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1. 发明专利

ES2410057T3 Procedimiento para producir 1,3-propanodiol 未知
公开(公告)号：ES2410057T3
公开(公告)日：2013-06-28
申请号：ES11158112
申请日：2004-05-06
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC分类号： B01D11/00 , B01D11/04 , C02F1/00 , C02F1/26 , C02F1/44 , C07C29/86 , C07C31/18 , C12P7/04 , C12P7/14
摘要： Un procedimiento para recuperar 1,3-propanodiol de un caldo de fermentación que comprende 1,3-propanodiol, que comprende las etapas de: poner en contacto un caldo de fermentación que contiene agua, 1,3-propanodiol y al menos uncontaminante con al menos un disolvente de extracción para formar una primera mezcla yseparar la primera mezcla en una primera fase y una segunda fase, en el cual la primera fase comprende la mayor parte del disolvente de extracción y al menos parte del 1,3-propanodiol que estaba presente en el caldo de fermentación y la relación de pesos de 1,3-propanodiol acualquier contaminante presente en la primera fase es mayor que la relación de pesos de 1,3-propanodiol almismo contaminante en el caldo de fermentación antes de que se haya puesto en contacto con eldisolvente de extracción y en el que la segunda fase comprende la mayor parte del agua y al menos alguno de los contaminantes delcaldo de fermentación; de modo que dicho procedimiento comprende además: ajustar la temperatura de la primera mezcla durante la etapa de puesta en contacto de tal modo que el 1,3-propanodiol sea más soluble en el disolvente de extracción que en el caldo de fermentación, donde eldisolvente de extracción es hexanol; separar la primera mezcla en la primera fase y la segunda fase; retirar la primera fase de la segunda fase; ajustar la temperatura de la primera fase de tal modo que se forme una segunda mezcla; y separar la segunda mezcla en una tercera fase y una cuarta fase, de modo que la tercera fase comprendela mayor parte del hexanol de la primera fase y la cuarta fase comprende 1,3-propanodiol; en el que la relación de pesos, en la cuarta fase, de 1,3-propanodiol a cualquier contaminante presente esmayor que la relación de pesos de 1,3-propanodiol al mismo contaminante en el caldo de fermentaciónantes de que el caldo de fermentación se haya puesto en contacto con el disolvente de extracción.

2. 发明专利

NO20055383L 未知
公开(公告)号：NO20055383L
公开(公告)日：2005-12-02
申请号：NO20055383
申请日：2005-11-14
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC分类号： B01D11/00 , B01D11/04 , C02F1/26 , C07C29/86
摘要： Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

3. 发明专利

ES2505541T3 Proceso para producir 1,3-propanodiol 未知
公开(公告)号：ES2505541T3
公开(公告)日：2014-10-10
申请号：ES11158110
申请日：2004-05-06
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM M , JANSEN ROBERT P , VITTNER ASHER , BAIADA ANTHONY
IPC分类号： B01D11/04 , C02F1/26 , C07C29/86
摘要： Un proceso para la recuperación de 1,3-propanodiol a partir de un caldo de fermentación que comprende 1,3-propanodiol y que comprende las etapas consistentes en: poner en contacto un caldo de fermentación que comprende agua, 1,3-propanodiol, y al menos un contaminante con al menos un disolvente de extracción para formar una primera mezcla, y separar la primera mezcla en una primera fase y una segunda fase, donde la primera fase comprende una mayoría del disolvente de extracción y al menos parte del 1,3-propanodiol que estaba presente en el caldo de fermentación, y la relación de peso en la primera fase de 1,3-propanodiol con respecto a cualquier contaminante presente es mayor que la relación de peso de 1,3-propanodiol con respecto al mismo contaminante en el caldo de fermentación antes de que el caldo de fermentación entre en contacto con el disolvente de extracción, y donde la segunda fase comprende una mayoría del agua y al menos parte del contaminante del caldo de fermentación; y recuperar 1,3-propanodiol eliminando la primera fase de la segunda fase; donde la primera fase eliminada comprende además al menos un poco de agua, y donde el proceso comprende además la etapa consistente en poner en contacto la primera fase eliminada con al menos un disolvente hidrófobo para formar una segunda mezcla, separar la segunda mezcla en una tercera fase y una cuarta fase, donde la tercera fase comprende a la vez la mayoría del disolvente de extracción y del disolvente hidrófobo de la segunda mezcla, donde la cuarta fase comprende 1,3-propanodiol y la mayoría del agua de la primera fase, y donde la relación de peso en la cuarta fase de 1,3-propanodiol con respecto a cualquier contaminante presente es mayor que la relación de peso de 1,3-propanodiol con respecto al mismo contaminante en el caldo de fermentación antes de que el caldo de fermentación entre en contacto con el disolvente de extracción.

4. 发明专利

NO20055383A 未知
公开(公告)号：NO20055383A
公开(公告)日：2005-12-02
申请号：NO20055383
申请日：2005-11-14
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC分类号： B01D11/00 , B01D11/04 , C02F1/26 , C07C29/86
CPC分类号： C07C29/86 , B01D11/0446 , B01D11/0488 , B01D11/0492 , C02F1/26 , C07C31/205
摘要： Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

5. 发明专利

AU2004238804B2 Process for producing 1, 3-propanediol 未知
公开(公告)号：AU2004238804B2
公开(公告)日：2009-03-12
申请号：AU2004238804
申请日：2004-05-06
申请人： TATE & LYLE INGREDIENTS AMERICAS LLC
发明人： BAIADA ANTHONY , BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER
IPC分类号： B01D11/04 , C02F1/26 , C07C29/86
摘要： Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

6. 发明专利

BRPI0410680A 未知
公开(公告)号：BRPI0410680A
公开(公告)日：2006-06-20
申请号：BRPI0410680
申请日：2004-05-06
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC分类号： B01D11/04 , C02F1/26 , C07C29/86 , B01D11/00 , C02F1/44 , C02F1/00 , C12P7/04 , C12P7/14 , C07C31/18
摘要： Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

7. 发明专利

BRPI0410680B1 未知
公开(公告)号：BRPI0410680B1
公开(公告)日：2014-07-08
申请号：BRPI0410680
申请日：2004-05-06
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC分类号： B01D11/00 , B01D11/04 , C02F1/00 , C02F1/26 , C02F1/44 , C07C29/86 , C07C31/18 , C12P7/04 , C12P7/14
摘要： Disclosed herein is a process for the recovery of 1,3-propanediol from an aqueous feed stream. The present invention involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The first phase is removed from the separated second phase and is contacted with at least one hydrophobic solvent to form a second mixture. The second mixture is separated into a third phase and a fourth phase. The third phase comprises the majority of both the solvent extractant and the hydrophobic solvent. The fourth phase comprises 1,3-propanediol and the majority of the water of the first phase. The weight ratio in the fourth phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant.

8. 发明专利

UA84289C2 СПОСОБ ВЫТЯГИВАНИЯ 1,3-ПРОПАНДИОЛА ИЗ ФЕРМЕНТАТИВНОГО БУЛЬОНА 未知
公开(公告)号：UA84289C2
公开(公告)日：2008-10-10
申请号：UAA200511455
申请日：2004-05-06
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC分类号： C12P7/18 , B01D11/04 , C02F1/26 , C07C29/76 , C07C29/86 , C07C31/00
摘要： Изобретениеотноситсяк способуэкстракции 1,3-пропандиолаизферментативногобульона, которыйвключаетконтактированиеферментативногобульона, содержащеговоду, 1,3-пропандиоли хотябыоднупримесь, с, какминимум, однимэкстрагентомс образованиемсмеси. Смесьразделяютнапервуюи вторуюфазу. Втораяфазавключаетбольшуючастьводыс водногопотокаматериала, которыепоступает. Перваяфазавключаетэстрагенти хотябынекотороеколичество 1,3-пропандиола, которыеприсутствовалв водномпотокематериала, которыепоступает. Массовоесоотношение 1,3-пропандиолак любойоднойизприсутствующихпримесейв первойфазебольше, чеммассовоесоотношение 1,3-пропандиолак тойжепримесив водномпотокематериала, которыйпоступает, дотого, какводныйпотокматериала, которыйпоступает, былвведенв контактс экстрагеном.

9. 发明专利

NZ543388A Process for producing 1,3-propanediol 未知
公开(公告)号：NZ543388A
公开(公告)日：2008-07-31
申请号：NZ54338804
申请日：2004-05-06
申请人： TATE & LYLE INGREDIENTS
发明人： BANIEL AVRAHAM M , JANSEN ROBERT P , VITNER ASHER , BAIADA ANTHONY
IPC分类号： B01D11/04 , C02F1/26 , C07C29/86 , B01D11/00 , C02F1/44 , C02F1/00 , C12P7/04 , C12P7/14 , C07C31/18
摘要： Disclosed herein are processes for the recovery of 1,3-propanediol from an aqueous feed stream. The process involves contacting an aqueous feed stream that comprises water, 1,3-propanediol, and at least one contaminant with at least one solvent extractant to form a mixture. The mixture is separated into a first phase and a second phase. The second phase comprises a majority of the water from the aqueous feed stream. The first phase comprises solvent extractant and at least some of the 1,3-propanediol that was present in the aqueous feed stream. The weight ratio in the first phase of 1,3-propanediol to any one contaminant present is greater than the weight ratio of 1,3-propanediol to the same contaminant in the aqueous feed stream prior to the aqueous feed stream being contacted with the solvent extractant. The first phase can be removed from the separated second phase in order to recover the 1,3-propanediol.

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