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    • 2. 发明专利
    • Method for manufacturing r-t-b magnet
    • 制造R-T-B磁铁的方法
    • JP2009295638A
    • 2009-12-17
    • JP2008145068
    • 2008-06-02
    • Tdk CorpTdk株式会社
    • KOGA TOSHIYUKINISHIZAWA KOICHIFUKAZAWA ARITERUISHIZAKA TSUTOMU
    • H01F41/02B22F3/00B22F3/10B22F3/24C22C38/00H01F1/053
    • PROBLEM TO BE SOLVED: To provide a method for manufacturing an R-T-B magnet capable of suppressing fluctuation in a composition of a molded body in baking, improving magnetic characteristics of the obtained R-T-B magnet and preventing a variation in the magnetic characteristics accompanied by the fluctuation in the composition of the R-T-B magnet. SOLUTION: This method for manufacturing an R-T-B magnet comprises: a molding step of forming a molded body of a magnetic material, a temperature rise step of heating the molded body to raising the temperature of the molded body up to a baking temperature T s °C, and a temperature maintaining step of maintaining the temperature of the molded body at T s °C. In the temperature rise step or the temperature maintaining step, the atmosphere is switched from a vacuum atmosphere to an inert gas atmosphere, and switching from the vacuum atmosphere to the inert gas atmosphere is executed before a time point t 1 and after a time point t 2 , where t 1 is a time point when the temperature of the molded body reaches T s °C, and t 2 is a time point when the temperature of the molded body reaches T s °C and 50 minutes have not elapsed while maintaining the temperature at T s °C after t1. COPYRIGHT: (C)2010,JPO&INPIT
    • 要解决的问题:为了提供一种制造能够抑制烘焙中的成型体的组成变动的RTB磁体的方法,改善所获得的RTB磁体的磁特性,并防止伴随着 RTB磁体的组成波动。 解决方案:这种制造RTB磁体的方法包括:形成磁性材料成型体的成型步骤,加热成型体以将成型体的温度升高到烘烤温度T的升温步骤 < SB>℃,以及将成型体的温度保持在T SB>℃的温度保持步骤。 在升温步骤或温度保持步骤中,将气氛从真空气氛切换到惰性气体气氛,并且在时间点t 1 并且在t 2 的时间点之后,其中t 1 是成型体的温度达到T S ℃的时间点, 并且t 2 是当成型体的温度达到T S S时的时间点,并且在保持温度为T S时没有经过50分钟, / SB>℃。 版权所有(C)2010,JPO&INPIT
    • 3. 发明专利
    • Method for producing rare earth permanent magnet
    • 生产稀土永磁体的方法
    • JP2007270164A
    • 2007-10-18
    • JP2006093764
    • 2006-03-30
    • Tdk CorpTdk株式会社
    • ISHIZAKA TSUTOMUKATO EIJI
    • B22F3/00B22D11/06B22F1/00B22F3/02B22F3/10B22F9/04C21D6/00C22C38/00
    • PROBLEM TO BE SOLVED: To provide a method for producing a rare earth permanent magnet where an R-T-B based rare earth permanent magnet in which variation in coercive force is suppressed, and which has satisfactory magnetic properties can be stably produced. SOLUTION: Raw material alloy pieces in the same lot formed from the same molten metal are sampled by a prescribed number N of pieces. Then, the ratio between the average crystal grain diameter D1 in one face side in the sampled respective raw material alloy pieces and the average crystal grain diameter D2 in the other face side, D1/D2 is calculated. In the sampled number N of pieces of raw material alloy pieces, the number n of pieces of the raw material alloy pieces in which the ratio D1/D2 satisfies a predetermined standard value or above is calculated, and the abundance ratio of the raw material alloy pieces in which the ratio D1/D2 satisfies the predetermined standard value or above, i.e., including coarse grains, n/N is obtained. Then, only the group of the raw material alloy pieces in the lot in which the abundance ratio n/N satisfies the fixed value or below is fed to a pulverization stage, thus an R-T-B based permanent magnet having high coercive force is produced. COPYRIGHT: (C)2008,JPO&INPIT
    • 解决的问题:为了提供一种稀土永磁体的制造方法,其中可以稳定地制造矫顽力的变化被抑制的R-T-B系稀土永磁体。

      解决方案:由相同熔融金属形成的同批次中的原材料合金片由规定数量的N片取样。 然后,计算取样的各原料合金片中的一个面侧的平均晶粒直径D1与另一面的平均晶粒直径D2之比D1 / D2。 在取样数量N的原料合金片中,计算比率D1 / D2满足规定标准值以上的原料合金片数n,原料合金的丰度比 比率D1 / D2满足预定标准值以上,即包括粗晶粒,n / N的片。 然后,仅将丰度比n / N满足固定值以下的批次中的原料合金块的一组进料到粉碎阶段,由此制造具有高矫顽力的R-T-B系永久磁铁。 版权所有(C)2008,JPO&INPIT

    • 4. 发明专利
    • Rare earth permanent magnet
    • 稀土永磁体
    • JP2006295140A
    • 2006-10-26
    • JP2006066733
    • 2006-03-10
    • Tdk CorpTdk株式会社
    • NAKANE MAKOTOKATO EIJIISHIZAKA TSUTOMUOJI NAOTO
    • H01F1/053C21D6/00C22C33/02C22C38/00H01F1/08
    • PROBLEM TO BE SOLVED: To obtain a rare earth permanent magnet exhibiting excellent magnetic characteristics such as residual magnetic flux and coercive force in which productivity can be enhanced by expanding both the sintering temperature width and the aging temperature width. SOLUTION: The rare earth permanent magnet has a composition of 25-35 wt.% of R (R is one kind or more than one kind selected from rare earth elements), 0-4 wt.% of Co (excluding 0), 0.5-4.5 wt.% of B, 0.02-0.6 wt.% of one kind or more than one kind selected from Cu and Al, 0.03-0.25 wt.% of Zr, 0.05-0.25 wt.% of Ga, 0.03-0.2 wt.% of O, and the reminder of Fe and inevitable impurities. COPYRIGHT: (C)2007,JPO&INPIT
    • 解决的问题:为了获得具有优异的磁特性(例如剩余磁通量和矫顽力)的稀土永磁体,通过扩大烧结温度宽度和老化温度宽度,可提高生产率。 解决方案:稀土永磁体的组成为R(R是选自稀土元素中的一种或多于一种)的25-35重量%,Co的0-4重量%(不包括0 ),0.5-4.5重量%的B,0.02-0.6重量%的一种或多于一种选自Cu和Al,0.03-0.25重量%的Zr,0.05-0.25重量%的Ga,0.03 -0.2重量%的O,以及Fe和不可避免的杂质的提醒。 版权所有(C)2007,JPO&INPIT
    • 5. 发明专利
    • Manufacturing method of rtb-based sintered magnet
    • 基于RTB的烧结磁体的制造方法
    • JP2006165008A
    • 2006-06-22
    • JP2004349400
    • 2004-12-02
    • Tdk CorpTdk株式会社
    • NISHIZAWA KOICHIISHIZAKA TSUTOMUOJI NAOTO
    • H01F1/08B22D11/06B22D23/00B22F1/00C22C33/02C22C38/00H01F1/053H01F41/02
    • PROBLEM TO BE SOLVED: To obtain an RTB-based sintered magnet having magnetic characteristics and particularly high coersive force, by utilizing a main-phase forming alloy manufactured by the centrifugal casting method and a particle-phase forming alloy which has been manufactured by strip casting method. SOLUTION: The manufacturing method of the RTB system sintered magnet includes a process to obtain a molding body with the pressurized molding process while applying a magnetic field to the mixed powder including the alloy powder for main-phase forming including the R 2 T 14 B compound and the alloy powder for particle-phase forming including R in the amount larger than that of the alloy powder for main-phase forming and a process to sinter the molding element. The alloy powder for main-phase forming has been manufactured, by milling the alloy which has been obtained by depositing and solidifying the splashed molten metal 4 at the internal surface of a rotating cylindrical casting die 3, through contact with a rotating body 6 under the condition that the rotating axis X of the rotating body 6 and the rotating axis Z of the cylindrical casting die 3 be allocated in parallel. The alloy powder for particle-phase forming has been manufactured, by milling the alloy which has been obtained through strip casting method. COPYRIGHT: (C)2006,JPO&NCIPI
    • 要解决的问题为了获得具有磁特性和特别高的共强力的RTB型烧结磁体,通过利用由离心铸造法制造的主相成形合金和已经制造的颗粒相形成合金 通过带铸法。 解决方案:RTB系烧结磁体的制造方法包括在包含包括R SB的主相成型用合金粉末的混合粉末中施加磁场的情况下,通过加压成型工序获得成型体的工序 > 2 T 14 B化合物和用于颗粒相形成的合金粉末,其包含R的量大于用于主相成型的合金粉末的量,以及烧结成型 元件。 已经通过在旋转的圆柱形铸模3的内表面上沉积和固化溅出的熔融金属4而获得的合金,通过与旋转体6的内部的旋转体6接触来制造用于主相成型的合金粉末 条件是旋转体6的旋转轴线X和圆筒形铸模3的旋转轴线Z被并列分配。 已经通过研磨通过带状铸造法获得的合金来制造用于颗粒相成形的合金粉末。 版权所有(C)2006,JPO&NCIPI
    • 6. 发明专利
    • Rare earth sintered magnet and its producing process
    • 稀土烧结磁铁及其生产工艺
    • JP2006128426A
    • 2006-05-18
    • JP2004315196
    • 2004-10-29
    • Tdk CorpTdk株式会社
    • ENOKIDO YASUSHINISHIZAWA KOICHIISHIZAKA TSUTOMU
    • H01F1/08B22F3/24C22C38/00H01F41/02
    • PROBLEM TO BE SOLVED: To provide a rare earth sintered magnet in which pealing strength of a protective film can be ensured for stress impartment. SOLUTION: A rare earth sintered magnet comprises a rare earth sintered magnet body having anisotropy in surface roughness, and a protective film formed on the surface of the rare earth sintered magnet body. When a grinding mark is formed on the surface of the rare earth sintered magnet body along one predetermined direction, it can be said that the rare earth sintered magnet body has anisotropy in surface roughness. Furthermore, it can be said that the rare earth sintered magnet body has anisotropy in surface roughness when following relation is satisfied between the surface roughness Ra1 (arithmetic mean surface roughness) of the rare earth sintered magnet body in the predetermined direction and the surface roughness Ra2 in the direction intersecting the predetermined direction perpendicularly; Ra2≥1.1×Ra1. COPYRIGHT: (C)2006,JPO&NCIPI
    • 要解决的问题:提供一种能够确保保护膜的剥离强度的稀土烧结磁体。 解决方案:稀土烧结磁体包括具有表面粗糙度各向异性的稀土烧结磁体和形成在稀土烧结磁体的表面上的保护膜。 当沿着一个预定方向在稀土烧结磁体的表面上形成磨痕时,可以说稀土烧结磁体具有各向异性的表面粗糙度。 此外,可以说,稀土烧结磁体在预定方向的表面粗糙度Ra1(算术平均表面粗糙度)与表面粗糙度Ra2(算术平均表面粗糙度)之间的关系满足时,表面粗糙度各向异性 在与预定方向垂直的方向上; Ra2≥1.1×器Ra1。 版权所有(C)2006,JPO&NCIPI
    • 7. 发明专利
    • Method for producing raw powder for rare earth sintered magnet and method for producing rare earth sintered magnet
    • 用于生产稀土烧结磁体的原始粉末的方法和用于生产稀土烧结磁体的方法
    • JP2006016644A
    • 2006-01-19
    • JP2004193726
    • 2004-06-30
    • Tdk CorpTdk株式会社
    • BABA FUMITAKAENOKIDO YASUSHIISHIZAKA TSUTOMUMASUDA TAKESHI
    • B22F1/00C22C19/07C22C33/02C22C38/00H01F1/053H01F1/08H01F41/02
    • PROBLEM TO BE SOLVED: To produce raw powder for a rare earth sintered magnet using granules having excellent fluidity and capable of attaining the improvement in the dimensional precision of a compact and the improvement of productivity. SOLUTION: This method for producing raw powder for a rare earth sintered magnet is provided with: a stage where primary alloy grains having a prescribed composition are added with a first organic liquid and a liquid component having saturated vapor pressure higher than that of the first organic liquid to obtain a mixture; and a stage where granules composed of the primary alloy grains are producing using the mixture. As the liquid component, a second organic liquid having a saturated vapor pressure higher than that of the first organic liquid is desirably used, and, it is desirable that, to the primary alloy grains, the first organic liquid is added by ≤6.0 wt% (exclusive of zero), and the second organic liquid is added by ≤15.0 wt.% (exclusive of zero). COPYRIGHT: (C)2006,JPO&NCIPI
    • 要解决的问题:使用具有优异的流动性的颗粒制造稀土烧结磁体的原料粉末,并且能够获得小型化的尺寸精度的提高和生产率的提高。 解决方案:该稀土类烧结磁体用粉末的制造方法具备:将具有规定成分的一次合金粒子添加有第一有机液体和饱和蒸气压高于 第一种有机液体得到混合物; 以及使用该混合物制造由一次合金粒子构成的颗粒的阶段。 作为液体成分,优选使用饱和蒸气压高于第一有机液体的第二有机液体,对于一次合金粒子,优选添加≤6.0重量%的第一有机液体, (不包括零),第二有机液体加入≤15.0重量%(不包括零)。 版权所有(C)2006,JPO&NCIPI