , C08G64/10 , G02B1/041 , G02B27/0037 , G02B27/4211 , G02B27/4272 , C08L69/00

2. 发明专利

JPH11240849A BROMINE COMPOUND AND ITS PRODUCTION 失效
公开(公告)号：JPH11240849A
公开(公告)日：1999-09-07
申请号：JP32042798
申请日：1998-11-11
申请人： TEIJIN CHEMICALS LTD
发明人： TAKEYA YUTAKA , MONRI MASANORI , TANABE SEIICHI , SHIMIZU YASUHIRO , HOSHIMI HARUHISA
IPC分类号： C07C41/22 , C07C43/225 , C07C315/04 , C07C317/20 , C07C317/22 , C07C319/20 , C07C323/17 , C07C323/20 , C08K5/06 , C08L101/00 , C09K21/08
摘要： PROBLEM TO BE SOLVED: To produce a highly pure bromine compound excellent in heat stability by reacting a solution obtained by dissolving a compound having an aliphatic unsaturated bond in a halogenated aliphatic hydrocarbon solution with a bromine-mixed solution in the presence of a specific compound having hydroxy group. SOLUTION: This method for producing a bromine compound by mixing and reacting a solution of (A) a compound of the formula R -O-Ar -Y-Ar -O-R (Ar and Ar are each a 5-16C aromatic hydrocarbon or the like; Y is sulfone or the like; R and R are each a 2-11C hydrocarbon having an aliphatic unsaturated group), e.g. 2,2-bis[(3,5-dibromo-4-allyloxy)phenyl]propane} dissolved in (B) a halogenated aliphatic hydrocarbon solvent with bromine or a solution of the bromine comprises using (C) a compound of the formula R -(OH)u [R is a (u)-valent 1-6C aliphatic group; (u) is 1-4] in an amount corresponding to 0.5-20 hydroxy groups based on 100 unsaturated groups of the component A in the bromine-mixed solution.

3. 发明专利

JPH0527101A PLASTIC LENS 失效
公开(公告)号：JPH0527101A
公开(公告)日：1993-02-05
申请号：JP20355591
申请日：1991-07-19
申请人： TEIJIN CHEMICALS LTD
发明人： MONRI MASANORI , OTSUBO HIROKI , TOKUDA TOSHIMASA
IPC分类号： C08L25/12 , C08L69/00 , G02B1/04
摘要： PURPOSE:To improve transparency, workability, and dimensional stability by forming a lens from a mixture of each specified polycarbonate resin and acrylonitrile-styrene copolymer. CONSTITUTION:This lens is formed from a mixture of 90-10wt.% of polycarbonate resin having 0.451-1.176 specific viscosity essentially comprising the recurring unit expressed by formula I and 10-90wt.% of acrylonitrile-styrene copolymer. This copolymer contains 5-15wt.% of acrylonitrile to the weight of the copolymer and 30000-600000 weight means mol.wt. In formula I, X is an alkylidene group of 2-6 carbon number, cycloalkyidene group of 5-6 carbon number, and -S- or -SO2-. The bivalent phenol compd. which constitutes the recurring unit expressed by formula I is bis(4-hydroxy-3,5dimethylphenyl)propane,bis(4- hydroxy-3,5-dimethylphenyl)methane, etc., and these may be used in a single form or a mixture of two or more.

4. 发明专利

JPH0333242B2 失效
公开(公告)号：JPH0333242B2
公开(公告)日：1991-05-16
申请号：JP21109885
申请日：1985-09-26
申请人： TEIJIN CHEMICALS LTD
发明人： MYAUCHI MASAYOSHI , MONRI MASANORI
IPC分类号： G02B1/04 , C08G64/24 , C08K3/00 , C08L69/00

5. 发明专利

JP2002097195A METHOD FOR PRODUCING SPIROCYCLIC DERIVATIVE 失效
公开(公告)号：JP2002097195A
公开(公告)日：2002-04-02
申请号：JP2000286780
申请日：2000-09-21
申请人： TEIJIN CHEMICALS LTD
发明人： MONRI MASANORI , TAKEYA YUTAKA
IPC分类号： C07F9/6574
摘要： PROBLEM TO BE SOLVED: To provide a purifying method with good operability for obtaining a high-quality spirocyclic derivative in high yield. SOLUTION: The objective method for producing a specific spirocyclic derivative comprises reaction between pentaerythritol and at least one specific phosphorus compound; wherein the method is characterized by involving the following process: a crude spirocyclic derivative formed by the above reaction is mixed with hot water at 40-90 deg.C under agitation followed by separation and purification.

6. 发明专利

JPH06322022A METHOD FOR PURIFYING POLYSTYRENE BROMINATION SOLUTION 失效
公开(公告)号：JPH06322022A
公开(公告)日：1994-11-22
申请号：JP11294793
申请日：1993-05-14
申请人： TEIJIN CHEMICALS LTD
发明人： IKEMURA YOSHIFUMI , FUJII KOJI , AIDA SHINICHI , MONRI MASANORI
IPC分类号： C08F8/20 , C08F8/22 , C08F12/00 , C08F12/08
摘要： PURPOSE:To completely and easily remove hydrogen bromide and a Friedel- Crafts catalyst from the bromination soln. to thereby obtain a brominated poly styrene excellent in heat resistance by putting the soln. into a specified amt. of water in the process for porducing the brominated polystyrene by reacting polystyrene with bromine in an org. solvent in the presence of the catalyst. CONSTITUTION:Polystyrene having a wt. average mol. wt. of 10,000-5000,000 is brominated and purified by dessolving the resin in an org, solvent, pref. a satd. aliph. halogenated hydrocarbon (e. g. methylene chloride), adding a Friedel-Crafts catalyst (e. g. aluminum chloride) to the resin soln. in an amt. of 110mol% based on the benzene ring of the resin, adding a brominating agent (e. g. bromine) in an amt. of 1-3.3mol based on 1mol of the benzene ring of the resin dropwise to the soln. to brominate the resin, putting the reaction soln. into 0.3-10 times as much water after completion of the bromination, and extracting the water layer with the solvent.

7. 发明专利

JPH11139996A PRODUCTION OF BROMINE COMPOUND 失效
公开(公告)号：JPH11139996A
公开(公告)日：1999-05-25
申请号：JP23428898
申请日：1998-08-20
申请人： TEIJIN CHEMICALS LTD
发明人： TAKEYA YUTAKA , MONRI MASANORI , TANABE SEIICHI , SHIMIZU YASUHIRO , HOSHIMI HARUHISA
IPC分类号： C07B39/00 , C07C41/22 , C07C43/225 , C07C45/63 , C07C49/577 , C07C49/84 , C07C315/04 , C07C317/22 , C07C319/20 , C07C323/20 , C09K21/08
摘要： PROBLEM TO BE SOLVED: To obtain the subject high-purity compound in a high yield without causing a side reaction, by carrying out the reaction between an aliphatic unsaturated compound and bromine in an inert solvent and removing a reaction heat out of the system by using the evaporation heat of the solvent or bromine. SOLUTION: A compound of formula I (Ar and Ar are each a 5-6C aromatic hydrocarbon or a 5-12C saturated alicyclic hydrocarbon; Y is a 1-6C saturated hydrocarbon, a ketone or the like; R and R are each an aliphatic unsaturated group-containing 2-11C hydrocarbon) is reacted with bromine in the presence of an inert solvent (preferably methylene chloride or the like) while removing the substantial amount of the reaction heat out of the system by the vaporization heat of the solvent or bromine to give the objective compound of formula II (R and R are each a group obtained by saturating the unsaturated group of R or R , respectively). 2,2-Bis (3,5-dibromo-4-allyloxy)phenyl}propane is preferable as the compound of formula I.

8. 发明专利

JPH11130716A PRODUCTION OF BROMINE COMPOUND 失效
公开(公告)号：JPH11130716A
公开(公告)日：1999-05-18
申请号：JP23736598
申请日：1998-08-24
申请人： TEIJIN CHEMICALS LTD
发明人： TAKEYA YUTAKA , MONRI MASANORI , TANABE SEIICHI , SHIMIZU YASUHIRO
IPC分类号： C07C41/22 , C07C43/225
摘要： PROBLEM TO BE SOLVED: To provide a method for efficiently producing a high-purity bromine compound in a short time by a compact and simple apparatus by continuously feeding a specific compound, a specific amount of bromine and a specific solvent to a reactor and removing reaction heat by a specific method. SOLUTION: (A) A compound having an aliphatic unsaturated bond of formula I [Ar and Ar are each a (halogen-substituted) 5-16C aromatic hydrocarbon or the like; Y is a 1-6C saturated hydrocarbon or the like; R and R are each a 2-11C hydrocarbon having aliphatic unsaturated group and in either one of R and R , a halogen may be added to a part of the unsaturated group], (B) bromine in an amount corresponding to number of 1-5 bromine molecules per unsaturated group in the component A and (C) a solvent which is inert to reaction are continuously fed to a reactor and reaction of the compound A with the compound B is carried out while removing substantial amount of reaction heat by vaporization heat of component B or A and the reaction mixture is taken to continuously provide the objective bromine compound of formula II (R and R are each a group in which unsaturated groups of R and R are saturated by bromine).

9. 发明专利

JPH10130325A PRODUCTION OF HALOGENATED STYRENE POLYMER 失效
公开(公告)号：JPH10130325A
公开(公告)日：1998-05-19
申请号：JP28968996
申请日：1996-10-31
申请人： TEIJIN CHEMICALS LTD
发明人： MONRI MASANORI
IPC分类号： C08F4/06 , C08F8/20 , C08F12/08
摘要： PROBLEM TO BE SOLVED: To simply and economically obtain the subject polymer of highly halogenated styrene excellent in thermal stability in a high yield by using a reaction product between a Lewis acid and a nucleophilic substance as a polymerization catalyst in one reaction solution. SOLUTION: (A) unsaturated monomers comprising (i) 50-100wt.% of styrene monomer and (ii) 0-50wt.% of a monomer cationically copolymerizable with the styrene monomer are polymerized in the presence of (B) a catalyst and (C) the styrene polymer product is halogenated. In this case, (B) the polymerization catalyst is prepared by reaction of (iii) a Lewis acid represented by the formula [Me is a tri- or tetravalent metal atom; X is a halogen; R is H, a 1-6C alkyl, an aliphatic amine; a is 3, 4, (a-x)/x is 0-999] with (iv) a nucleophilic substance, used in an amount of 0.001-10 pts.wt. per 100 pts.wt. of the component A to effect cationic polymerization. Then, the resultant styrene polymer is halogenated using a Lewis acid as a halogenation catalyst in an amount of 0.01-20 pts.wt. per 100 pts.wt. of the styrene polymer.

10. 发明专利

JPH04246416A PRODUCTION OF AROMATIC POLYCARBONATE 失效
公开(公告)号：JPH04246416A
公开(公告)日：1992-09-02
申请号：JP2914891
申请日：1991-01-31
申请人： TEIJIN CHEMICALS LTD
发明人： TOKUDA TOSHIMASA , MONRI MASANORI
IPC分类号： C08G64/22 , C08G64/20
摘要： PURPOSE:To prepare a polycarbonate with excellent optical characteristics such as high refractive index or low birefringence index and excellent hue and transparency and which is not of bisphenol A type. CONSTITUTION:In the interfacial polycondensation of a dihydric phenol except 2,2-bis(4-hydroxyphenyl)propane with phosgene in the presence of an org. solvent to prepare and arom. polycarbonate, phosphorous acid and/or phosphite is added to an alkaline watery soln. of the dihydric phenol to perform phosgene reaction.

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