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1. 发明公开

EP1310789A3 Rapid characterization of polymers with temperature control in a mixing zone 审中-公开
标题翻译：通过聚合物的快速表征在混合区中的温度控制下进行
公开(公告)号：EP1310789A3
公开(公告)日：2004-08-04
申请号：EP03003138.9
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/02 , G01N33/44 , G01N30/88
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterizing a non-biological polymer sample, the method comprising injecting a polymer sample into a mobile-phase of a liquid chromatography system, the mobile-phase being supplied to a liquid chromatography column from a mixing zone, the mixing zone being in fluid communication with a first reservoir containing a first mobile phase fluid at a first temperature, and with a second reservoir containing a second mobile phase fluid at a second temperature, controlling the temperature of the mobile-phase in the mixing zone to vary over time by varying the relative amounts of the first and second mobile-phase fluids supplied to the mixing zone, separating one or more sample components of the polymer sample in the chromatography column, and detecting a property of at least one of the separated sample components.

2. 发明公开

EP1310791A2 Rapid characterization of polymers with a high-aspect ratio column 审中-公开
标题翻译：通过具有高的长度对直径的比率列的装置的聚合物的快速表征
公开(公告)号：EP1310791A2
公开(公告)日：2003-05-14
申请号：EP03003136.3
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/60 , G01N33/44
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterizing a combinatorial library of non-biological polymer samples, the method comprising providing a combinatorial library comprising a plurality of non-biological polymer samples, each of the plurality of polymer samples being polymerization polymer mixtures resulting from polymerization reactions that are varied with respect to a factor affecting polymerization, serially injecting the plurality of polymer samples into a mobile phase of a liquid chromatography system, chromatographically separating at least one sample component of the injected samples from other sample components thereof in a chromatographic column having a stationary-phase and an aspect ratio ranging from about 0.1 to about 1, and detecting a property of at least one of the separated components of the plurality of samples.
摘要翻译：一种用于表征非生物聚合物样品的组合文库的方法，包括：提供一个组合文库，其包含非生物聚合物样品的复数，各自为聚合的聚合物混合物从聚合反应所得到的没有聚合物样品的多个方法是具有不同对于影响聚合，连续地注入聚合物样品的多元性到液相色谱系统的移动相，具有固定相色谱分离其他样品组分注入的样品的至少一个样品成分在色谱柱上和系数的纵横比为约0.1至约1，和检测样品的多个分离的部件中的至少一个的属性。

3. 发明公开

EP1308722A3 Rapid characterization of polymers with heated injection probe 审中-公开
标题翻译：通过加热的注射探针的装置的聚合物的快速表征
公开(公告)号：EP1308722A3
公开(公告)日：2004-08-04
申请号：EP03003137.1
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/02 , G01N33/44 , G01N30/88
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterising a polymer sample, the method comprising withdrawing a sample from a sample container into an injection probe of an auto-sampler, the injection probe being heated to maintain the withdrawn sample at a temperature of not less than about 75 °C while resident in the injection probe, the heated injection probe residing in a first environment maintained at about ambient temperature while withdrawing the polymer sample, loading at least a portion of the withdrawn sample into an injection port or a loading port of a liquid chromatography system or a flow injection analysis system, the injection port or loading port being adaptable for fluid communication with a chromatographic column or a flow injection analysis system, the chromatographic column residing in a heated second environment maintained at a temperature of not less than about 75 °C, injecting the loaded 5 ample into a mobile phase of the liquid chromatography system or a flow injection analysis system chromatographically separating the injected sample, as in the case of using liquid chromatography, detecting a property of the sample or of a component thereof and, maintaining the sample at a temperature of not less than about 75 °C during a period of time including from when the sample is withdrawn from the sample container to when the sample is within the heated second environment or when the property of the sample or of a component thereof is detected.

4. 发明公开

EP1310789A2 Rapid characterization of polymers with temperature control in a mixing zone 审中-公开
标题翻译： Schlerle Charakterisierung von Polymeren mittels in der MischzonedurchgeführterTemperaturregelung
公开(公告)号：EP1310789A2
公开(公告)日：2003-05-14
申请号：EP03003138.9
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/30 , G01N30/34
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterizing a non-biological polymer sample, the method comprising injecting a polymer sample into a mobile-phase of a liquid chromatography system, the mobile-phase being supplied to a liquid chromatography column from a mixing zone, the mixing zone being in fluid communication with a first reservoir containing a first mobile phase fluid at a first temperature, and with a second reservoir containing a second mobile phase fluid at a second temperature, controlling the temperature of the mobile-phase in the mixing zone to vary over time by varying the relative amounts of the first and second mobile-phase fluids supplied to the mixing zone, separating one or more sample components of the polymer sample in the chromatography column, and detecting a property of at least one of the separated sample components.
摘要翻译：一种用于表征非生物聚合物样品的方法，所述方法包括将聚合物样品注入到液相色谱系统的流动相中，将流动相从混合区域供应到液相色谱柱，混合区域与在第一温度下含有第一流动相流体的第一储存器以及在第二温度下含有第二流动相流体的第二储存器流体连通，控制混合区中流动相的温度随时间变化随时间变化改变供应到混合区的第一和第二流动相流体的相对量，分离色谱柱中的聚合物样品的一个或多个样品组分，并检测至少一个分离的样品组分的性质。

5. 发明公开

EP1308722A2 Rapid characterization of polymers with heated injection probe 审中-公开
标题翻译： on onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde onde
公开(公告)号：EP1308722A2
公开(公告)日：2003-05-07
申请号：EP03003137.1
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/30 , G01N30/16
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterising a polymer sample, the method comprising withdrawing a sample from a sample container into an injection probe of an auto-sampler, the injection probe being heated to maintain the withdrawn sample at a temperature of not less than about 75 °C while resident in the injection probe, the heated injection probe residing in a first environment maintained at about ambient temperature while withdrawing the polymer sample, loading at least a portion of the withdrawn sample into an injection port or a loading port of a liquid chromatography system or a flow injection analysis system, the injection port or loading port being adaptable for fluid communication with a chromatographic column or a flow injection analysis system, the chromatographic column residing in a heated second environment maintained at a temperature of not less than about 75 °C, injecting the loaded 5 ample into a mobile phase of the liquid chromatography system or a flow injection analysis system chromatographically separating the injected sample, as in the case of using liquid chromatography, detecting a property of the sample or of a component thereof and, maintaining the sample at a temperature of not less than about 75 °C during a period of time including from when the sample is withdrawn from the sample container to when the sample is within the heated second environment or when the property of the sample or of a component thereof is detected.
摘要翻译：用于表征聚合物样品的方法，所述方法包括将样品从样品容器中取出到自动进样器的注射探针中，所述注射探针被加热以将抽出的样品保持在不低于约75℃的温度，同时驻留在注射探针中，加热的注射探针位于保持在大约环境温度的第一环境中，同时抽出聚合物样品，将至少一部分抽出的样品加载到液相色谱系统的注入口或装载端口流动注射分析系统，注射口或装载口适用于与色谱柱或流动注射分析系统的流体连通，色谱柱位于保持在不低于约75℃的加热的第二环境中，注入将5荷载入液相色谱系统的流动相或流动注射分析系统色谱分离注入的样品，如在使用液相色谱法的情况下，检测样品或其组分的性质，并在一段时间内将样品保持在不低于约75℃的温度，包括当样品从样品容器中取出到样品处于加热的第二环境中或当检测到样品或其组分的性质时。

6. 发明公开

EP1308723A3 Rapid characterization of polymers by use of variable flow and light scattering 审中-公开
标题翻译：通过可变流量和光散射的聚合物的快速表征
公开(公告)号：EP1308723A3
公开(公告)日：2004-08-11
申请号：EP03003139.7
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/02 , G01N33/44 , G01N30/88
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterising a non-biological polymer sample, the method comprising injecting a non-biological polymer sample into a mobile phase of a continuous-flow light-scattering detector, advancing the injected sample toward a detection cavity of the detector, the flowrate of the sample-containing mobile phase having an advancing flowrate, V ADVANCE , while the injected sample is advanced toward the detection cavity, reducing the flowrate of the sample-containing mobile phase to a detection flowrate, V DETECT , detecting light scattered from the injected sample or from a component thereof in the detection cavity of the detector while the mobile-phase flowrate is reduced to the detection flowrate, V DETECT , and flushing the sample from the detection cavity after detecting the scattered light.

7. 发明公开

EP1310791A3 Rapid characterization of polymers with a high-aspect ratio column 审中-公开
标题翻译：通过具有高的长度对直径的比率列的装置的聚合物的快速表征
公开(公告)号：EP1310791A3
公开(公告)日：2004-08-04
申请号：EP03003136.3
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/02 , G01N33/44 , G01N30/88
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterizing a combinatorial library of non-biological polymer samples, the method comprising providing a combinatorial library comprising a plurality of non-biological polymer samples, each of the plurality of polymer samples being polymerization polymer mixtures resulting from polymerization reactions that are varied with respect to a factor affecting polymerization, serially injecting the plurality of polymer samples into a mobile phase of a liquid chromatography system, chromatographically separating at least one sample component of the injected samples from other sample components thereof in a chromatographic column having a stationary-phase and an aspect ratio ranging from about 0.1 to about 1, and detecting a property of at least one of the separated components of the plurality of samples.

8. 发明公开

EP1308723A2 Rapid characterization of polymers by use of variable flow and light scattering 审中-公开
标题翻译： Schnelle Charakterisierung von Polymeren durch variablen Fluss und Lichtstreuung
公开(公告)号：EP1308723A2
公开(公告)日：2003-05-07
申请号：EP03003139.7
申请日：1999-04-02
申请人： Symyx Technologies, Inc.
发明人： Carlson, Eric , Safir, Adam , Petro, Miroslav , Nielson, Ralph, B., , Lee, Thomas, S. , Frechet, Jean, M.J., , Dales, G., Cameron, , Kuebler, Sigrid, C., , Bennett,James
IPC分类号： G01N30/74 , G01N33/44
CPC分类号： G01N35/1097 , B01D15/12 , B01D15/14 , B01D15/26 , B01D15/265 , B01D15/325 , B01D15/34 , B01J19/26 , B01J20/28078 , B01J2219/00119 , B01J2219/00274 , G01N15/0205 , G01N30/16 , G01N30/30 , G01N30/60 , G01N30/6052 , G01N33/44 , G01N33/442 , G01N35/085 , G01N2015/0288 , G01N2015/0294 , G01N2030/347 , G01N2030/885 , G01N2030/8886
摘要： A method for characterising a non-biological polymer sample, the method comprising injecting a non-biological polymer sample into a mobile phase of a continuous-flow light-scattering detector, advancing the injected sample toward a detection cavity of the detector, the flowrate of the sample-containing mobile phase having an advancing flowrate, V ADVANCE , while the injected sample is advanced toward the detection cavity, reducing the flowrate of the sample-containing mobile phase to a detection flowrate, V DETECT , detecting light scattered from the injected sample or from a component thereof in the detection cavity of the detector while the mobile-phase flowrate is reduced to the detection flowrate, V DETECT , and flushing the sample from the detection cavity after detecting the scattered light.
摘要翻译：一种用于表征非生物聚合物样品的方法，所述方法包括将非生物聚合物样品注入连续流光散射检测器的流动相中，将注入的样品推向检测器的检测腔，流速含有样品的流动相具有提前的流速VADVANCE，同时注入的样品朝向检测腔前进，将包含样品的流动相的流量降低到检测流量VDETECT，检测从注入的样品散射的光或从其检测器的检测腔中的成分被移动相流量降低到检测流量VDETECT，并且在检测到散射光后从检测腔中冲洗样品。

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